• Title/Summary/Keyword: DMAC

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The study of bloody fingerprint enhancement on paper with chemical reagents (화학시약들을 이용한 지류에서 혈흔지문 증강에 관한 연구)

  • Lim, Seung;Kim, Im-Soon;Noh, Jong-Yun;Kim, Sang-Il;Yu, Je-Sul
    • Analytical Science and Technology
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    • v.25 no.5
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    • pp.284-291
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    • 2012
  • Bloody fingerprint is a very important evidence. In this study, we confirmed the enhancement effects of ninhydrin, leucocrystal violet (LCV), fuchsin acid, iodine and dimethylaminocinnamaldehyde (DMAC) on bloody fingerprints which were deposited on paper. Bloody fingerprint were deposited on paper sequentially and used after drying at room temperature. If a ridge of bloody fingerprint was clear, ninhydrin and LCV was the most effective but was not good for invisible ridge. Fuchsin acid reagent dyed paper surface so that the contrast of enhanced bloody fingerprint was decreased. Although bloody fingerprint was enhanced with iodine reagent, but the developed color was very weak after reaction. We thought that the enhancement effect of iodine to bloody fingerprint was negligible. Also, the enhancement effect of DMAC reagent to relatively clear bloody fingerprint was not good. However, it was very effective to faint or invisible ridge. By washing with methanol, contrast of enhanced bloody fingerprint was increased.

Effects of Mixed Casting Solvents on Morphology and Characteristics of Sulfonated Poly(aryl ether sulfone) Membranes for DMFC Applications (직접 메탄올 연료전지용 술폰화 폴리아릴에테르술폰 전해질 막의 혼합 캐스팅 용매에 따른 형태 및 특성)

  • Hong, Young-Taik;Park, Ji-Young;Choi, Jun-Kyu;Choi, Kuk-Jong;Hwang, Taek-Sung;Kim, Hyung-Joong
    • Membrane Journal
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    • v.18 no.4
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    • pp.282-293
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    • 2008
  • Partially sulfonated poly(aryl ether sulfone) membranes were prepared from the sulfonated sulfone monomer, which was synthesized by a nucleophilic substitution, non-sulfonated monomers and potassium carbonate by a direct polymerization method and a subsequent solution casting technique with mixed solvents of N-methyl-2-pyrrolidone (NMP) and dimethylacetamide (DMAc). To investigate the effect of mixed solvent, the volume ratios of NMP and DMAc were varied in the range of $0{\sim}100%$ and the degrees of sulfonation of the copolymers were fixed as 50%. The surface properties of the resulting membranes were examined by scanning electron microscope (SEM) and atomic force microscope (AFM), and a comparative study of the morphology changes and the physicochemical properties such as proton conductivity and methanol permeability was achieved. It was found that proton conductivities depend on the volume ratio of NMP-DMAc mixed solvents, and the proton conductivity determined at the condition of $25^{\circ}C$ and 100% relative humidity was $1.38{\times}10^{-1}\;S/cm$ for the membrane prepared in the 50:50 v/v-% of NMP : DMAc mixed solvent.

Design and Implementation of DMA priority section module (DMA Priority selection module 설계 및 구현)

  • Hwang, In-Ki
    • Proceedings of the KIEE Conference
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    • 2002.11c
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    • pp.264-267
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    • 2002
  • This paper proposed a effective priority selection algorithm named weighted round-robin algorithm and show the implementation result of DMAC priority selection module using prosed weighted round-robin algorithm. I parameterize timing constraints of each functional module, which decide the effectiveness of system. Proposed weighted round-robin algorithm decide the most effective module for data transmission using parameterize timing constraints and update timing parameter of each module for next transmission module selection. I implement DMAC priority selection module using this weighted round-robin algorithm and can improve the timing effective for data transmission from memory to functional module or one functional module to another functional module.

