• Title/Summary/Keyword: DSC measurement

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A Study on Thermal & Electrical Performance of Glazings with DSC modules (염료감응태양전지(DSC)를 적용한 Glazing의 구성에 따른 단열 및 전기 성능 분석)

  • kim, Ji-Seong;Park, Se-Hyeon;Kang, Jun-Gu;Kim, Jun-Tae
    • 한국태양에너지학회:학술대회논문집
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    • 2011.11a
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    • pp.158-163
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    • 2011
  • Recently, more attention has been paid to DSC(Dye-sensitized Solar Cell) with the potential of glazing applications. The aim of the study is to analyze thermal and electrical performance according to composition of glazing with DSC. For this study, the electrical and thermal performance of glazing with DSC modules were measured and their result were compared. The measurement were performed according to the KS L2525 and with a solar simulator of DSC modules. The result show that the U-value of the DSC double glazings with clear glass and low-e glass were 2.78 $W/m^2K$ and 1.70 $W/m^2K$, respectively. The electrical measurement indicated that the electrical efficiency of the DSC double glazings with clear glass and low-e glass decreaced by 9.9% and 13.3%, respectively, compared to the DSC medules electrical performance.

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Current Status of Heat Capacity Measurement Techniques for Ionic Liquids by DSC (DSC를 이용한 이온성 액체 열용량 측정 기술 현황)

  • Jo, Ye Lim;Kim, Ki-Sub;Park, Byung Heung
    • Journal of Institute of Convergence Technology
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    • v.4 no.1
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    • pp.5-8
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    • 2014
  • Recently ionic liquids received much attention as novel materials capable of replacing traditional solvents. The applicability of the ionic liquids should be determined based on their physico-chemical properties. Heat capacity is one of the most important properties to be considered when a process is developed using the ionic liquids and currently DSC has been proved as an effective technique to measure the heat capacity. Micro DSCII can measure heat capacities of various liquids by both an isothermal step method and a scanning method. DSC Q100 and MDSC are able to measure heat capacities of several ionic liquids. For each ionic liquid linear regression of the heat capacity as a function of temperature has been performed to increase accuracy. To investigate the feasibility of ionic liquids as PCMs, their heat capacities have been measured by using Pysis I DSC. This paper briefly summarizes the present techniques of measuring heat capacities of ionic liquids by DSC.

Analysis of cure behavior of low temperature curing liquid silicone rubber (LSR) for multi-material injection molding (이중사출 성형을 위한 저온 경화 액상실리콘고무 (LSR)의 경화 거동 분석)

  • Hyeong-min Yoo
    • Design & Manufacturing
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    • v.17 no.1
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    • pp.1-5
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    • 2023
  • In multi-material injection molding, since two or more materials with different process conditions are used, it is essential to maximize process efficiency by operating the cooling or heating system to a minimum. In this study, Liquid silicone rubber (LSR) that can be cured at a low temperature suitable for the multi-material injection molding was selected and the cure behavior according to the process conditions was analyzed through differential scanning calorimetry (DSC). Dynamic measurement results of DSC with different heating rate were obtained, and through this, the total heat of reaction when the LSR was completely cured was calculated. Isothermal measurement results of DSC were derived for 60 minutes at each temperature from 80 ℃ to 110 ℃ at 10 ℃ intervals, and the final degree of cure at each temperature was calculated based on the total heat of reaction identified from the Dynamic DSC measurement results. As the result, it was found that when the temperature is lowered, the curing start time and the time required for the curing reaction increase, but at a temperature of 90 ℃ or higher, LSR can secure a degree of cure of 80% or more. However, at 80 ℃., it was found that not only had a relatively low degree of curing of about 60%, but also significantly increased the curing start time. In addition, in the case of 110 ℃, the parameters were derived from experimental result using the Kamal kinetic model.

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Studies on the Maximum Bound Water Content by the Differential Scanning Calorimetry on Lipstick (립스틱에서 DSC를 이용한 최대결합수량에 관한 연구)

  • Choi, Khee-Hwan;Ann, Myung-Jin;Son, Hong-Ha;Kim, Kyong-Seub;Lee, Sang-Min;Jeong, Ji-Hee
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.38 no.3
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    • pp.197-200
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    • 2012
  • To develop lipstick products with superior moisturizing effect using moisture base, bound water capacity and water holding capacity were investigated by DSC. Bound water capacity of the lipstick sample excluding moisture base is found to be 5.12 %. DSC measurement showed that bound water capacity and the concentration of moisture base were positively correlated. Additionally, DSC measurements and in vitro effective water holding capacity measurement showed similar patterns. Therefore, measuring of bound water capacity by DSC can predict the moisturizing effect of lipstick products.

A Study on the Wigner Energy Release Characteristics of Irradiated Graphite of KRR-2 (연구로 2호기 중성자 조사 흑연의 Wigner 에너지 방출 특성 연구)

  • Jeong Gyeong-Hwan;Yun Sei-Hun;Lee Dong-Gyu;Jung Chong-Hun;Lee Keun-Woo
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.4 no.3
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    • pp.209-216
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    • 2006
  • Characteristics of heat release process, while the Wigner energy was drawn off the graphite during DSC(Differential Scanning Calorimenter) measurement as an example of annealing process which is one of release methods of Wigner energy that is contained in the irradiated graphite, was studied. Linear temperature rise method in DSC operation was selected to estimate the total Wigner energy content and the heat release rate of each graphite samples, which were located in several positions in the thermal column in KRR-2 research reactor. As an annealing process in DSC operation Wigner energy of the irradiated graphite samples were totally released by heat supplying to the graphite from room temperature to $500^{\circ}C$, in DSC. Characteristics of Wigner energy release from the graphite sample was well correlated with the various activation energy model of the kinetic equation.

