• Journal of Dental Rehabilitation and Applied Science
• /
• v.31 no.1
• /
• pp.1-9
• /
• 2015

Purpose: The purpose of this study was to evaluate the mechanical properties of several dual-cure cements by different curing modes. Materials and Methods: One resin-modified glass ionomer cement (FujiCEM 2), two conventional dual-cure resin cements (RelyX ARC, Multilink N), and two dual-cure self-adhesive resin cements (RelyX U200, G-CEM LinkAce) were used. To evaluate the influence of the curing methods, each cements divided into four conditions (n = 20); Condition 1: self-curing for 10 minutes, Condition 2: immediate after 20 seconds light-curing, Condition 3: 24 hours after self-curing, Condition 4: 24 hours after light-curing. The compressive strength and diametral tensile strength were measured with a universal testing machine. All data were statistically analyzed using t-test, one-way ANOVA and Scheffe's test. Results: The results showed the compressive strength and diametral tensile strength after 24 hours in all curing modes were higher than immediate except RelyX ARC light-cured and Multilink N light-cured. The FujiCEM 2 showed lowest values (P < 0.05). Conclusion: The outcome was cement-depend, but there is no significant difference about compressive strength and diametral tensile strength between dual-cure self-adhesive resin cements and conventional resin cements. And this result will be used as a base line data selecting resin cement for favorable long-term prognosis.

• The Journal of Advanced Prosthodontics
• /
• v.7 no.4
• /
• pp.317-322
• /
• 2015

PURPOSE. The aim was to evaluate the effect of curing mode and different dentin surface pretreatment on microtensile bond strength (${\mu}TBS$) of self-adhesive resin cements. MATERIALS AND METHODS. Thirty-six extracted human permanent molars were sectioned horizontally exposing flat dentin surface. The teeth were divided into 12 groups (3 teeth/group) according to the dentin surface pretreatment methods (control, 18% EDTA, 10% Polyacrylic acid) and curing mode (self-curing vs. light-curing) of cement. After pretreatment, composite resin blocks were cemented with the following: (a) G-CEM LinkAce; (b) RelyX U200, followed by either self-curing or light-curing. After storage, the teeth were sectioned and ${\mu}TBS$ test was performed using a microtensile testing machine. The data was statistically analyzed using one-way ANOVA, Student T-test and Scheffe's post-hoc test at P<.05 level. RESULTS. For G-CEM LinkAce cement groups, polyacrylic acid pretreatment showed the highest ${\mu}TBS$ in the self-cured group. In the light-cured group, no significant improvements were observed according to the dentin surface pretreatment. There were no significant differences between curing modes. Both dentin surface pretreatment methods helped to increase the ${\mu}TBS$ of RelyX U200 resin cement significantly and degree of pretreatment effect was similar. No significant differences were found regarding curing modes except control groups. In the comparisons of two self-adhesive resin cements, all groups within the same pretreatment and curing mode were significantly different excluding self-cured control groups. CONCLUSION. Selecting RelyX U200 used in this study and application of dentin surface pretreatment with EDTA and polyacrylic acid might be recommended to enhance the bond strength of cement to dentin.

• Restorative Dentistry and Endodontics
• /
• v.33 no.5
• /
• pp.428-434
• /
• 2008

The purpose of this study was to compare the microtensile bond strength in Class I cavities associated with different light curing modes of same light energy density. Occlusal enamel was removed to expose a flat dentin surface and twenty box-shaped Class I cavities were prepared in dentin. Single Bond (3M Dental product) was applied and Z 250 was inserted using bulk technique. The composite was light-cured using one of four techniques, pulse delay (PD group), soft-start (SS group), pulse cure (PC group) and standard continuous cure (CC group). The light-curing unit capable of adjusting time and intensity (VIP, Bisco Dental product) was selected and the light energy density for all curing modes was fixed at $16J/cm^2$. After storage for 24 hours, specimens were sectioned into beams with a rectangular cross-sectional area of approximately $1mm^2$ Microtensile bond strength $({\mu}TBS)$ test was per- formed using a univel·sal testing machine (EZ Test, Shimadzu Co.). The results were analyzed using oneway ANOVA and Tukey's test at significance level 0.05. The ${\mu}TBS$ of PD group and SS group was higher than that of PC group and CC group. Within the limitations of this in vitro study, modification of curing modes such as pulse delay and soft start polymerization can improve resin/dentin bond strength in Class I cavities by controlling polymerization velocity of composite resin.

