• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 1993.11a
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• pp.3-3
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• 1993

In mechanical testing of W-Ni-Pe heavy alloys, the cracks nucleate at W/W interface and propagate through W/ Imatrix interface or through matrix phase together with the cleavage of W grains. The mechanical properties can therefore be improved by control of the interfacial strength and area. In this presentation, some experimental result and techniques on this subject will be reviewed and discussed. The hydrogen embrittlement caused by the hydrogen segregation at interfaces during sintering in an hydrogen atmosphere can be removed by an heat-treattnent in vacuum or in an inert atmosphere. The heat-treatment condition can be estimated by using a diffusion equation for a cylindrical shape. The mechanical properties, in particular the impact property, are degraded by the segregation of non-metallic impurities, such as Sand P. The degradation can be prevented by adding a fourth element, such as La or Ca, active with the non-metallic impurities. The cyclic heat-treatment at usual heat-treattnent tempemture causes the penetration of matrix between W/W grain boundaries and results in remarkable increase in impact energy. This is due to an increase in the area of ductile failure during the impact test. The instability of W/matrix interface casued by addition of Mo or Re can be controlled by using W powders of different size. The increase in the interfacial area in found to be related to the presence of non-equilibrium pure W gmins among W(Mo or Re) solid solution gmins.

• The korean journal of orthodontics
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• v.52 no.6
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• pp.412-419
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• 2022

Objective: This study evaluated the effect of cyclic pre-calcification treatment on the improvement of bioactivity and osseointegration of Ti-6Al-4V mini-screws. Methods: The experimental groups were: an untreated group (UT), an anodized and heat-treated group (AH), and an anodized treatment followed by cyclic pre-calcification treatment group (ASPH). A bioactive material with calcium phosphate was coated on the mini-screws, and its effects on bioactivity and osseointegration were evaluated in in vitro and in vivo tests of following implantation in the rat tibia. Results: As a result of immersing the ASPH group in simulated body fluid for 2 days, protrusions appearing in the initial stage of hydroxyapatite precipitation were observed. On the 3rd day, the protrusions became denser, other protrusions overlapped and grew on it, and the calcium and phosphorus concentrations increased. The removal torque values increased significantly in the following order: UT group (2.08 ± 0.67 N·cm), AH group (4.10 ± 0.72 N·cm), and ASPH group (6.58 ± 0.66 N·cm) with the ASPH group showing the highest value (p < 0.05). In the ASPH group, new bone was observed that was connected to the threads, and it was confirmed that a bony bridge connected to the adjacent bone was formed. Conclusions: In conclusion, it was found that the surface treatment method used in the ASPH group improved the bioactivity and osseointegration of Ti-6Al-4V orthodontic mini-screws.

• Journal of the Korea institute for structural maintenance and inspection
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• v.26 no.4
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• pp.1-10
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• 2022

In this study, to evaluate the possibility of using a steel spring as a displacement-dependent damping device, tensile loading and cyclic loading tests were performed. The main experimental variables were the type of steel (SAE9254 and SS275), the spring constant (700 N/mm, 1,000 N/mm, and 1,400 N/mm), and the presence or absence of heat treatment for SAE9254. As a result of the tensile test, the ratios of the measured spring constant to the design spring constant of the steel springs made with SAE9254 ranged from 1.08 to 1.13, while the ratios of the design spring constant and the measured spring constant of the steel springs made with SS275 ranged from 0.86 to 0.97. After yielding, the slope values of the load-displacement curve of the SAE9254 with/without heat treatment were about 240~251 N/mm and 92 N/mm, respectively, but the slope values of the load-displacement response of SS275 were almost zero. According to the uniaxial cyclic loading test results, all specimens were satisfied with three conditions for a displacement-dependent damping device in KDS 41 17 00 (2019): the maximum force and minimum force at zero displacement, the maximum force and minimum force at the maximum displacement, and the energy dissipation capacity. In addition, the equivalent damping ratios of steel springs made with SAE9254(non-heat treatment) and SS275 were approximately 2.8 times and 1.9 times greater, respectively, than that of steel springs made with SAE9254.

• Nuclear Engineering and Technology
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• v.46 no.1
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• pp.117-124
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• 2014

The effect of various process variables on the powder properties of recycled $U_3O_8$ from MnO-$Al_2O_3$ doped large grain $UO_2$ pellets and the effect of those recycled $U_3O_8$ powders on the sintered density and grain size of MnO-$Al_2O_3$ doped large grain $UO_2$ pellets have been investigated. The evolution of morphology, size, and BET surface area of the recycled $U_3O_8$ powders according to the respective variation of the thermo-mechanical treatment variables of oxidation temperature, powder milling, and sequential cyclic heat treatment of oxidation and then reduction was examined. The correlation between the BET surface area of recycled $U_3O_8$ powder and the sintered pellet properties of MnO-$Al_2O_3$ doped pellets showed that the pellet density and grain size of doped pellets were increased and then saturated by increasing the BET surface area of the recycled $U_3O_8$ powder. The density and grain size of the pellets were maximized when the BET surface area of the recycled $U_3O_8$ powder was in the vicinity of $3m^2/g$. Among the process variables applied in this study, the cyclic heat treatment followed by low temperature oxidation was a potential process combination to obtain the sinter-active $U_3O_8$ powder.

