• Title/Summary/Keyword: Cryogenic Detector

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Development of an Analytical Approach to Measure Volatile Sulfur Compounds Using a Non-Cryogenic Preconcentration Method (비냉각형 선농축 방식에 의한 대기 중 휘발성 황화합물의 분석방법 개발)

  • 김기현;이강웅
    • Journal of Korean Society for Atmospheric Environment
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    • v.13 no.5
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    • pp.355-360
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    • 1997
  • The atmospheric concentration of dimethylsulfide (DMS), known as the predominant volatile organic. sulfur compound, is determined at subnanogram level by a combined application of non-cryogenic preconcentration method and gas chromatography with flame photometric detection (GC/FPD). The volatile DMS in air is preconcentrated using a trapping tube containing adsorbent like Molecular Sieve 5A (or gold-coated sands). The tube is then connected to the GC/FPD system via a six-way rotary valve, thermally desorbed at 40$0^{\circ}C$, separated on OV101 column, and detected by a flame photometric detector. The DMS peak elutes at about 2.5 mins and is integrated electronically. The analytical precision, if expressed in terms of relative standard error, is around 5%. The detection limit of our GC/FPD system is ca 1 ng of DMS. Details of our analytical system are presented.

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Optimization and Performance Evaluation for the Science Detector Systems of IGRINS

  • Jeong, Ueejeong;Chun, Moo-Young;Oh, Jae-Sok;Park, Chan;Yu, Young Sam;Oh, Heeyoung;Yuk, In-Soo;Kim, Kang-Min;Ko, Kyeong Yeon;Pavel, Michael;Jaffe, Daniel T.
    • The Bulletin of The Korean Astronomical Society
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    • v.39 no.2
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    • pp.91.1-91.1
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    • 2014
  • IGRINS (the Immersion GRating INfrared Spectrometer) is a high resolution wide-band infrared spectrograph developed by the Korea Astronomy and Space Science Institute (KASI) and the University of Texas at Austin (UT). This spectrograph has H-band and K-band science cameras, both of which use Teledyne's $2.5{\mu}m$ cutoff $2k{\times}2k$ HgCdTe HAWAII-2RG CMOS science grade detectors. Teledyne's cryogenic SIDECAR ASIC boards and JADE2 USB interface cards were installed to control these detectors. We performed lab experiments and test observations to optimize and evaluate the detector systems of science cameras. In this presentation, we describe a process to optimize bias voltages and way to reduce pattern noise with reference pixel subtraction schemes. We also present measurements of the following properties under optimized settings of bias voltages at cryogenic temperature (70K): read noise, Fowler noise, dark current, and reference-level stability, full well depth, linearity and conversion gain.

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High Energy Resolution Alpha Spectrometer Using a Cryogenic Detector (저온검출기를 이용한 에너지 고 분해능 알파분광 구현)

  • Kim, M.S.;Lee, S.H.;Yoon, W.S.;Jang, Y.S.;Lee, S.J.;Kim, Y.H.;Lee, M.K.
    • Journal of Radiation Protection and Research
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    • v.38 no.3
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    • pp.132-137
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    • 2013
  • Cryogenic particle detectors have recently been adopted in radiation detection and measurement because of their high energy resolution. Many of these detectors have demonstrated energy resolutions better than the theoretical limit of semiconductor detectors. We report the development of alpha spectrometer using a micro-fabricated magnetic calorimeter coupled to a large-area particle absorber. A piece of gold foil of $2{\times}2{\times}0.05mm^3$ was glued to the paramagnetic temperature sensor made of sputtered Au:Er film to serve as an absorber for incident alpha particles. We performed experiments with 241Am source at cryogen free adiabatic demagnetization refrigerator (CF-ADR). A high energy resolution of 6.8 keV in FWHM was obtained for 5.5 MeV alpha particles.

Operating Conditions Proposal of Bandgap Circuit at Cryogenic Temperature for Signal Processing of Infrared Detector and a Performance Analysis of a Manufactured Chip (적외선 탐색기 신호처리를 위한 극저온 밴드갭 회로 동작 조건 제안 및 제작된 칩의 성능 분석)

  • Kim Yon Kyu;Kang Sang-Gu;Lee Hee-Chul
    • Journal of the Institute of Electronics Engineers of Korea SD
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    • v.41 no.12
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    • pp.59-65
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    • 2004
  • A stable reference voltage generator is necessary to the infrared image signal readout circuit(ROIC) to improve noise characteristics of signal originated from infrared devices, that is, to gain good images. In this paper, bandgap circuit operating at cryogenic temperature of 77K for Infrared image ROIC(readout integrated circuit) was first made. It demonstrates practical use possibility through taking measurements and estimations. Bandgap circuit is a representative voltage reference circuit. Most of bandgap reference circuits which are presented so far operate at room temperature, and their characteristic are not suitable for infrared image ROIC operating at liquid nitrogen temperature, 77K. To design bandgap circuit operating at cryogenic temperature, suitable circuit is selected and the parameter characteristics of used devices as temperature change are seen by a theoretical study and fitted at liquid temperature with considering such characteristics. This circuit has been fabricated in the Hynix 0.6um standard CMOS process, and the output voltage measured shows that the stability is 1.042±0.0015V over the temperature range of 60K to 110K and is better than bandgap circuits operated at room temperature.

