• Title/Summary/Keyword: Data Retention Time

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p-Coumaroylamino Acids from Yeast-Elicited Ephedra distachya Cultures

  • Song, Kyung-Sik;Sankawa, Ushio;Ebizuka, Yutaka
    • Archives of Pharmacal Research
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    • v.17 no.1
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    • pp.48-50
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    • 1994
  • Three p-coumaroylamino acids (p-CAAs) were isolated from the yeast-elicited Ephedra distachya cultures by consecutive purification using XAD_2, silicagel and RP-HPLC. Retention times on HPLC as well as their UV, IR, NMR and MS spectral data indicated that the yeast-induced p-CAAs wre p-coumaroyl--D-valine, p-coumaroyl-D-serine and p-coumarouyl-D-threonine, respectively. The structures of p-CAAs were confirmed by the comparison of their physico-chemical properties 3with those of synthetic ones. They were isolated and identified for the first time from natural products and supposed to be accumulated as phytoalexins of Ephedra.

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Chiral Separation of Tryptophan Enantiomers by Liquid Chromatography with BSA-Silica Stationary Phase

  • Kim Kwonil;Lee Kisay
    • Biotechnology and Bioprocess Engineering:BBE
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    • v.5 no.1
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    • pp.17-22
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    • 2000
  • The separation of tryptophan enantiomers was carried out with medium-pressure liquid chromatography using BSA (bovine serum albumin)-bonded silica as a chiral stationary phase. The influence of various experimental factors such as pH and ionic strength of mobile phase, separation temperature, and the presence of organic additives on the resolution was studied. In order to expand this system to preparative scale, the loadability of sample and the stability of stationary phase for repeated use were also examined. The separation of tryptophan enantiomers was successful with this system. The data indicated that a higher separation factor (a) was obtained at a higher pH and lower temperature and ionic strength in mobile phase. Addition of organic additives (acetonitrile and 2-propanol) in mobile phase contributed to reduce the retention time of L-tryptophan. About $30\%$ of the separation factor was reduced after 80 days of repeated use.

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Application of SMBR process in food wastewater advanced treatment (SMBR을 이용한 음식폐수의 고도처리)

  • 윤용수;강광남;정순형
    • Journal of environmental and Sanitary engineering
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    • v.16 no.1
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    • pp.34-39
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    • 2001
  • Submerged Membrane Bio-Reacter(SMBR) process was used to food wastewater treatment. From laboratory pilot-scale experiment data, it was confirmed that this process was very effective process for organics, suspended solid, and N, P treatment. It was found that BOD and COD removal rate were obtained 90% and 92%, respectively, for 150 days operation. Organics loading rate did not affect to the removal efficiency because MLSS concentration in aerobic tank was highly maintained. IN the case of first reactor operated with anoxic and second reactor operated as aerobic, T-N, T-P removal rate were obtained 93% and 95%, respectively. It was shown that removal efficiency could be maintained stable due to the complete removal of SS and sludge production decreased with increasing of sludge retention time.

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Isolation of Prenylated Isoflavonoids from Cudrania tricuspidata Fruits that Inhibit A2E Photooxidation

  • Uddin, Golam Mezbah;Lee, Hee-Ju;Jeon, Je-Seung;Chung, Dong-Hwa;Kim, Chul-Young
    • Natural Product Sciences
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    • v.17 no.3
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    • pp.206-211
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    • 2011
  • High-performance liquid chromatography coupled to an online $ABTS^+$-based assay (online HPLC-$ABTS^+$) system was used to determine the principal antioxidants in Cudrania tricuspidata fruits. Six prenylated isoflavonoids (1 - 6) were isolated from C. tricuspidata fruits according to the online HPLC-$ABTS^+$ system. The structures of isolated compounds, alpiniumisoflavone (1), 6,8-diprenylorobol (2), 6,8-diprenylgenistein (3), pomiferin (4), 4'-methylalpiniumisoflavone (5), and osajin (6) were identified by their retention time, UV spectra, ESI-MS, and NMR data. Among these compounds, 6,8-diprenylorobol (2) and pomiferin (4) reduced A2E photooxidation in a dose dependent manner.

