• Title/Summary/Keyword: Cyanoacrylate

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A study on the optimal conditions for latent fingerprint development using cyanoacrylate fuming method in vacuum chamber (시아노아크릴레이트 진공 훈증법에 의한 잠재지문 현출 최적화에 관한 연구)

  • Yu, Je-Seol;Jung, Jin-Sung;Lim, Seung;Park, Sung-Woo
    • Analytical Science and Technology
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    • v.25 no.3
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    • pp.164-170
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    • 2012
  • Cyanoacrylate fuming mehod is effective for latent fingerprints developing on non-porous surfaces. In this study, we investigated optimal conditions for latent fingerprint development using cyanoacrylate fuming method in vacuum chamber. The effects of temperature, relative humidity, fuming method and processing time were checked throughly. The amount of evaporated cyanoacrylate was increased at higher temperature, but cyanoacrylate polymerization on the fingerprint ridge was best at $30^{\circ}C$. With a relative humidity of 40% to 50% conditions, good quality of fingerprints were developed. If a relative humidity is lower than 30% or higher than 60%, polymerization rate of cyanoacrylate monomers on the fingerprint ridge was decreased. It was identified that application of $OMEGA-PRINT^{TM}$ dispersal pad or cotton ball with sodium hydroxide fuming method in vacuum chamber was more effective than natural fuming method. We found that cyanoacrylate processing time in vacuum chamber did not have more significant than relative humidity.

Comparing intra-oral wound healing after alveoloplasty using silk sutures and n-butyl-2-cyanoacrylate

  • Suthar, Pratik;Shah, Sonal;Waknis, Pushkar;Limaye, Gandhali;Saha, Aditi;Sathe, Pranav
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • v.46 no.1
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    • pp.28-35
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    • 2020
  • Objectives: The need for proper wound closure is of paramount importance after any intra-oral surgery. Various wound closure techniques have been described in literature using traditional non-absorbable suture materials. These include like synthetic absorbable sutures, surgical staples and tissue adhesives. Cyanoacrylates are among the most commonly used biocompatible tissue adhesives. To evaluate and compare intraoral wound healing using 3-0 silk sutures and n-butyl-2-cyanoacrylate after alveoloplasty. Materials and Methods: A total of 20 patients requiring bilateral alveoloplasty in the same arch (upper or lower) were included in this study. Patients with any pre-existing pathology or systemic disease were excluded. After alveoloplasty was performed, the wound was closed using 3-0 braided silk sutures on one side, and using n-butyl-2-cyanoacrylate bio adhesive on the other side. Patients were evaluated based on the following parameters: time required to achieve wound closure; the incidence of immediate and postoperative hemostasis; the time to the use of the first rescue medication; the side where pain first arises; and the side where wound healing begins first. Results: Compared to 3-0 silk sutures, cyanoacrylate demonstrated better hemostatic properties, reduced operative time, reduced postoperative pain and better wound healing. Conclusion: These data suggest that cyanoacrylate glue is an adequate alternative to conventional sutures to close the surgical wound after alveoloplasty, and better than are 3-0 silk sutures.

CYANOACRYLATE ADHESIVE FOR CLOSING OF SINUS MEMBRANE PERFORATION DURING SINUS LIFTS (상악동거상술시 발생된 상악동점막 천공의 폐쇄를 위한 Cyanoacrylate 접착제)

  • Choi, Byung-Ho;Zhu, Shi-Jiang;Kim, Byung-Young;Huh, Jin-Young;Lee, Seoung-Ho;Jung, Jae-Hyung
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • v.30 no.6
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    • pp.526-529
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    • 2004
  • Aim: To assess the efficacy of cyanoacrylate adhesive in the management of large perforations of the maxillary sinus membrane during sinus lifts. Material and methods: Eight rabbits were used in the study. Sinus membrane perforation(about 1.5cm) was repaired with cyanoacrylate adnesive on one side of the maxillary sinus and the opppsite side was used as a control. Histological evaluation was performed 4 weeks after the operation. Results: Histological studies showed normal healing of the sinus membrane across the site of previous perforation and no evidence of inflammation. Conclusion: Our results support the clinical use of cynoacrylate adhesive for repairing sinus membrane perforation.

