• 한국재료학회지
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• 제15권1호
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• pp.6-13
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• 2005

Copper based leadframe sheets were immersed in two kinds of hot alkaline solutions to form brown-oxide or blackoxide layer on the surface. The oxide-coated leadframe sheets were molded with epoxy molding compound (EMC). After post mold curing, the oxide-coated EMC-leadframe joints were machined to form sandwiched double-cantilever beam (SDCB) specimens. The SDCB specimens were used to measure the fracture toughness of the EMC/leadframe interfaces under quasi-Mode I loading conditions. After fracture toughness testing, the fracture surface were analyzed by various equipment to investigate failure path. An adhesion model was suggested to explain the failure path formation. The adhesion model is based on the strengthening mechanism of fiber-reinforced composite. The present paper deals with the introduction of the adhesion model. The explanation of the failure path with the proposed adhesion model was introduced in the companion paper.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2002년도 춘계학술발표대회 논문집
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• pp.109-113
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• 2002

Interfacial and electrical properties for the carbon fiber reinforced epoxy-amine terminated (AT) PEI composites were performed using microdroplet test and electrical resistance measurements. As AT PEI content increased, the fracture toughness of epoxy-AT PEI matrix increased, and IFSS was improved due to the improved toughness and energy absorption mechanisms of AT PEI. The microdroplet in the carbon fiber/neat epoxy composite showed brittle microfailure mode. At 15 wt% AT PEI content, ductile microfailure mode appeared because of improved fracture toughness. After curing, the changes of electrical resistance (ΔR) with increasing AT PEI content increased gradually because of thermal shrinkage. The matrix fracture toughness was correlated to IFSS, TEC and electrical resistance. In cyclic strain test, the maximum stress and their slope of the neat epoxy case were higher than those of 15 wt% AT PEI. The results obtained from electrical resistance measurements under curing process and reversible stress and strain were consistent well with matrix toughness properties.

• Composites Research
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• 제17권6호
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• pp.14-21
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• 2004

본 연구에서는 몇 가지 접합 방법에 따라 일방향 복합재료 단일 겹치기 접합 조인트의 파손 과정, 모드 및 강도를 실험적으로 평가하였다 접합 방법으로는 접착제 없는 동시성형, 접착제를 사용한 동시성형 및 이차 접합의 세 가지를 고려하였다 또한 이차 접합 조인트에서 몇 가지 파라미터의 영향도 살펴보았다. 접착제 없는 동시성형 시편은 가장 우수한 조인트 강도를 나타내었다. 이차접합 조인트에서는 접착제 층의 점진적인 파손이 발생하였다. 접착제의 재료 및 접합 강도가 상대적으로 강한 필름 접착제의 동시성형 조인트는 갑작스런 층간분리 파손이 발생하였으며 이차 접합 조인트보다 더 낮은 파손 강도를 나타내었다. 이차 집합 조인트에서 층간분리 파손이 발생하지 않은 것은 접착제 층에서의 균열 진전 및 점진적 파손이 층간분리 파손을 방지한 것으로 보인다. 따라서 복합재료 접합 조인트의 파손 강도는 접착제의 재료 강도 또는 접착 성능과 항상 비례하지 않으며 이것은 복합재료가 층간 분리 파손에 약하기 때문이다.

• Composites Research
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• 제16권2호
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• pp.62-67
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• 2003

Microdroplet 시험법과 전기저항 측정을 이용하여 탄소섬유강화 epoxy-AT-PEI 복합재료의 손상 감지능 및 계면물성평가에 대한 연구를 수행하였다. AT-PEI 함량이 증가함에 따라 기지재료의 파괴인성은 증가하였으며, 이로 인한 에너지흡수 메커니즘에 의해서 계면전단강도 역시 증가하였다. Microdroulet 시험에서 순수 에폭시는 취성파괴 현상을 그리고 15 phr AT-PEI의 경우에는 파괴인성의 증가로 인해 연성 파단 현상을 관찰할 수 있었다. 경화 후에 열 수축에 의한 전기저항 변화는 AT-PEI 함량 증가에 따라 증가하였으며. 가변하중 하에서 순수 에폭시에 함침된 탄소섬유의 같은 응력까지의 도달시간과 기울기는 15 phr AT-PEI의 경우보다 더 빠르고 높았다. 경화과정과 가역적인 하중 하에서의 전기저항 측정으로부터 얻은 결과는 기지재료의 파괴인성과 잘 일치하였다.