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Development of Antimicrobial and Deodorizing Cellulose Fiber (항균방취 셀룰로오스섬유 제조에 관한 연구)

  • 홍영근
    • Textile Coloration and Finishing
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    • v.10 no.1
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    • pp.38-42
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    • 1998
  • Both cellulose and chitin together were dissolved in DMAc/LiCl and these solutions were extruded into coagulant of $DMAc/H_2O$. Fibers thus obtained were treated in NaOH aqueous solution. Results showed that the fiber surface contains celluose and chitosan. This means that these fibers treated are composed of three components, ie, cellulose, chitin, and chitosan. These fiber showed secure antibacterial and mechanical properties.

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Effects of Coagulants and Annealing on Properties of Regenerated Cellulose Fibers (재생셀룰로오스섬유 물성에 대한 응고액과 열처리의 효과)

  • Hong, Young Keun
    • Textile Coloration and Finishing
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    • v.7 no.4
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    • pp.54-60
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    • 1995
  • Cellulose(cell)/dimethylacetamide(DMAc)/lithium chloride(LiCl) solutions were prepared and spun to fibers in coagulants. Then, obtained fibers were annealed in appropriate chemicals. The fibers from cell/DMAc/LiCl showed cell III morophology prior to annealing without differenciating the kind of coagulants. Morphology of crystallite, however, was affected by annealing. Annealed fibers at 17$0^{\circ}C$ showed cell IV morphology and had better mechanical properties than others.

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Synthesis and Properties of Polybenzoxazole Precursors having Oligo(oxy ethylene) pendant (Oligo(oxy ethylene) pendant를 갖는 PBO 전구체의 합성 및 특성)

  • Lee, Eung-Jae;Yoon, Doo-Soo;Bang, Moon-Soo;Choi, Jae-Kon
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.14 no.5
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    • pp.2550-2558
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    • 2013
  • Poly(o-hydroxyamides)(PHAs) copolymers having oligo(oxy ethylene) pendant in the main chain were synthesized by solution polycondensation reaction at low temperature. Copolymer precursors were studied by fourier transform infrared(FT-IR), differential scanning calorimeter(DSC), thermogravimetric analyzer(TGA), universal testing machine(UTM) and limited oxygen index(LOI). The inherent viscosities of the PHAs measured at $35^{\circ}C$ in DMAc or DMAc/LiCl solution were in the range of 0.74~1.42 dL/g. Solubility of the precursors with higher oligo(oxy ethylene) unit was increased, but the PBOs were nearly insoluble in a variety of solvents. The degradation temperature of the copolymer precursors was recorded in the ranges of $408{\sim}664^{\circ}C$ in nitrogen and char yields showed 13~59% values at $900^{\circ}C$. The mechanical properties and flame retardancy of copolymer precursors decreased with higher oligo(oxy ethylene) unit.

A Medium Access Control Mechanism for Distributed In-band Full-Duplex Wireless Networks

  • Zuo, Haiwei;Sun, Yanjing;Li, Song;Ni, Qiang;Wang, Xiaolin;Zhang, Xiaoguang
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • v.11 no.11
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    • pp.5338-5359
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    • 2017
  • In-band full-duplex (IBFD) wireless communication supports symmetric dual transmission between two nodes and asymmetric dual transmission among three nodes, which allows improved throughput for distributed IBFD wireless networks. However, inter-node interference (INI) can affect desired packet reception in the downlink of three-node topology. The current Half-duplex (HD) medium access control (MAC) mechanism RTS/CTS is unable to establish an asymmetric dual link and consequently to suppress INI. In this paper, we propose a medium access control mechanism for use in distributed IBFD wireless networks, FD-DMAC (Full-Duplex Distributed MAC). In this approach, communication nodes only require single channel access to establish symmetric or asymmetric dual link, and we fully consider the two transmission modes of asymmetric dual link. Through FD-DMAC medium access, the neighbors of communication nodes can clearly know network transmission status, which will provide other opportunities of asymmetric IBFD dual communication and solve hidden node problem. Additionally, we leverage FD-DMAC to transmit received power information. This approach can assist communication nodes to adjust transmit powers and suppress INI. Finally, we give a theoretical analysis of network performance using a discrete-time Markov model. The numerical results show that FD-DMAC achieves a significant improvement over RTS/CTS in terms of throughput and delay.