Closure of a Postoperative Bronchopleural Fistula with Bronchoscopic Instillation of n-butyl-2-cyanoacrylate ($Histoacryl^{(R)}$) (N-butyl-2-cyanoacrylate($Histoacryl^{(R)}$)을 이용한 기관지흉막루의 치료 1예)

  • Cho, Jae-Hwa;Lee, Hong-Lyeol;Ryu, Jeong-Sun;Chun, Jeong-Bae;Lee, Don-Haeng;Yoon, Yong-Han;Kim, Kwang-Ho
    • Tuberculosis and Respiratory Diseases
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    • v.47 no.4
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    • pp.543-548
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    • 1999
  • Bronchopleural fistula(BPF) occurs as a postoperative complication in 2 to 5 percent of pulmonary resection. The detection of BPF is generally difficult and various diagnostic methods have been utilized to identify the site of the fistula in order to treat it adequately. Closure of these BPF can be surgical intervention or bronchoscopic application of various sealing agents. We report an experience with use of bronchoscopic instillation of n-butyl-2-cyanoacrylate($Histoacryl^{(R)}$) for closure of a postpneumonectomy BPF.

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Clinical usefulness of fixation of absorbable implants with cyanoacrylate in comminuted fractures of the maxilla

  • Ju, Gang San;Son, Kyung Min;Choi, Woo Young;Cheon, Ji Seon
    • Archives of Craniofacial Surgery
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    • v.20 no.4
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    • pp.233-238
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    • 2019
  • Background: The open reduction of craniofacial bone fractures requires internal fixation using metal plates and screws, which have been considered the gold standard. However, metal implants pose a risk of palpation, protrusion, and foreign body reaction, and they may require an additional operation for removal. Recently, good results have been reported for absorbable implants which complement the disadvantages of metal implants. This study presents the results of using absorbable mesh, plates, and screws with cyanoacrylate for more accurate and firmer fixation of comminuted fractures of the maxilla. Methods: In total, 235 patients underwent operations for comminuted fractures of the maxilla. From January 2012 to December 2014, absorbable mesh and screws were used in 114 patients, while from January 2015 to December 2017, absorbable mesh, plates, and screws with cyanoacrylate were used in 121 patients. Open reduction of the bone fragments was performed, after which absorbable implants were accurately molded and fixed by screws. Results: All patients underwent postoperative computed tomography scans, which showed highly accurate reduction and firm fixation in the patients who underwent procedures using absorbable implants, screws, and cyanoacrylate. There were no postoperative complications or cases of abnormal facial contour. Conclusion: When absorbable implants and screws are used for maxillary fractures, no additional surgery to remove the metal plate is required. In addition, the use of cyanoacrylate enables accurate and firm fixation of the tiny bone fragments that cannot be fixed with screws.

A Study on the Reaction Rate and Cause Analysis of Cyanoacrylate Adhesives According to the Coating Mixtures for Metal Artifacts (금속유물 코팅제와 Cyanoacrylate 접착제의 반응속도 및 원인분석: 초기접착속도를 중심으로)

  • Kwon, Hee-Hong;Huh, Il-Kwon;Kim, Soo-Ki
    • Journal of Conservation Science
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    • v.27 no.2
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    • pp.135-144
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    • 2011
  • When metal artifacts have to undergo conservation treatment, the person in charge of the treatment selects and uses various coating mixtures based on his judgment regarding their condition, material, or environment. Since the kinds of coating mixtures or solvents make a difference in the set time of cyanoacrylate adhesives, they have something to do with the efficiency of the conservation treatment. This study examines the effects and causes that affect the set time of cyanoacrylate adhesives according to the kinds of coating mixtures and solvents and suggests ways to increase the set time. As a result, it is thought that as the surface roughness gets flatter, the wettability of adhesive is improved further, which increases the set time. Moreover, the C-F binding of V-Flon, C-O-C absorption peak, molecular weight of the coating mixtures, and glass transition temperature (Tg) were the factors that significantly affected the set time. According to the result of measuring the set time based on the result of superficial and chemical analysis, relative difference was shown according to the kind and viscosity of adhesive, but all the adhesives indicated the following order of the set time: V-Flon > Paraloid B-72 (in xylene) > Paraloid NAD-10 > Paraloid B-72 (in acetone).