• 한국광학회지
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• 제6권4호
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• pp.310-316
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• 1995

유한영역에서의 조화함수전개법으로 인접한 두 도파로 코어 중심간의 거리 및 도파로 변수에 따른 결합길이를 계산하여 $1.3/1.55\mum$ WDM coupler을 설계하였다. 저압화학기상증착법에 의해 PSG 도파박막을 제작하고 laser lithography와 $CF_4/O_2$ RIE 공정 등을 이용하여 WDM coupler를 제작하였다. 또한 광섬유를 지지 및 고정하기 위하여 Si 기판 위에 V-groove를 만들었으며 제작된 WDM coupler와 V-groove로 지지된 광섬유를 UV curing epoxy를 사용하여 접속하였다. 제작된 WDM coupler의 $1.3.\mum$, $1.55\mum$에서의 분지별 도파모드를 관측하고 분할비를 측정한 결과 최대 분할비는 각각 9dB, 12dB였다.

• 대한소아치과학회지
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• 제24권1호
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• pp.139-147
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• 1997

Argon laser used in this case report, is special in having two wavelength of 488, 514nm blue-green visible light spectrum. Blue light is used for composite resin polymerization and caries detection. Green light is used for soft tissue surgery and coagulation. Maximum absorption of this laser light occurs in red pigmentation such as hemoglobin. The argon laser may be well-suited for selective destruction of blood clots and hemangioma with minimal damage to adjacent tissues. Argon laser light penetrates tissue to the 1 mm depth, so its thermal intensity is lower than $CO_2$ laser light. Also, due to its short wavelength it can be focused in a small spot and even single gene can be excised by this laser and microscopy. After applicating argon laser to 4 patient for surgical procedure and to 1 patient for curing the composite resin, following results were obtained. 1. Improved visibility were gained due to hemostasis and no specific technique were needed according to easy recontouring of the tissue. 2. Ability to use by contact mode, tactile sense was superior but tissue dragability and accumulation of tissue on the tip needed sweeping motion. 3. Additive local anesthetic procedure was needed. 4. No suture and less curing time reduced chair time, this made argon laser available in pediatric dentistry.

• 한국도로학회논문집
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• 제19권1호
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• pp.11-19
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• 2017

PURPOSES : The purpose of this study is to verify the property of self-healing, and to propose an appropriate duration for wet curing of bridge deck concrete overlays. METHODS : In this study, reinforced bars were inserted into concrete molds in order to prevent brittle fracture and induced cracks in the concrete resulting from indirect tension mode. The induced time of concrete cracking was 3 to 7 days, following which the concrete specimens were cured in water. The resulting concrete crack width was measured using image analysis equipment. Additionally, the self-healing tests were performed using the following three mixtures: OPC, SFC, and LMC. RESULTS : Concrete mixtures with crack widths of $150{\mu}m$ or lower were completely healed by Day 28. Hydrates of crack fills were found to be the calcium carbonate. CONCLUSIONS : The cement-based mixtures exhibit properties of self-healing. Considering these properties, it is necessary to increase the curing duration of concrete overlays for bridge decks.

