• Title/Summary/Keyword: Dense

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Microstructure and Mechanical Properties of the $Al_2O_3-SiC$ Ceramics Produced by Melt Oxidation (용융산화법으로 제조한 $Al_2O_3-SiC$ 세라믹스의 미세구조와 기계적 성질)

  • ;H. W. Hennicke
    • Journal of the Korean Ceramic Society
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    • v.31 no.10
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    • pp.1169-1175
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    • 1994
  • Five Al2O3/SiC/metal composites with four different particle sizes of green SiC abrasive grains are grown by the directed oxidation of an commercially available Al-alloy. Oxidation was conducted in air at 100$0^{\circ}C$, 96 hours long. Slip casted SiC-fillers were placed on the alloy or SiC powder deposited up to the required layer thickness. Their microstructures are described and measurements of density, elastic constants, frexural strength, fracture toughness and work of fracture are reported. The results are compared with those of commercial dense sintered Al2O3. The properties of produced materials have a strong relationship to not only the properties of Al2O3, SiC, Al and Si but also to the phase share and phase distribution. The composite materials are dense (0.5% porosity), tough (KIC = 3.4~6.4 MPa{{{{ SQRT { m} }}), strong ({{{{ sigma }}B = 170~345 MPa) and reasonably shrinkage free producible. The reinforcements is attained mainly through the plastic deformation of ductile metal phase.

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Effect of Slurry Property on Preparation of Zirconia Film in Electrophoretic Deposition (전착법에서 용액특성이 지르코니아 막형성에 미치는 영향)

  • 김상우;이병호;손용배;송휴섭
    • Journal of the Korean Ceramic Society
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    • v.36 no.9
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    • pp.991-996
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    • 1999
  • Effect of solution property on the weight varation and microstructural change of film was studied by electrophoretic deposition in order to obtain a homogeneous and dense zirconia film. As a result of weight kinetics of film which obtained in alcohol or aqueous solution having different polarity experimental data showed large deviation from theoretical ones calculated by Zhang's kinetic model. It had been shown that the weight affecting factors was largely dependent on properties other than dielectric constant and viscosity of solvent zeta potential appiled field and time. In initial stage a main factor of the drastic weight increase was the capillary drag of porous substrate. The cause of weight decrease with time in aqueous solution after 300 s was attributed to the defect of film by sagging and electrolytic reaction. The electrolyte film which prepared in alcohol solution with good wetting for substrate had better homogeneous and dense microstructure than one in aqueous solution with high surface tension.

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Preparation of Hydroxyapatite Powder Derived from Tuna Bone and Its Sintering Property (참치 뼈로부터 수산화아파타이트 분말의 제조 및 소결 특성)

  • Seo, Dong-Seok;Kim, Young-Gook;Hwang, Kyu-Hong;Lee, Jong-Kook
    • Journal of the Korean Ceramic Society
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    • v.45 no.10
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    • pp.594-599
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    • 2008
  • Hydroxyapatite(HA) was prepared from waste tuna bone, and its sintering property and dissolution behavior were investigated. Tuna bone derived-HA powder consisted of mainly HA and small amount of MgO. Porous HA ceramics with sintered density of 79% was obtained by pressureless sintering at $1200^{\circ}C$. Meanwhile, HA ceramics prepared by hot pressing at $1000^{\circ}C$ showed dense microstructure with sintered density of 95%. Immersion test revealed that both porous and dense HA ceramics were stable in liquid environment without distinct evidence of surface dissolution. It may be assumed that the presence of Mg in tuna bone-derived HA may improve dissolution resistance of HA.

Grain Boundary Protonic Conductivity in Highly Dense Nano-crystalline Y-doped BaZrO3

  • Park, Hee-Jung;Munir, Zuhair A.;Kim, Sang-Tae
    • Journal of the Korean Ceramic Society
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    • v.47 no.1
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    • pp.71-74
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    • 2010
  • We have investigated protonic conduction in highly dense (>98%) polycrystalline Y-doepd $BaZrO_3$ (BYZ) ceramic with an average grain size of ~85 nm. It is observed that the protonic conductivity across the grain boundaries in this nano-crystallilne BYZ (n-BYZ) is significantly higher than the microcrystalline counterpart. Such a remarkable enhancement in grain boundary conductivity results in high overall conductivity that may allow this chemically stable protonic conductor to serve as a solid electrolyte for low-temperature solid oxide fuel cell applications.

Eutectic Nanocomposites for Thermophotovoltaic Application

  • Han, Young-Hwan;Lee, Jae-Hyung;Kakegawa, Kazuyuki
    • Transactions on Electrical and Electronic Materials
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    • v.11 no.6
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    • pp.249-252
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    • 2010
  • The ground amorphous powder was consolidated into a dense sintered body with a typical ultrafine $Al_2O_3-GdAlO_3$ eutectic structure by spark plasma sintering (SPS). Sintered material with ultrafine and dense eutectic structure was obtained by an appropriate combination of rapid quenching and SPS at lower temperature and more quickly than by conventional sintering. The $Al_2O_3$-based rare earth eutectic ceramics for solar cell emitters are believed to have a higher efficiency and the $Al_2O_3$ based eutectic ceramics with ultrafine grains will be one of the promising materials showing excellent selective emitter characteristics.