Comparison of aging fingerprint enhancement by pre-treatment of various initiator powders in the cyanoacrylate fuming method (다양한 개시제(initiator)분말 전처리(pre-treatment)를 통한 노화된 지문의 Cyanoacrylate Fuming법 현출 증강 비교)

  • Kim, Kyung-Soo;Lee, Yoon-Jeong;Seo, Kyung-Suk
    • Analytical Science and Technology
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    • v.35 no.3
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    • pp.129-135
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    • 2022
  • We tested the pre-treatment of alumina, leucine, alumina mixed with leucine at ratios of 9:1 (Al-Leu (9:1)) and 5:1 (Al-Leu (5:1)), and alumina mixed with sodium lactate at a ratio of 5:1 (Al-Lac (5:1)) on aged fingerprints (1, 7, 14, and 30 days after natural fingerprinting) before cyanoacrylate (CA) fuming to improve the development efficacy. As a result of the experiment, fingerprints with pre-treatment of alumina, leucine, Al-Leu (9:1), Al-Leu (5:1), and Al-Lac (5:1) showed better development efficacy (area and minutiae) than fingerprints without pre-treatment. Therefore, this modified CA fuming method improved the development efficacy with five pretreatments.

Synthesis of Alternating Head-to-Head Copolymer of Methyl $\alpha$-cyanoacrylate and 2,3-Dihydrofuran. Ring-Opening Polymerization of 3-Methoxy-4-cyano-2,9-dioxabicyclo[4.3.0]non-3-ene

  • Lee, Ju-Yeon;Cho, I-Whan
    • Bulletin of the Korean Chemical Society
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    • v.9 no.3
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    • pp.176-179
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    • 1988
  • 3-Methoxy-4-cyano-2,9-dioxabicyclo[4.3.0]non-3-e ne (1) was prepared by (4 + 2) cycloaddition reaction of methyl ${\alpha}$-cyanoacrylate with 2,3-dihydrofuran. Compound 1 was ring-open polymerized by cationic catalyst such as boron trifluoride etherate to obtain alternating head-to-head (H-H) copolymer (2) of methyl $\alpha$ -cyanoacrylate and 2,3-dihydrofuran. For comparison, head-to-tail (H-T) copolymer (3) was also prepared by free radical copolymerization of the corresponding monomers. The H-H copolymer exhibited minor differences in its $^1H$-NMR and IR spectra, but in the $^{13}C$-NMR spectra significant differences were observed between the H-H and H-T copolymers. All of the H-H and H-T copolymers were soluble in common solvents and the inherent viscosities were in the range 0.2-0.3 dl/g.

A study on Enhancement Effectiveness of Cyanoacrylate Fumed Fingermark by the Solvent of Rhodamine 6G (Rhodamine 6G 용매에 따른 CA 훈증 지문 증강 효과에 관한 연구)

  • Shim, Yea-Ra;Yu, Je-Seol
    • The Journal of the Korea Contents Association
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    • v.17 no.7
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    • pp.294-302
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    • 2017
  • In this study, latent fingermarks deposited in porous or non-porous surface was developed by cyanoacrylate fuming, and then the developed fingermark is enhanced by using Rhodamine 6G. Between water-based R6G and organic solvent-based R6G, author studied about which material have higher effectiveness in enhancing fingermark. In all seven types of surfaces depositing fingermark, water-based R6G have higher effectiveness in enhancing fingermark and lower surface coloring than organic solvent-based R6G. But because the surfaces found in crime scene have multicolor background and various quality, the additional study about various surfaces is needed.

Core-shell Poly(D,L-lactide-co-glycolide )/Poly(ethyl 2-cyanoacrylate) Microparticles with Doxorubicin to Reduce Initial Burst Release

  • Lee, Sang-Hyuk;Baek, Hyon-Ho;Kim, Jung-Hyun;Choi, Sung--Wook
    • Macromolecular Research
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    • v.17 no.12
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    • pp.1010-1014
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    • 2009
  • Monodispersed microparticles with a poly(D,L-lactide-co-glycolide) (PLGA) core and a poly(ethyl 2-cyanoacrylate) (PE2CA) shell were prepared by Shirasu porous glass (SPG) membrane emulsification to reduce the initial burst release of doxorubicin (DOX). Solution mixtures with different weight ratios of PLGA polymer and E2CA monomer were permeated under pressure through an SPG membrane with $1.9\;{\mu}m$ pore size into a continuous water phase with sodium lauryl sulfate as a surfactant. Core-shell structured microparticles were formed by the mechanism of anionic interfacial polymerization of E2CA and precipitation of both polymers. The average diameter of the resulting microparticles with various PLGA:E2CA ratios ranged from 1.42 to $2.73\;{\mu}m$. The morphology and core-shell structure of the microparticles were observed by scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The DOX release profiles revealed that the microparticles with an equivalent PLGA:E2CA weight ratio of 1:1 exhibited the optimal condition to reduce the initial burst of DOX. The initial release rate of DOX was dependent on the PLGA:E2CA ratio, and was minimized at a 1:1 ratio.