• 한국세라믹학회지
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• 제39권11호
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• pp.1083-1089
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• 2002

알루미나 세라믹스에 MgO와 $TiO_2$를 각각 단독으로 첨가했을 때의 치밀화와 소결 거동을 수축률-소결 밀도 관계를 통해 비교 조사하였다. MgO가 첨가되었을 때는 소결 전과정을 통해 입성장은 억제되고 치밀화는 촉진되었으나, $TiO_2$가 첨가되었을 때는 입성장은 촉진된 반면 치밀화는 떨어졌다. 또한 입자 크기, 밀도, 수축률등을 통해 수축률-소결 밀도 관계를 구하여 최대 수축률을 나타내는 밀도값(Density of Maximum Shrinkage Rate:${\rho}$J.S.R)을 조사해 보았다. 이때 최대 수축률을 나타내는 밀도값보다 낮은 밀도를 보이는 영역에서는 치밀화가 입성장보다 우세하게 진행되었으며 최대 수축률을 나타내는 밀도값보다 높은 밀도의 영역에서는 입성장이 보다 우세하게 진행되는 것으로 추정하였다. 이때 최대 수축률을 나타내는 밀도값은 $TiO_2$가 첨가된 알루미나 < 순수 알루미나 < MgO가 첨가된 알루미나의 순서로 높은 값을 보였다.

• 대한기계학회논문집A
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• 제28권7호
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• pp.930-939
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• 2004

Constitutive models for final stage densification of metal powder compacts with power-law creep deformation were investigated. The constitutive models were implemented into a finite element program (ABAQUS) by using user subroutine CREEP and, from FEM results, useful densification curves were obtained when hydrostatic and uniaxial stress were applied to the powder compacts at various pressures and temperatures. Because the densification behavior varied as the constitutive models, the equivalent stress surface on each constitutive equation was investigated to analyze the difference of densification behavior.

• 대한기계학회논문집A
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• 제24권11호
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• pp.2749-2761
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• 2000

Densification, grain growth, and phase transformation of nanocrystalline ceramic powder were investigated under pressureless sintering, sinter forging, and hot pressing. A constitutive model for densification of nanocrystalline ceramic powder was proposed and implemented into a finite element program (ABAQUS). A grain growth model was also proposed by including the effect of applied stress on grain growth when phase transformation occurs. Finite element results by using the proposed models well predicted densification behavior, deformation, and grain growth of nanocrystalline titania powder during pressureless sintering, sinter forging, and hot pressing. Finite element results by using the proposed model also well predicted experimental data in the literature for densification behavior of nanocrystalline zirconia powder during pressureless sintering and sinter forging.

• 한국세라믹학회지
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• 제33권7호
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• pp.725-734
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• 1996

점토질 소지에 있어서 수축 특성은 성형, 건조 및 소성 공정에 수반되어 치말화거등에 기여할 수 있는 구동력이 될 수 있다. 점토질 소지에서 저수축 치말화거동은 입자크기효과와 상전이 특성에 기인하는 열간 반응전이 거동을 포함하는 공정변수에 따라 크게 변화됨을 보였다. 90$0^{\circ}C$ 및 120$0^{\circ}C$에서 열처리된 Chamotte의 첨가를 통해서 점토질 소지의 열간 치밀화 과정에 기인하는 공정수축은 크게 억제될 수 있었다. 120$0^{\circ}C$에서 열처리된 조대한 Chamotte 입자는 점토 소지의 치밀화 거동을 억제하여 치밀한 소결미세구조를 얻을 수는 없었지만, 조대한 Chamotte 입자의 첨가는 neat-net-shape 제어를 촉진할 수 있었다. 점토질 소지에 있어서 미세구조/물성간의 연관관계는 저수축과 치밀화 거동사이의 상반된 특성을 제어함으로써 얻어진 최적조건에 따라 직접적인 영향을 받을 것으로 판단되었다.