• Journal of the korean academy of Pediatric Dentistry
• /
• v.46 no.1
• /
• pp.57-63
• /
• 2019

This study aimed to determine whether the curing times of Xtra Power and High Power modes of high-power light emitting diode (LED) curing light are sufficient for polymerization of resin sealants. The specimens were prepared and their microhardness values were measured and compared with those of specimens polymerized under conventional LED curing light. The filled sealant polymerized for 8 seconds in the High Power mode and for 3 seconds in the Xtra Power mode showed significantly lower microhardness than the control specimen (p = 0.000). The unfilled sealant polymerized for 8, 12 seconds in the High Power mode and for 6 seconds in the Xtra Power mode showed significantly lower microhardness than the control specimen (p = 0.000). The results of this study suggest that the short curing time with the Xtra Power and High Power modes of highpower LED curing light are not sufficient for adequate polymerization of sealants under specific conditions, taking into account the curing times and the type of sealant.

• Journal of the korean academy of Pediatric Dentistry
• /
• v.33 no.2
• /
• pp.221-232
• /
• 2006

The purpose of this study was to investigate the effect of step-curing mode on polymerization shrinkage and contraction of composite resin restoration. Class I cavities were prepared on the extracted human premolars. The cavities were ailed with Filtek $Z-250^{TM}$ (hybrid resin, 3M ESPE, USA) and Filtek $flow^{TM}$ (flowable resin, 3M ESPE, USA) and cured with one of the following irradiation modes; Halogen 40sec with continuous curing, LED 10sec with continuous curing, and LED 13sec with step-curing. Contraction stress was measured with strain gauge which was connected to TML $Datalogger^{TM}$ (TDS-102, SOKKI, Japan) and resin-dentin interfaces were observed by scanning electron microscope. The results of present study can be summarized as follows : 1. Composite resin restoration showed transient expansion just after irradiation of curing light. Contraction stress was increased rapidly at the early phase of polymerization and reduced slowly as time elapsed (P<0.05) 2. $Filtek\;flow^{TM}$ showed lower contraction stress than Filtek $Z-250^{TM}$ regardless of curing modes. 3. LED step-curing mode showed lowest contraction stress in Filtek $Z-250^{TM}$ compared with other curing modes(P<0.05). 4. LED step-curing mode showed lowest contraction stress in $Filtek\;flow^{TM}$ compared with other curing modes(P<0.05), but difference in contraction stress was not so greate as in $Filtek\;Z-250^{TM}$. 5. Polymerization of composite resin by LED light with step-curing mode and halogen light with continuous ode resulted in better marginal sealing than LED light with continuous mode.

• Proceedings of the KIPE Conference
• /
• 2006.06a
• /
• pp.532-533
• /
• 2006

In this research work attempts were made to study the bonding of thermoplastics with adhesives using solar energy. In order to study the curing behaviour necessary experiments were conducted under varying conditions of temperature, exposure time and power. The cured samples were then studied under the optical microscope before subjecting to tensile testing in order to study their mechanical properties. The fracture surfaces were further studied under the Scanning Electron Microscopy in order to study the microstructural changes that are taken place during curing. From the present study it is evident that curing under higher solar energy temperature, generally improves bond strength and quality of the adhesive joints when compared to other modes of curing process expect the microwave curing process.

• Advances in concrete construction
• /
• v.7 no.4
• /
• pp.277-288
• /
• 2019

The formulation of self-compacting concretes (SCC) and the study of their properties at the laboratory level were currently well mastered. The aim of this work is to characterize SCC under hot climatic conditions and their effects on the properties of fresh and hardened SCC. Particularly, the effect of the initial wet curing time on the mechanical behavior such as the compressive strength and the durability of the SCCs (acid and sulfate attack) as well as the microstructure of SCCs mixtures. In this study, we used two types of cement, Portland cement and slag cement, three water/binder (W/B) ratio (0.32, 0.38 and 0.44) and five curing modes. The obtained results shows that the compressive strength is strongly influenced by the curing methods, 7-days of curing in the water and then followed by a maturing in a hot climate was the optimal duration for the development of a better compressive strength, regardless of the type of binder and the W/B ratio.