Isolation and Identification of Biologically Active Components from Korean Valerian Roots (한국산 쥐오줌풀로부터 생리활성 성분의 분리 및 동정)

  • 김삼곤;김근수;김용하;이운철;안대진;김영회
    • Journal of the Korean Society of Tobacco Science
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    • v.25 no.1
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    • pp.80-86
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    • 2003
  • The contents of valepotriates, valerenic acid and their derivatives as mild sedative and antispamodic principles in two Korean valerian roots (Valeriana officinalis var. latifolia Miq. and V. fauriei var. dasycarpa Hara) were investigated and were compared with those in European valerian roots(Valeriana officinalis L.) by BPLC method. Among valepotriate compounds, valtrate was detected as a small amount in two Korean valerian roots, and iso-valtrate and dihydrovaltrate were detected as a trace amount. Among valerenic acid and their derivatives, valerenic acid were contained from 0.9∼3.46 mg/g base on dry weight. Over the vegetation periods investigated, the content of valepotriates remained more or less constant, hut the content of valerenic acid reached its maximum in 3-year old age. The compound isolated from Korean V. officinalis var. latifolia was elucidated as valerenic acid by spectroscopic data such as GC-MS, $^1$H-NMR and $^{13}$ C-NMR, and comparison of GC retention time with that of authentic compound.

Mass transfer characteristics of continuous electrocoagulation for dyestuff solution using aluminum flat plate electrode (Al 전극에 의한 염료의 전기응집에서 물질전달 특성)

  • Kim, Tak-Hyun;Park, Chulhwan;Shin, Eung-Bai;Kim, Sangyong
    • Proceedings of the KAIS Fall Conference
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    • 2001.05a
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    • pp.290-291
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    • 2001
  • The relationship between velocity, viscosity, diffusion coefficient, mass transfer coefficient and characteristic length and mass transfer data can be correlated by dimensionless relationship in electrolytic process. The performance of dyestuff removal was decreased as the flow rate of electrolyte was increased. It was due to the effect of retention time decreasing was superior to that of turbulent inlet mixing. Sh/Sc$\^$1/3/ vs Re plot for Al flat electrode did not showed the general tendency of the relationship between Sh/Sc$\^$1/3/ and Re. It can be thought that flow rate was not sufficiently high to increase the effect of mixing.

The Trap Characteristics of SILC in Silicon Oxide for SoC

  • Kang C. S.
    • Proceedings of the IEEK Conference
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    • summer
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    • pp.209-212
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    • 2004
  • In this paper, The stress induced leakage currents of thin silicon oxides is investigated in the nano scale structure implementation for Soc. The stress and transient currents associated with the on and off time of applied voltage were used to measure the distribution of high voltage stress induced traps in thin silicon oxide films. The stress and transient currents were due to the charging and discharging of traps generated by high stress voltage in the silicon oxides. The channel current for the thickness dependence of stress current, transient current, and stress induced leakage currents has been measured in oxides with thicknesses between $41\square\;and\;113.4\square,$ which have the channel width x length 10x1um, respectively. The stress induced leakage currents will affect data retention and the stress current, transient current is used to estimate to fundamental limitations on oxide thicknesses. The weight value of synapse transistor was caused by the bias conditions. Excitatory state and inhitory state according to weighted values affected the channel current. The stress induced leakage currents affected excitatory state and inhitory state.