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A Study on Transformation of Dynamic DSC Results into Isothermal Data for the Formation Kinetics of a PU Elastomer

  • Ahn, WonSool
    • Elastomers and Composites
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    • v.53 no.2
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    • pp.52-56
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    • 2018
  • The present study examines the transformation of dynamic DSC data into the equivalent isothermal data for the formation kinetics of a polyurethane elastomer. The reaction of 2'-dichloro-4,4'-methylenedianiline (MOCA) with a PTMG/TDI-based isocyanate prepolymer was evaluated. DSC measurement was performed in the dynamic scanning mode with several different heating rates to obtain the reaction thermograms. Then, the data was transformed into the isothermal data through a procedure based on Ozawa analysis. The main feature of this procedure was the transformation of $({\alpha}-T)_{\beta}$ curves from dynamic DSC into $({\alpha}-t)_T$ curves using the isoconversional $(t-T)_{\alpha}$ diagram. Validity was discussed for the relationship between the dynamic DSC data and the transformed isothermal results.

A Correlation Analysis between DSC (Dye Sensitized Cell) and Daylighting-Focusing on Educational Space (염료감응형 태양전지(DSC)와 자연채광의 상관관계 분석-교육공간을 중심으로)

  • Lee, Eung-Jik
    • Journal of the Korean Solar Energy Society
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    • v.40 no.1
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    • pp.35-47
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    • 2020
  • Due to the large window area, the lighting environment of the educational space between the window and deep part of the room is not uniformly illuminated, and the phenomenon of glare is severe. For this reason, the daylight performance of DSC-BIPV windows was analyzed in order to improve the natural lighting in the educational sector. The method derives the correlation with natural lighting by measurement and simulation. Dynamic simulation confirmed that the average illuminance of the target space was higher at later than the early afternoon. The performance of natural lighting at 40% and 30% transmission of DSC has the effect of significantly reducing the amount of excess light in existing windows. Nevertheless, the actual average illuminance in all seasons corresponds to the standard illuminance of the educational facility, 300 Lux. In addition, the uniformity is also seen through the skylight illuminance ratio.

Freezing Behaviors of Frozen Foods Determined by $^1H$ NMR and DSC

  • Lee, Su-Yong;Moon, Se-Hun;Shim, Jae-Yong;Kim, Yong-Ro
    • Food Science and Biotechnology
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    • v.17 no.1
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    • pp.102-105
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    • 2008
  • The freezing patterns of commercial frozen foods were characterized by using proton nuclear magnetic resonance ($^1H$ NMR) relaxometry and differential scanning calorimetry (DSC). The liquid-like components like unfrozen water were investigated as a function of temperature (10 to $-40^{\circ}C$) and then compared with the unfrozen water content measured by DSC. The formation of ice crystals and the reduction of water in the foods during freezing were readily observed as a loss of the NMR signal intensity. The proton NMR relaxation measurement showed that the decreasing pattern of the liquid-like components varied depending on the samples even though they exhibited the same onset temperature of ice formation at around $0^{\circ}C$. When compared with the unfrozen water content obtained by the DSC, the NMR and DSC results could be closely correlated at the temperature above $-20^{\circ}C$. However, the distinct divergence in the values between 2 methods was observed with further decreasing temperatures probably due to the solid glass formation which was not detected by DSC.

Study on the Thermal Property and Aging Prediction for Pressable Plastic Bonded Explosives through ARC(Heat-wait-search method) & Isothermal Conditions (ARC(Heat-wait-search method)와 Isothermal 조건을 이용한 압축형 복합화약의 열적 특성 및 노화 예측 연구)

  • Lee, Sojung;Kim, Seunghee;Kwon, Kuktae;Jeon, Yeongjin
    • Journal of the Korean Society of Propulsion Engineers
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    • v.22 no.4
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    • pp.55-60
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    • 2018
  • The thermal property is one of the most important characteristics in the field of energetic materials. Because energy materials release decomposition heat, differential scanning calorimetry (DSC) is frequently used for thermal analysis. However, thermodynamic events, such as melting can interfere with DSC kinetic analysis. In this study, we use isothermal mode for DSC measurement to avoid thermodynamic issues. We also merge accelerating rate calorimetry(ARC) data with DSC data to obtain a robust prediction results for small scale samples and for large scale samples as well. For the thermal property prediction, advanced kinetics and technology solutions(AKTS) programs are used.

A Study on application of EMC to Digital Selective Calling VHF Transceiver for Maritime mobile service (해상이동업무용 디지털선택호출 VHF 송수신장치의 EMC 적용에 관한 연구)

  • 임종근;이동식;김기문
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2002.05a
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    • pp.529-534
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    • 2002
  • It was recommended for all ship engaged in international voyages to carry the dedicated Digital Selective Calling receiver, DSC equipment, VHF transceiver, etc according to Global Maritime Distress & Safety System. Also International Maritime Organization recommended for navigation and communication equipments to applicate the EMC regulations, therefore most of electronic equipments using in the vessel to be faced with problems to cope with new regulations. This study has applied and analyzed the EMC for an equipment integrated with Ch.70 dedicated DSC receiver, DSC equipment, VHF transceiver and groped for solutions to cope with. The test has applied the electromagnetic interference such as the measurement for unwanted emissions from conductive & radio emission and the electromagnetic susceptibility such as the immunity from voltage, frequency variation and electro static discharge, hence comes to be understand the problems related with the power and the earth.

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