A Study on Magnetic Properties of Amphiphilic Polymer Networks Nanocomposites by Mossbauer Spectroscopy (뫼스바우어 분광법에 의한 양친매성 고분자 망상구조 나노복합체의 자기적 성질 연구)

  • Yoon, In-Seop
    • Journal of the Korean Magnetics Society
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    • v.20 no.6
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    • pp.216-221
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    • 2010
  • Magnetic nanocomposites contained iron oxide were synthesized by through cross-linking polymerization of dimethylacetamide (DMAc) solution and toluen solution on the amphiphilic polymer networks based on urethan acrylate nonionomer (UAN) precursor chains. For the study on microscopic structures and magnetic properties of the magnetic nanoparticles, FESEM and XRD and Mossbauer spectroscopy were used. The results investigated show that there are magnetic nanoparticles of $Fe_2O_3$ in samples and the magnetic nanocomposites contained iron oxide in polymer networks of UAN using DMAc solution are more smaller than using toluen solution. All of the Fe ions in the samples present $Fe^{3+}$ and the magnetic property of samples are paramagnetic by superparamagnetic effect at room temperature.

Norfloxacin Release from Surfactant-Free Nanoparticles of Poly(DL-lactide-co-glycolide) and Biodegradation (계면활성제를 사용하지 않는 Poly(DL-lactide-co-glycolide) 나노입자로부터의 Norfloxacin 방출과 생분해 특성)

  • 권중근;정영일;장미경;이창형;나재운
    • Polymer(Korea)
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    • v.26 no.4
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    • pp.535-542
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    • 2002
  • We have prepared the surfactant-free nanoparticles of poly(DL-lactide-co-glycolide) (PLGA) by dialysis method and their physicochemical properties such as particle size and drug contents were investigated against various solvent. The size of PLGA nanoparticles prepared by using dimethylacetamide (DMAc), dimethylformamide (DMF), and dimethylsulfoxide (DMSO) was smaller than that from acetone. Also, the order of drug contents was DMAc>DMF>DMSO=acetone. These phenomena could be expected from the fact that solvent affects the size of nanoparticles and drug contents. The PLGA nanoparticles have a good spherical shapes as observed from scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Also, surfactant-free nanoparticles entrapping norfloxacin (NFx) have a good drug loading capacity without free-drug on the surface of nanoparticles confirmed by the analysis of X-ray powder diffraction. Release kinetics of NFx used as a model drug was governed not only by drug contents but also by particle size. Also, the biodegradation rate of PLGA nanoparticles prepared from DMF was faster than that prepared from acetone, indicating that the biodegradation of PLGA nanoparticles is size-dependent.

Preparation and Water Vapor Barrier Properties of PET/Nanohybrid PI Films (폴리에스테르/폴리이미드 나노복합필름의 제조 및 수분차단 특성)

  • Han, Seung San;Kim, Yong Seok;Won, Jong Chan;Lee, Jae Heung;Choi, Kil-Yeong
    • Journal of Adhesion and Interface
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    • v.5 no.1
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    • pp.29-35
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    • 2004
  • We have prepared polyster/nanQhybridized polyimide films in the range of 1~9 wt% of organophilic synthetic layered silicate (STN). Firstly, poly(amic acid)/STN nanocomposite solutions were prepared via solution blending method in DMAc or THF/MeOH solution, and then cast on the polyester film followed by imidization reaction, thermal and chemical method repestively. XRD and TEM experiment showed that the STN was fully exfoliated through the polyimide matrix. Surface morphologies of nanohybridized polyimide films were characterized by AFM and thermal, mechanical properties were also confirmed by TGA, DMA and UTM each. And also, the water vapor permeabilities highly depended on the content of STN. The sample from chemical imidization route and THF/MeOH solvent system showed better water vapor barrier properties than thermal one and DMAc system.

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