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Comparisons of Middle- and Old-Aged Drivers' Recognition for Driving Scene Elements using Sensitivity, Response Bias, and Response Time (중년 및 고령운전자의 운전장면 개별요소에 대한 재인기억 차이: 민감도, 반응기준 및 반응시간 비교)

  • Lee, Jaesik
    • Journal of the Korean Data Analysis Society
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    • v.20 no.6
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    • pp.3185-3199
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    • 2018
  • Middle- and old-aged driver's capability in recognition for driving scene elements was compared. Central and ambient stimuli were selected from natural driving scene and sensitivity, bias and reaction time were measured as dependent measures. The results are as follows. First, in general, older drivers showed lower sensitivity than middle-aged drivers. In particular, the older drivers' sensitivity was significantly lower for the ambient stimuli than central stimuli, whereas the middle-aged drivers showed no significant difference between the two types of stimuli. Second, the older drivers tended to show more lenient responses whereas the middle-aged drivers responded more conservatively. Third, the older drivers showed longer reaction time than the middle-aged drivers, in particular, in the responses of miss and correct rejection. This results suggested that the older drivers' retention for driving scene elements in their working memory may not be stable, which can be resulted in difficulties in rapid and accurate responses in a real life driving.

Retention Effects of Dietary Education Program on Diet Knowledge, Diet Self-Care Compliance, Physiologic Indices for Hemodialysis Patients (혈액투석 환자의 식이 교육프로그램이 식이지식, 식이 자가간호 이행 및 생리적 지표에 미치는 지속효과)

  • Kim, Sang-Suk;Jo, Hyun Sook;Kang, Meung-Sue
    • Journal of Korean Biological Nursing Science
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    • v.19 no.2
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    • pp.51-59
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    • 2017
  • Purpose: The purpose of this study was to identify the retention effects of an individualized dietary education program for hemodialysis patients on diet knowledge, diet self-care compliance, and physiological indices, thus to find the most effective time period for re-education. Method: This study utilized one-group repeated pretest-posttest design. The participants were 52 hemodialysis patients in C hospital, Gyeonggi-Do. Data were collected at 4 and 12 weeks after the education from January through April 2016. Results: There was significant increases in diet knowledge even 12 weeks after the education (p= .007). Diet self-care compliance showed a significant increase at 4 weeks (p= .001), but a decrease at 12 weeks after the education. The level of blood natrium was significantly decreased between 4 and 12 weeks after the education (p= .006). The weight was significantly decreased at 12 weeks after the education. Conclusion: It has been identified that re-education for hemodialysis patients should be implemented between 4 and 12 weeks after education in order to maintain patients' diet self-care compliance, an ultimate aim of diet education. By helping them with their self-care compliance, the patients would maintain their physical and psychological function optimally, thus contributing to a better quality of life among hemodialysis patients.

Hydraulic Evaluation and Performance of On-Site Sanitation Systems in Central Thailand

  • Koottatep, Thammarat;Eamrat, Rawintra;Pussayanavin, Tatchai;Polprasert, Chongrak
    • Environmental Engineering Research
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    • v.19 no.3
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    • pp.269-274
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    • 2014
  • On-site sanitation systems are typically installed to treat grey and toilet wastewaters in areas without sewer and centralized treatment systems. It is well known that, due to inappropriate design and operation, treatment performance of these systems in developing countries is not satisfactory in the removal of pathogens and organic matters. This research aimed to investigate the hydraulic conditions occurring in some on-site sanitation systems and the effects of hydraulic retention times (HRTs) on the system performance. The experiments were conducted with a laboratory-scale septic tank (40L in size) and an actual septic tank (600L in size), to test the hydraulic conditions by using tracer study with HRTs varying at 12, 24 and 48 hr. The experimental results showed the dispersion numbers to be in the range of 0.017-0.320 and the short-circuit ratios in the range of 0.014-0.031, indicating the reactors having a high level of sort-circuiting and approaching complete-mix conditions. The removal efficiency of $BOD_5$ was found to be 67% and the $k_{30}$ values for $BOD_5$ was $2.04day^{-1}$. A modified complete-mix model based on the relationship between $BOD_5$ removal efficiencies and HRTs was developed and validated with actual-scale septic tank data having a correlation coefficient ($R^2$) of 0.90. Therefore, to better protect our environment and minimizing health risks, new generation toilets should be developed that could minimize short-circuiting and improving treatment performance.