• 대한기계학회논문집A
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• 제32권4호
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• pp.333-339
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• 2008

Densification behavior of copper powder was investigated to study the effect of an aluminum mold under warm pressing. The low flow stress of an aluminum mold is appropriate to apply hydrostatic stress to powder compacts during compaction under high temperature. The suggested powder metallurgy process is very useful under high temperature since copper powder compacts have higher relative density over axial stress of 100 MPa and show more homogeneity as compared with conventional warm pressing. Elastoplastic constitutive equation proposed by Shima and Oyane was implemented into a finite element program (ABAQUS) for densification behavior under warn pressing by using a metal mold. Finite element results agreed well with experimental data for densification and deformation of copper powder compacts in the mold.

• 대한기계학회논문집A
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• 제24권2호
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• pp.394-402
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• 2000

Densification behavior of titanium alloy powder was investigated under hot isostatic pressing at various pressures and temperatures. Uniaxial creep responses of a dense specimen were also obtained at high temperatures. The densification model of Abouaf and co-workers was implemented into a Finite element program (ABAQUS) to compare with experimental data for titanium alloy powder. The agreements between finite element calculations and experimental data for deformation and densification of titanium alloy powder were good during hot isostatic pressing.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2000년도 춘계학술대회논문집A
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• pp.363-368
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• 2000

Densification, grain growth, and phase transformation of nanocrystalline ceramic powder were investigated under pressureless sintering, sinter forging, and hot pressing. A constitutive model for densification of nanocrystalline ceramic powder was proposed and implemented into a finite element program (ABAQUS). A grain growth model was also proposed by including the effect of applied stress on grain growth when phase transformation occurs. Finite element results by using the proposed models well predicted densification behavior, deformation, and grain growth of nanocrystalline titania powder during pressureless sintering, sinter forging, and hot pressing.

• 한국세라믹학회지
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• 제39권1호
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• pp.45-50
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• 2002

평균입경 25$\mu m$의 Si조대분말에 소결조제의 조성과 양을 변화시켜 질화반응 질화규소 (RBSN)세라믹스를 제조할 때 나타나는 치밀화 거동, 미세구조의 발달 및 기계적 특성에 대하여 고찰하였다. 6wt% $Y_2O_3$ + 1wt% $Al_2O_3$(6YlA)의 소결조제를 첨가한 경우에는 치밀화를 이루지 못하였으나, 6wt% $Y_2O_3+3\;wt%\;Al_2O_3+2\;wt%\;SiO_2(6Y3A2S)$와 9wt% $Y_2O_3$+1.5wt% $A1_2O_3$+ 3w% $SiO_2$(9Yl.5A3S)의 소결조제를 첨가하여 이론밀도에 가까운 치밀화를 이루었다. $1900^{\circ}C$에서 소결한 6Y3A2S시편의 경우, 960MPa의 높은 파괴강도값과 $6.5MPa.m^{1/2}$의 파괴인성값을 얻었다.

• 대한기계학회논문집A
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• 제26권7호
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• pp.1324-1331
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• 2002

Densification behavior of composite powders was investigated during cold compaction. Experimental data were obtained for aluminum alloy powder mixed with zirconia powder inclusion under triaxial compression. The Cap model with constraint factors was implemented into a finite element program (ABAQUS) to simulate compaction responses of composite powders during cold compaction. Finite element results were compared with experimental data for densification behavior of composite powders under cold isostatic pressing and die compaction. The agreements between experimental data and finite element calculations from the Cap model with constraint factors were good.

• 대한기계학회논문집A
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• 제24권3호
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• pp.735-742
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• 2000

Densification behaviors of mixed metal powder under high temperature were investigated. Experimental data of mixed copper and tool steel powder with various volume fractions of Cu powder were obtained under hot isostatic pressing and hot pressing. By mixing the creep potentials of McMeeking and co-workers and of Abouaf and co-workers originally for pure powder, the mixed creep potentials with various volume fractions of Cu powder were employed in the constitutive models. The constitutive equations were implemented into a finite element program (ABAQUS) to compare with experimental data for densification of mixed powder under hot isostatic pressing and hot pressing. Finite element calculations by using the creep potentials of Abouaf and co-workers agreed reasonably well with experimental data, however, those by McMeeking and co-workers underestimate experimental data as observed in the case of pure metal powders.