• Title/Summary/Keyword: Curing Method

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A STUDY OF THE BOND STRENGTHS OF COMPOSITE RESIN TO DENTIN SURFACES PREPARED WITH MICROABRASIVE (Microabrasive로 처리한 상아질표면에 대한 복합레진의 결합강도에 관한 연구)

  • Choi, Kyoung-Kyu;Min, Byung-Soon
    • Restorative Dentistry and Endodontics
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    • v.22 no.1
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    • pp.61-75
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    • 1997
  • The bond strengths of composite resin to tooth dentin vary with the methods of cavity preparation and surface treatment. Recent developments in techniques of dentinal surface treatment have renewed interest in microabrasive as a means of tooth preparation, The purpose of this study was to determine the effects of a new method of cavity preparation on the bond of composite resin to dentin. Freshly extracted 144 healthy human third molars were used in this study. The dentin surfaces prepared with #600 SiC abrasive paper were divided into control and air abrasion groups according to the method of dentin surface preparation using different combinations of delivery pressure, time, and acid etching. The shear bond strengths were measured after the composite resin (Clearfil Photo Bright) was bonded to prepared dentin surfaces by light-curing using a dentin bonding system (All-bond 2), In addition, the average surface roughness was measured to investigate the effect of differently prepared dentin surfaces on the shear bond strengths. The surface changes of prepared dentin and the debonded dentin surfaces were observed with SEM (S-2300, Hitachi Co., Japan). The following results from this-study were obtained ; 1. There was no significant difference of shear bond strengths according to the changes of delivery pressure and time. 2. The shear bond strengths were lower than the control in the air abraded-only groups, but those of the additional acid-etched groups were higher than the control. 3. The shear bond strengths to all air-abraded surfaces were increased by acid etching. 4. The correlation between shear bond strengths and surface roughness was not certain, although the mean surface roughness of all air-abraded surfaces has increased evidently while it has slightly decreased for additional acid etching. 5. On SEM examination, the dentinal tubules were almost occluded in the air abraded-only groups, but those were opened in the additional acid-etched groups. 6. The debonded surfaces were showed adhesive failure mode in the air abraded- only groups, while those were showed mainly the mixed and cohesive failure mode in the additional acid-etched groups. These results suggest that the layer produced during cavity preparation or surface treatment with air abrasion must be removed for maximum bond strength of composite resin to dentin.

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Behavior Characteristics of Cement Bentonite Impervious Walls Related to Mixing Methods and Curing Time (강화벤토나이트 차수벽체의 배합방법 및 양생일에 따른 거동 특성)

  • Hwang, Jungsoon;Kim, Seungwook;Jung, Jungi;Lee, Seungjoo;Oh, Byeungsam;Baek, Seungcheol
    • Journal of the Korean GEO-environmental Society
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    • v.17 no.12
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    • pp.45-54
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    • 2016
  • In this study, the construction method of new underground continuos impervious wall that the bentonite slurry keeps the stability of excavated trench and the mixture of cement and bentonite plays a role as a constituent of impervious wall in the trench. The merit of homogeneity of the method so called as a cement-bentonite slurry wall enables to accurately make an estimation of hydraulic conductivity of the walls compared with that by other general grouting methods and to verify their waterproof efficiency without difficulty at the design stage. The use of cement-bentonite slurry walls for the containment of groundwater flow has also proven a cost-effective impervious wall technology by employing the simple combination of construction equipments and easy and fast construction procedures. The engineering characteristics of cement-bentonite impervious wall obtained by carrying out the laboratory experiments under various conditions. This study reveals the effect of variation of constituent materials and their mixing methods (Water-Cement-Bentonite) on the engineering characteristics of a composition. Also, this study makes some recommendations on the optimum mixing ratio and mixing sequence for the best quality at the site. That is the most important factors to estimate the construction cost and design of the technique. The comparison is lastly made to evaluate the effect of ordinary Portland and blast furnace slag cement as a bonding material on the behavior of impervious walls.

