Browse > Article
http://dx.doi.org/10.4191/KCERS.2008.45.1.594

Preparation of Hydroxyapatite Powder Derived from Tuna Bone and Its Sintering Property  

Seo, Dong-Seok (Department of Advanced Materials Engineering, Chosun University)
Kim, Young-Gook (Department of Advanced Materials Engineering, Chosun University)
Hwang, Kyu-Hong (School of Nano and Advanced Materials Engineering, Gyeongsang National University)
Lee, Jong-Kook (Department of Advanced Materials Engineering, Chosun University)
Publication Information
Abstract
Hydroxyapatite(HA) was prepared from waste tuna bone, and its sintering property and dissolution behavior were investigated. Tuna bone derived-HA powder consisted of mainly HA and small amount of MgO. Porous HA ceramics with sintered density of 79% was obtained by pressureless sintering at $1200^{\circ}C$. Meanwhile, HA ceramics prepared by hot pressing at $1000^{\circ}C$ showed dense microstructure with sintered density of 95%. Immersion test revealed that both porous and dense HA ceramics were stable in liquid environment without distinct evidence of surface dissolution. It may be assumed that the presence of Mg in tuna bone-derived HA may improve dissolution resistance of HA.
Keywords
Hydroxyapatite; Tuna bone; Sintering; Hot pressing; Dissolution;
Citations & Related Records

Times Cited By SCOPUS : 1
연도 인용수 순위
1 L. L. Hench and J. Wilson, "An Introduction to Bioceramics," pp. 139-180, World Scientific, Singapore, 1993
2 H. Wang H, J. K. Lee, A. M. Moursi, D. Anderson, P. Winnard, H. Powell, and J. J. Lannutti, "Microstructural Disassembly of Calcium Phosphates," J. Biomed. Mater. Res., 68 61-70 (2004)
3 T. Nonami and F. Wakai, "Evaluation of Crack Propagation in Hydroxyapatite by Double-torsion Method in Air, Water and Toluene," J. Ceram. Soc. Jpn., 103 648-52 (1995)   DOI
4 J. T. Edwards, J. B. Brunski, and H. W. Higuchi, "Mechanical and Morphologic Investigation of the Tensile Strength of a Bone-hydroxyapatite Interface," J. Biomed. Mater. Res., 36 454-68 (1997)   DOI   ScienceOn
5 J. E. Davies and N. Baldan, "Scanning Electron Microscopy of the Bone-bioactive Implant Surface," J. Biomed. Mater. Res., 36 429-40 (1997)   DOI
6 H. K. Koerten and J. van der Meulen, "Degradation of Calcium Phosphate Ceramics," J. Biomed. Mater. Res., 44 78- 86 (1999)   DOI   ScienceOn
7 D. S. Seo and J. K. Lee, "Microstructural Disintegration in Dense Hydroxyapatite and Hydroxyapatite-coated Metal Implants," Metals and Materials Intl., 13 [4] 311-16 (2007)   DOI   ScienceOn
8 G. Daculsi, R. Z. LeGeros, and D. Mitre, "Crystal Dissolution of Biological and Ceramic Apatites," Calcif. Tissue Int., 45 95-103 (1989)   DOI
9 W. L. Suchanek, K. Byrappa, P. Shuk, R. E. Riman, V. F. Janas, and K. S. TenHuisen, "Preparation of Magnesiumsubstituted Hydroxyapatite Powders by the Mechanochemical- hydrothermal Method," Biomaterials 25 4647-57 (2004)   DOI   ScienceOn
10 W. Suchanek and M. Yoshimura, "Processing and Properties of Hydryoxyapatite-based Biomaterials for Use as Hard Tissue Replacement Implants," J. Mater. Res., 13 [1] 94-117 (1998)   DOI   ScienceOn