• E2M - 전기 전자와 첨단 소재
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• 제7권1호
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• pp.32-41
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• 1994

In this study, the TSC spectroscopy has been applied to investigate the influence of structural change due to a process of curing reaction on the electrical properties of epoxy composites cured with acid-anhydride. Five TSC peaks appeared in -160-250[.deg.C]: in the low temperature region below glass transition temperature(T$\_$g/), three relaxation mode peaks due to action of side chains, substitution group or terminal groups have been observed, a peak associated with T$\_$g/, appeared in 110[.deg. C] and p peak due to ionic space charges located in 150[.deg.C]. Each peak was separated into elementary peaks by the partial polarization procedure, and the distribution of activation energy and relaxation time were analized to clearify the origin of each peak. Also, overaboundantly added hardener separated a .betha. peak near 10[.deg. C] into two peaks of .betha.$\_$1/(10.deg. C) and .betha.$\_$2/(20.deg. C) according to increasement of forming field, and the separated hardener was oxidated thermally with increasing surrounding temperatures. The expansion of the free volume need in molecular motion and the reduction of the structural packing density through thermal oxidation process increased TSC between .alpha. peak and .betha. peak and decreased T$\_$g/.

• Computers and Concrete
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• 제19권4호
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• pp.429-434
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• 2017

Failure of basic structures material is usually accompanied by expansion of interior cracks due to stress concentration at the cracks tip. This phenomenon shows the importance of examination of the failure behavior of concrete structures. To this end, 4 types of mortar samples with different amounts of nano-silica (0%, 0.5%, 1%, and 1.5%) were made to prepare twelve $50{\times}50{\times}50mm$ cubic samples. The goal of this study was to describe the failure and micro-crack growth behavior of the cement mortars in presence of nano-silica particles and control mortars during different curing days. Failure of mortar samples under compressive strength were sensed with acoustic emission technique (AET) at different curing days. It was concluded that the addition of nano-silica particles could modify failure and micro-crack growth behavior of mortar samples. Also, monitoring of acoustic emission parameters exposed differences in failure behavior due to the addition of the nanoparticles. Mortar samples of nano-silica particles revealed stronger shear mode characteristics than those without nanoparticles, which revealed high acoustic activity due to heterogeneous matrix. It is worth mentioning that the highest compressive strength for 3 and 7 test ages obtained from samples with the addition of 1.5% nano-silica particles. On the other hand maximum compressive strength of 28 curing days obtained from samples with 1% combination of nano-silica particles.

• 한국구조물진단유지관리공학회 논문집
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• 제19권3호
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• pp.149-160
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• 2015

이 연구에서는 초고성능 콘크리트 (UHPC)와 보통 콘크리트 (NSC)간 계면부착강도에 관한 연구를 수행하였다. UHPC를 보수 보강재로 활용하기 위한 기존의 부착강도에 관한 연구와 달리, UHPC를 프리캐스트 합성부재로 활용하기 위한 연구에 초점을 맞추었으며, 여기에 영향을 미칠 수 있는 다양한 요인에 대하여 검토하였다. 기존 연구들을 분석한 결과, UHPC-NSC 계면 부착강도에 영향을 미칠 수 있는 요인으로는 계면의 형상, 합성 전 UHPC의 경화 진행상태, 합성 전 UHPC의 수분 흡수상태, 그리고 합성 후 양생장소와 같이 크게 4가지로 구분되었다. 계면의 형상을 변수로 한 실험에서는 형상에 따라 각기 다른 파괴모드가 나타났으며, 기존 연구에서 확인되지 않았던 거칠게 처리한 UHPC 계면 일부가 파괴되는 새로운 파괴모드가 발견되었다. 합성 전 UHPC의 경화진행 상태가 부착강도에 영향을 미치는 것으로 나타났으며, 이러한 영향은 부착 파괴모드에 따라 다르게 나타났다. 또한, 합성 전 UHPC의 수분상태가 부착강도에 영향을 주었으며, UHPC의 양생방법에 따라 서로 상반되는 결과를 보였다. 마지막으로, 합성한 시편의 양생조건 역시 계면 부착강도에 영향을 미친다는 것을 확인하였다.