Effects of Cryptotympana pustulata on the expression of cytokine genes in human monocytes of THP-1 (선퇴가 인간의 THP-1 단핵구에서 사이토카인 유전자 발현에 미치는 영향)

  • An, Jong-Hyun;Kim, Kyung-Jun
    • The Journal of Korean Medicine Ophthalmology and Otolaryngology and Dermatology
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    • v.23 no.1
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    • pp.94-110
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    • 2010
  • Objective : This study was performed to evaluate the effect of immune reaction inductive substances such as phorbol-myristate-acetate(PMA), lipopolysaccharide(LPS), dermato-phagoides pteronyssus crude extract(DPE), dinitrochloro-benzene(DNCB) and Cryptotympana pustulata(CP), the Cryptotympana pustulata extracting substance at simultaneously on the translocation of nuclear factor-kappa B(NF-${\kappa}B$) towards to the nucleus and the mRNA expression patterns of various cytokine genes in Human acute monocytic leukemia cell line(THP-1 cells), monocytes of human. Experiment : To analyze cytokine genes expression patterns, the RT-PCR method was used, measuring tumor necrosis factor(TNF)-$\alpha$ that had been secreted during cell culture in the ELISA method. The morphological change in the cell observed during THP-1 cell culture was observed using a scanning electron microscope (SEM) and the quantitative distribution in the cell NF-${\kappa}B$ was analyzed through immunocytochemistry and a confocal microscopy. Result : CP showed different influences onto the mRNA expression patterns of cytokine genes with PMA, LPS. DPE and DNCB according to the types of immune inductive substances in the THP-1 cells. The expressions of inter-leukin(IL)-10, interferon(INF)-$\gamma$, TNF-$\alpha$ and monocyte chemoattractantant protein(MCP)-1 induced by PMA were suppressed by CP while the expression of transforming growth factor(TGF)-$\beta$ was promoted. Regarding the secretion pattern of TNF-$\alpha$ according to PMA processing, its secretion amount was increased by CP concurrent processing, in case of processing CP onto PMA and LPS, We discovered that the secretion amount of TNF-$\alpha$ was increased. Upon processing PMA and LPS on the THP-1 cell strain at the same time or either additionally processing CP thereon, the movement increase towards the nucleus from the NF-${\kappa}B$ cell cytoplasm, a transcription factor was able to be observed. Conclusion : In this study, Cryptotympana pustulata extracting substance was confirmed that it had an influence on expression patterns of cytokine genes according to the actions of a variety kinds of immune reaction inductive substances processed on the monocyte THP-1 cell of humans. Therefore, additional studies as for the immune adjusting function of Cryptotympana pustulata are considered to be able to offer important materials for curing immune abnormal diseases such as atopy dermatitis afterward.

Preparation and Application of Rehmannia Glutinosa Extract Incorporated Functional Chitosan Based Biomaterials (지황 추출물 첨가 chitosan 기반 기능성 바이오 소재 제조 및 응용)

  • Lee, Si-Yeon;Kim, Kyeong-Jung;Kim, Youn-Sop;Yoon, Soon-Do
    • Applied Chemistry for Engineering
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    • v.33 no.2
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    • pp.195-201
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    • 2022
  • The main objective of this work is to prepare Rehmannia glutinosa extract (RE) incorporated functional chitosan (CH) based biomaterials and evaluate their physical properties, RE release properties, inhibitory effect of melanogenesis, and antioxidant and elastase inhibitory activities. RE incorporated CH based biomaterials were synthesized by a casting method and UV curing process. The surface and cross sections of prepared biomaterials were characterized by a field emission scanning electron microscope (FE-SEM). The physical properties such as tensile strength and elongation at break were also investigated. To apply the transdermal drug delivery system, RE release properties were examined with pH 4.5, 5.5, and 6.5 buffer solutions and artificial skin test at 36.5 ℃. Results indicated that RE release of RE incorporated biomaterials with/without the addition of plasticizers [glycerol (GL) and citric acid (CA)] at pH 6.5 was about 1.10 times higher than that of at pH 4.5. In addition, results of the artificial skin test verified that RE was released constantly for 6 h. To verify the applicability of the prepared biomaterials, tyrosinase, 2,2-diphenyl-1-picrylhydrazyl (DPPH), and elastase assays were investigated. Results indicated that RE incorporated biomaterials added CA exhibited tyrosinase activation, DPPH radical scavenging activity rate, and elastase activation of 45.12, 89.40, and 59.94%, respectively.