• Journal of Korea Foundry Society
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• v.25 no.1
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• pp.23-29
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• 2005

Mechanical characteristics of Hi-Cr cast irons containing 16.8%Cr and 3.0%C were studied with various heat treatments. After as-cast Y-block ingots were annealed fully, the ingots were machined into cylinderical specimens with the size of 9mm in diameter and 20mm in length in order to investigate the effect of heat-treatments on mechanical characteristics of high Cr cast irons. All specimens were heat-treated by quenching- tempering, austempering and cyclic heat at the various temperatures(950, 1000, 1050 and $1100^{\circ}C$) respectively. The wear amount was measured for each heat-treated specimens against the counterpart of a hardened SKD11 steel at the following conditions; wearing velocity: 0.7 m/s, load: 100N and sliding distance: 70 km. After as-cast specimens were annealed, fine $M_{3}C$ carbides were formed, which affected the hardness and the wear resistance of Hi-Cr specimens. High hardness and good wear resistance were appeared on the specimens treated at 950 and $1000^{\circ}C$ and the austempered specimens show excellent wear resistance as well as high hardness.

• Korean Journal of Materials Research
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• v.9 no.11
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• pp.1144-1147
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• 1999

The effect of the heat treatment on electrochromic properties of $\textrm{MoO}_3$ thin films is investigated by studing optical modulation, optical density, response time, and cyclic voltammetry. From the results of XRD analysis, heat-treated at $450^{\circ}C$ in air for 1 hour Moo3 thin films are found to be crystalline while as-deposited and heat- treated at low temperature ($\leq\;300^{\circ}C$) film are amorphous. The electrochromic devices using as-deposited $\textrm{MoO}_3$ films exhibit good electrochromic properties compared to those using the heat treated $\textrm{MoO}_3$ films. It has shown that the heat-treatment affected the reversible color change and the electrochromic properties of $\textrm{MoO}_3$ films.

• Journal of Urban Science
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• v.7 no.1
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• pp.5-9
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• 2018

The nickel-titanium shape memory alloy (SMA), referred to as Nitinol, exhibits a superelastic effect that can be restored to its original shape even if a significant amount of deformation is applied at room temperature, without any additional heat treatment after removal of the load. Owing to these unique material characteristics, it has widely used as displacement control devices for seismic retrofitting in civil engineering fields as well as medical, electrical, electronic and mechanical fields. Contrary to ordinarty carbon steel, superelastic SMAs are very resistant to fatigue, and have force-displacement properties depending on loading speed. The change for the mechanical properties of superelastic SMAs are experimentally inviestigated in this study when loading cycle numbers and loading speeds are different. In addition, the standardized force-displacement properties of such superelastic SMAs are proposed with an aim to efficiently design the seismic retrofitting devices made of these materials.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.28 no.9
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• pp.1391-1398
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• 2004

Railway wheels and axles belong to the most critical components in railway vehicles. The service conditions of railway vehicles became more severe in recent years due to the increase of speed. Therefore, a more precise evaluation of wheelset life and safety has been requested. Wheel/rail contact fatigue and thermal cracks due to braking heat are two main mechanisms of the railway wheel failure. In this paper, an evaluation procedure for the contact fatigue life of railway wheel is proposed. One of the main sources of the contact zone failure is the residual stress. The residual stress on wheel is formed during the manufacturing process which includes a heat treatment, and then is changed by contact stress developed by wheel/rail contact and thermal stress induced by braking. Also, the cyclic stress history for fatigue analysis is determined by applying finite elements analysis for the moving contact load. The objective of this paper is to estimate fatigue life by considering residual stress due to heat treatment, braking and repeated contact load, respectively.

• Journal of the Korean Ceramic Society
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• v.50 no.6
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• pp.480-484
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• 2013

Since SiOC was introduced as an anode material for lithium ion batteries, it has been studied with different chemical compositions and microstructures using various silicon based inorganic polymers. Poly(phenyl carbosilane) is a SiOC precursor with a high carbon supply in the form of the phenyl unit, and it has been investigated for film applications. Unlike any other siloxane-based polymers, oxygen atoms must be utilized in an oxidation process, and the amount of oxygen is controllable. In this study, SiOC anodes were prepared using poly(phenyl carbosilane) with different heat treatment conditions, and their electrochemical properties as an anode material for lithium ion batteries were studied. In detail, cyclic voltammetry and charge-discharge cycling behavior were evaluated using a half-cell. A SiOC anode which was prepared under a heat treatment condition at $1200^{\circ}C$ after an oxidation step showed stable cyclic performance with a reversible capacity of 360 mAh/g.

• Journal of the Microelectronics and Packaging Society
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• v.6 no.2
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• pp.69-74
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• 1999

Graphite and carbonaceous materials intercalate and deintercalate Li-ion reversibly into their layered structures. These materials show an excellent capacity for using a negative electrode in Li-ion batteries, because the electrochemical potential of Li-ion intercalated carbon is almost identical with that of lithium metal. Carbon used in this study was obtained by the pyrolysis of petroleum pitch, and heat-treated at the several temperatures between $700^{\circ}C$ and $1300^{\circ}C$. XRD analysis revealed that crystallization of carbon increased with increasing the heat treatment temperature. Charge/discharge properties were studied by a constant-current step at the rate of 0.1C, and the interfacial reaction between the electrolyte and the surface of carbon electrode was studied by cyclic voltammetry. Cell capacities were investigated in terms of the heat treatment temperature and the cycle number. Reversible capacity increased with the heat treatment temperature up to $1000^{\circ}C$, thereafter decreased continuously. Also, charge capacity decreased with the cycle number, while the reversibility improved with it.