• Journal of the korean academy of Pediatric Dentistry
• /
• v.32 no.2
• /
• pp.312-320
• /
• 2005

The purpose of this study was to evaluate the polymerization contraction and the microhardness of compostie resin($Supreme^{(R)}$, Filtek $Flow^{(R)}$, 3M-ESPE, USA) according to irradiation modes of LED curing unit(Elipar $Freelight^{(R)}$, 3M-ESPE, USA). The strain guage method was used for determination of polymerization contraction. Sample were divided by 6 groups according to curing modes and filling method. Group A: $Supreme^{(R)}$, Filtek $Flow^{(R)}$ lining, 10seconds curing, Group B: $Supreme^{(R)}$, Filtek $Flow^{(R)}$ lining, 15seconds curing, Group C: $Supreme^{(R)}$, Filtek $Flow^{(R)}$ lining, 15seconds soft start curing, Group D: $Supreme^{(R)}$ only, 10seconds curing, Group E: $Supreme^{(R)}$ only, 15seconds curing, Group F: $Supreme^{(R)}$ only, 15seconds soft start curing. Preparations of acrylic molds were followed by filling and curing. Strain guage attached to each sample were connected to a strainmeter. Measurements were recorded at each second for the total of 10 minutes including the periods of light application. And microhardness of each group after 24hours from light irradiation were measured. Obtained data were analyzed statistically using Repeated measures ANOVA and Tukey test. The results of the present study are as follows: 1. In flowable resin liner group, soft start curing group was not found decrease of polymerization contraction. But, In Supreme only filling group, the lowest polymeriation contraction was found in soft start curing group. 2. 10 seconds curing group showed statistically significant reduction of polymerization contraction compared with 15 seconds curing group(p<0.05). 3. The microhardness values of each group not revealed significant difference(p>0.05). But, lower surface microhardness was not reached 80% of upper surface microhardness.

• Restorative Dentistry and Endodontics
• /
• v.32 no.1
• /
• pp.28-36
• /
• 2007

The purpose of this study was to compare the effect of exponential curing method with conventional curing and soft start curing method on polymerization shrinkage of composite resins. Three brands of composite resins (Synergy Duo Shade, Z250, Filtek Supreme) and three brands of light curing units (Spectrum 800, Elipar Highlight, Elipar Trilight) were used. 40 seconds curing time was given. The shrinkage was measured using linometer for 90 seconds. The effect of time on polymerization shrinkage was analysed by one-way ANOVA and the effect of curing modes and materials on polymerization shrinkage at the time of 90s were analysed by two-way ANOVA. The shrinkage ratios at the time of 20s to 90s were taken and analysed the same way. The results were as follows : 1. All the groups except Supreme shrank almost within 20s Supreme cured by soft start and exponential curing had no further shrinkage after 30s (p < 0.05). 2. Statistical analysis revealed that polymerization shrinkage varied among materials (p = 0.000) and curing modes (p = 0.003). There was no significant interaction between material and curing mode. 3. The groups cured by exponential curing showed the statistically lower polymerization shrinkage at 90s than the groups cured by conventional curing and soft start curing (p < 0.05). 4. The initial shrinkage ratios of soft start and exponential curing were statistically lower than conventional curing (p < 0.05). From this study, the use of low initial light intensities may reduce the polymerization rate and, as a result, reduce the stress of polymerization shrinkage.

• Restorative Dentistry and Endodontics
• /
• v.40 no.4
• /
• pp.299-305
• /
• 2015

Objectives: The purpose of this study was to investigate the effectiveness of multiple decontamination procedures for salivary contamination after curing of a universal adhesive on dentin bond strength according to its etch modes. Materials and Methods: Forty-two extracted bovine incisors were trimmed by exposing the labial dentin surfaces and embedded in cylindrical molds. A universal adhesive (All-Bond Universal, Bisco) was used. The teeth were randomly divided into groups according to etch mode and decontamination procedure. The adhesive was applied according to the manufacturer's instructions for a given etch mode. With the exception of the control groups, the cured adhesive was contaminated with saliva for 20 sec. In the self-etch group, the teeth were divided into three groups: control, decontamination with rinsing and drying, and decontamination with rinsing, drying, and adhesive. In the etch-and-rinse group, the teeth were divided into four groups: control, decontamination with rinsing and drying, decontamination with rinsing, drying, and adhesive, and decontamination with rinsing, drying, re-etching, and reapplication of adhesive. A composite resin (Filtek Z350XT, 3M ESPE) was used for filling and was cured on the treated surfaces. Shear bond strength was measured, and failure modes were evaluated. The data were subjected to one-way analysis of variation and Tukey's HSD test. Results: The etch-and-rinse subgroup that was decontaminated by rinse, drying, re-etching, and reapplication of adhesive showed a significantly higher bond strength. Conclusions: When salivary contamination occurs after curing of the universal adhesive, additional etching improves the bond strength to dentin.