Evaluation of Chloride Extraction under Electrochemical Chloride Extraction (전기화학적 염화물 추출법에 따른 염소이온 제거 성능 평가)

  • Jiseok, Kim;Ki-Yong, Ann
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.10 no.4
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    • pp.553-557
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    • 2022
  • The present study evaluate the chloride extracion under electrochemical chloride extraction method. Chloride was penetrated into the concrete from external reservoir using a 4M NaCl solution, and an electrochemical chloride extraction method was applied after the curing period of 1 year. The current density was constantly kept 1000 mA/m2 for coulostatic application with the variation in potential difference. The duration of the ECE treatment was 2, 4, 8 weeks, respectively. The residual chloride concentration at all depths decreased, and the chloride concentration decreased as the application period increased. After the application period of 8 weeks, 62.9 to 77.6 % of chloride extracted in the total chloride profile, and 77.7 to 99.5 % of chloride extracted in the free chloride profile. In particular, the concentration of free chloride at a depth of 7 mm or more from the concrete surface was 0.01 % or less by cement. In addition, it was confirmed that the bound chloride could be extracted by the electrochemical chloride extraction.

3D printed surveyed restoration and metal framework in removable dentures: A case report (3D 프린팅 된 서베이드 금관과 금속 프레임워크를 이용한 양악 가철성 의치 수복 증례)

  • Song Yi Park;Sang-Won Park;Chan Park;Woohyung Jang;Kwi-Dug Yun
    • The Journal of Korean Academy of Prosthodontics
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    • v.61 no.2
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    • pp.153-159
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    • 2023
  • Computer-aided design-computer-aided manufacturing technology has been widely used in the manufacture of fixed prostheses including implants, but in the case of removable dentures, the analog method is still being used due to the errors such as a lack of fusion and over-fusion in selective laser meting process. With the recent development of CAD software, virtual surveying and framework design are made possible, and the designed file can be manufactured by milling or 3D printing. It replace the analog method of waxing and denture curing process and also can reduce the production time and cost. Therefore, this case is reported because good clinical results were obtained by digitally surveying on CAD software to produce a surveyed metal restoration and framework on maxillary and mandibular removable dentures.

Determination of Solidified Material's Optimum Mixing Ratio for Reservoir Embankment Reinforcement (저수지 제체 보강을 위한 고화재 최적 배합비 결정)

  • Jaegeun Woo;Jungsoon Hwang;Seungwook Kim;Seungcheol Baek
    • Journal of the Korean GEO-environmental Society
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    • v.25 no.6
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    • pp.5-12
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    • 2024
  • Currently, a grouting method that minimizes damage to the reservoir embankment by injecting solidification agent at low pressure is commonly used to ensure waterproofing and safety of the embankment, but the use of solidification agents can cause issues, such as a decrease in durability and a lack of clear method for determining the mixing ratio. In this study, when the base ground and solidification agent were stirred and mixed at various weight mixing ratios, the permeability coefficient and strength of the mixture were confirmed through laboratory tests, and the optimal mixing ratio was suggested through analysis of the test results. The specimen for the laboratory test was produced considering the mixing ratio of the solidification agent. The specimen for the permeability coefficient test was tested by producing one each of cohesionless and cohesive soil for a mixing amount of 1.5 kN/m3 of solidification agent, and the permeability test results confirmed that the water barrier performance was secured below the permeability coefficient value required by various design criteria. A total of 24 specimens for the strength test were produced, 3 for each of 5 mixing amounts for cohesive soil and 3 mixing amounts for cohesionless soil. The strength test results showed that the uniaxial compressive strength tends to increase linearly with increasing curing time for both cohesionless soil and cohesive soil when the mixing amount is less than 2.0 kN/m3. Therefore, the optimal mixing ratio applied to the site is determined to be mixing amount of 1.5 kN/m3 and 2.0 kN/m3. Finally, numerical analysis reflecting test results was conducted on design case for improvement projects for aging reservoirs embankment to verify the water barrier performance and safety improvement effects.

Synthesis of Silica Coated Silicon Substrate by Recycling Silicon Sludge Generated in Semiconductor Packaging Process and Their Application to Epoxy Molding Compound (반도체 패키징 공정에서 발생하는 실리콘 슬러지의 재활용을 통한 Si@SiO2 제조 및 에폭시 몰딩 컴파운드로의 응용)