Thermal Assisted UV-Ozone Treatment to Improve Reliability of Ag Nanoparticle Thin Films

  • Lee, Inhwa;Kim, Taek-Soo
    • Journal of the Microelectronics and Packaging Society
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    • v.21 no.1
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    • pp.41-44
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    • 2014
  • We employed UV-Ozone treatment method for the fabrication of dense and highly conductive nanoparticle thin films. We demonstrated the UV-Ozone treatment effect on the silver nanoparticle thin films as a function of time and temperature. The capping layers of nanoparticles were decomposed after UV-Ozone treatment and dense nanoparticle thin films were obtained. Moreover, electrical and mechanical properties of the thin films after UV-Ozone treatment were measured by using resistance measurements under tension in an in-situ tensile tester. The initial resistance of nanoparticle thin films was decreased by 82.6% with optimized UV-Ozone treatment condition of $150^{\circ}C$ for 20 minutes.

Effects of process variables on morphology of palladium metal deposit in hydrochloric acid medium

  • kim Min-Seuk;Lee Jae-Chun;Kim Won-Back;Jeong Jin-Ki;Nam Chul-Woo
    • 한국지구물리탐사학회:학술대회논문집
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    • 2003.11a
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    • pp.642-647
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    • 2003
  • Palladium is widely used for several applications and recovery of palladium from secondary sources becomes increasingly important since palladium is one of maldistributed platinum group metals. Electrochemical recovery of dense palladium metal sheet from Pd leaching solution is a simple and easily controlled method. The surface morphology of the recovered Pd metal was significantly affected by current density and temperature. Dense deposit morphology was in higher stress state regardless of preparation condition under $55^{\circ}C$. Rising temperature up to $70^{\circ}C$ had a stress releasing effect besides densification of Pd deposit.

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The Ultrastructure of Photoreceptor Cells in Frog Retina (개구리 망막에 있는 광수용세포의 미세구조)

  • Kim, Jin-Suk;Jeon, Jin-Seok
    • Applied Microscopy
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    • v.25 no.4
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    • pp.115-123
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    • 1995
  • This study was carried out to observe the functional ultrastructures of photoreceptor cells in frog(Rana catesbeiana) retina using transmission electron microscope. The photoreceptor cells are divided into two types-rod and cone cells-consist of outer and inner segment. The long outer segment of rod cell contains dense stacks of membrane and formed vertical and horizontal folds. The outer segment of cone cell is small, and vertical and horizontal folds are not exist. The electron dense cytoplasm of rod cell contains compact mitochondria, Golgi complexes, and endoplasmic reticula. The inner segment of cone cell shows low electron density and contains a large lipid droplet in the upper part of inner segment. In addition, cone cell contains many mitochondria, Golgi complexes. rough endoplasmic reticula, ribosomes and numerous glycogen particles. It is believed that these ultrastructural characteristics are closely associated with photoreceptive function of photoreceptor cells in frog retina.

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ALTERNATING DIRECTION IMPLICIT METHOD FOR TWO-DIMENSIONAL FOKKER-PLANCK EQUATION OF DENSE SPHERICAL STELLAR SYSTEMS

  • Shin, Ji-Hye;Kim, Sung-Soo
    • Journal of The Korean Astronomical Society
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    • v.40 no.4
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    • pp.91-97
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    • 2007
  • The Fokker-Planck (FP) model is one of the commonly used methods for studies of the dynamical evolution of dense spherical stellar systems such as globular clusters and galactic nuclei. The FP model is numerically stable in most cases, but we find that it encounters numerical difficulties rather often when the effects of tidal shocks are included in two-dimensional (energy and angular momentum space) version of the FP model or when the initial condition is extreme (e.g., a very large cluster mass and a small cluster radius). To avoid such a problem, we have developed a new integration scheme for a two-dimensional FP equation by adopting an Alternating Direction Implicit (ADI) method given in the Douglas-Rachford split form. We find that our ADI method reduces the computing time by a factor of ${\sim}2$ compared to the fully implicit method, and resolves problems of numerical instability.

A Study on Increase of Bearing Capacity of Dense Sandy Ground installed by Vertical Micropiles (연직 마이크로파일이 설치된 조밀한 모레지반의 지지력 증가에 관한 연구)

  • 최상민;임종철;이태형;공영주
    • Proceedings of the Korean Geotechical Society Conference
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    • 2001.03a
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    • pp.355-362
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    • 2001
  • Since micropiles were conceived in Italy in the early 1950s, which have been widely used for In-situ reinforcement, bearing pile or the concept of combination in the world-wide. The meaning of micropiles usually differs from that of a general deep foundation. Because the load capacity of it was mainly affected by skin friction. Also, it could be obtained the improvement effects of load capacity or ground's rigidity by the unitary behavior of ground and micropiles. In this study, The model tests were peformed on the dense sand where micropiles are set to the vertical direction. Strip footing was used in it. Steel bars of dia. 2 and 4㎜ were used in model tests of which the sand was attached on the surface, and the length of it was changed as 2B to 6B(where, B is width of strip footing) Through this process, the load capacity were analyzed from the test results in the relationship between load and displacement.

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