  • Yeon-Ryong Chu;Dahee Kang;Ha-Yeong Kim;Jisu Lim;Gyu-Sik Park;Suk Jekal;Chang-Min Yoon
    • Journal of the Korea Organic Resources Recycling Association
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    • v.32 no.3
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    • pp.57-66
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    • 2024
  • In this study, silicon sludge from a semiconductor packaging process is recycled to fabricate silica coated silicon-sludge and applied as a filler for an epoxy molding compound(EMC). Silicon-sludge powder(S-sludge) is treated with acid to remove metallic impurities and then coated using the sol-gel method to synthesize silica coated silicon-sludge powder(SS-sludge). The as-synthesized SS-sludge is subsequently mixed with epoxy resin, a curing agent, and carbon black to create an EMC(SS-sludge EMC). The heat dissipation properties of the EMC were examined using an IR camera. IR camera analysis confirmed that the SS-sludge EMC exhibited the highest surface temperature of 58.5℃ compared to SiO2-based EMC. This enhancement in heat dissipation using SS-sludge EMC is attributed to the excellent thermal conductivity(150W/mK) of the silicon substrate and the presence of the silica layer on the SS-sludge surface which effectively enhances the thermal property of the EMC. Therefore, this study successfully demonstrates the recycling of silicon sludge from a semiconductor packaging process by synthesizing silica coated silicon-sludge and suggests a novel application of this material in semiconductor packaging.

Evaluation of Usefulness on In-vivo Diode Dosimetry for Measuring the Tumor Dose of Oral Cancer Patient (구강암 환자의 종양 선량 측정을 위한 In-vivo Diode Dosimetry의 유용성 평가)

  • Na Kyung-Su;Lee Je-Hee;Park Heung-Deuk
    • The Journal of Korean Society for Radiation Therapy
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    • v.17 no.2
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    • pp.133-140
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    • 2005
  • Purpose : This test is designed to identify the validity of treatment plan by implementing real-time dosimetry by means of dose that is absorbed into PTV and OAR when preparing doses of 3D and POP plans. Materials and Methods : In treatment. error can be calculated be comparing Exp. Dose with the actual dose, which has been converted from 'the reading value obtained by placing diode detector on the area to be measured'. Same test can be repeated using Alderson-Rando phantom. Results : Errors were found: A patient(POP plan): 197.6/199=-1.2%, B patient(3D-plan): 199.9/198.7=+0.6%, C patient: 196/200=-1.5%. In addition, considering the resulted value of measuring OAR besides target-dose for C patient showed 96/200, representing does of 47%, the purpose of protection was judged to be duly accomplished. Also it was acknowledged the resulted value of -3.7% met the targeted dose within the range of ${\pm}5%$. Conclusion : Aimed for identifying the usefulness of pre-treatment dose measurement using diode detector, this test was useful to evaluate the validity of curing because it resulted in the identification of category to be protected as well as t dose. Moreover, it is thought to have great advantage in ascertaining the dose of target, dose of which is not calculated yet. Similar to L-gram before treatment, this test is thought to be very effective so that it can bring great advantages in the aspects such as validity of curing method and post-treatment plan as well.

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A Study on Improving the Performance of Shale for Application of Aggregate for Concrete (콘크리트용 골재활용을 위한 셰일 골재의 성능개선에 관한 연구)

  • Lee, Seung-Han;Jung, Yong-Wook;Jang, Seok-Soo;Yeo, In-Dong;Choi, Jong-Oh
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.14 no.11
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    • pp.5915-5922
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    • 2013
  • In this study, with the aim of improving the performance of shale to allow for its use as coarse aggregate for concrete, we coated shale aggregates with water repellents and polymers and evaluated their physical properties such as density, water absorption rate, wear rate, and stability depending on the coating method. In addition, the effects of the performance improvement were evaluated by assessing the properties of fresh concrete produced by varying the shale substitution ratio, as well as the compressive strength, flexural strength, and freeze-thaw resistance according to curing ages. The test results revealed that the absolute dry densities of all coated aggregates satisfied the standard density for coarse aggregates for concrete(>$2.50g/cm^3$),and the absorption rate of the shale aggregate coated with water repellent decreased by about 50% compared with that of uncoated shale. The wear rate of the polymer-coated shale decreased by up to 13.0% compared with that of uncoated shale. All coated aggregates satisfied the stability standard for coarse aggregates for concrete(${\leq}12$). The water repellent-induced performance improvement decreased the shale aggregates' slump by about 20~30mm compared with that of the uncoated shale aggregates, and the air content of the repellent-coated shale aggregate increased by up to 0.9% compared with that of the uncoated shale aggregate. The compressive strength of the polymer-coated shale aggregates at a curing age of 28 days was RS(F) 95.7% and BS(F) 90.0%, and the flexural strength was RS(F) 98.0 % and BS(F) 92.0% of the corresponding values of concretes produced using plain aggregates. Furthermore, the concrete using polymer-coated shale aggregates showed a dynamic modulus of elasticity of RS(F) 91% and BS(F) 88% after 300 freeze-thaw cycles, thus demonstrating improved freeze-thaw durability.