The Experimental Study of the Performance of the Rotary Stirling refrigerator (회전압축기형 스털링냉동기의 성능에 관한 실험적 연구)

  • Hong, Yong-Ju;Park, Seong-Je;Kim, Hyo-Bong;Kim, Yang-Hoon;Choi, Young-Don
    • Proceedings of the KSME Conference
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    • 2004.11a
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    • pp.1312-1316
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    • 2004
  • The Stirling refrigerators have been widely used for the cooling of the infrared detector and HTS to the cryogenic temperature. The Stirling refrigerator with the rotary compressor are applicable to the cooling device for the compact mobile thermal imaging system, because the refrigerators have the compact structure and light weight. The typical performance factors of the Stirling refrigerator are the cool-down time, cooling capacity at the desired temperature and the input power. And the above performance factors are depends on the thermal insulation characteristics of the Dewar. In this study, the steady thermal load of the Dewar and the performance of the Stirling refrigerator were measured. The results show the dependency of the input power and the charging pressure on the performance of the refrigerator.

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Vacuum and Radiation Insulation in the Cryogenic Engineering (진공 및 복사 단열에 의한 저온 유지 기술)

  • 박성제
    • Journal of the Korean Society for Precision Engineering
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    • v.19 no.11
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    • pp.9-17
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    • 2002
  • 최근에 초전도 산업과 저온 작동 정밀 센서 기술의 발전으로 극저온 냉동기 또는 극저온 한제에 의해 냉각된 저온 용기의 저온 유지 기술이 필요하게 되었다. 또한 의료용 MRI, 야간 투시경용 적외선 센서, 이동통신무선기지국용 초전도 필터 등과 같이 일반인들도 극저온을 이용하게 되어 보다 사용하기 쉽고 안정적인 저온용기가 요구되고 있다. 저온용기의 저온 유지 기술은 진공 및 복사 단열 기술 뿐만 아니라 극저온 발생기술과 진공 발생 기술이 같이 고려되어야 하는 복합기술로서 앞으로 전자, 정보 통신, 나노, 바이오 산업 등에도 널리 활용될 수 있는 기반 기술로 자리 매김 할 것으로 보여 관련 연구자들의 많은 노력과 관심이 요구된다.

A Study of Liquid Nitrogen Inert Gas System for LNGC Diesel Engine Crank Chamber (LNGC 디젤기관 크랭크 챔버용 액체질소 불활성가스 시스템에 관한 연구)

  • Choi, Bu-Hong;Kim, Hyun-Soo
    • Journal of the Korean Society of Marine Environment & Safety
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    • v.18 no.3
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    • pp.279-285
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    • 2012
  • It is necessary to install the inert gas system(IGS) for preventing fire and explosion in LNGC main diesel engine crankcase besides oil mist detector(OMD) unit with $CO_2$ gas injector. Therefore, to design the liquid nitrogen IGS, analytical work is conducted for predicting the heat input load of liquid nitrogen heater with two-phase stratified flow model. This paper also presents the effects of changes in pipe diameter, saturated pressure, and inclination angle by ship's movement on cryogenic two-phase stratified flows. It is found that the stratified model gives reasonable predictions, and the model is effective to predict the heat input load of liquid nitrogen IGS.

Development of the Near Infrared Camera System for Astronomical Application

  • Moon, Bong-Kon
    • The Bulletin of The Korean Astronomical Society
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    • v.35 no.1
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    • pp.39.2-39.2
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    • 2010
  • In this paper, I present the domestic development of near infrared camera systems for the ground telescope and the space satellite. These systems are the first infrared instruments made for astronomical observation in Korea. KASINICS (KASI Near Infrared Camera System) was developed to be installed on the 1.8m telescope of the Bohyunsan Optical Astronomy Observatory (BOAO) in Korea. KASINICS is equipped with a $512{\times}512$ InSb array enable L band observations as well as J, H, and Ks bands. The field-of-view of the array is $3.3'{\times}3.3'$ with a resolution of 0.39"/pixel. It employs an Offner relay optical system providing a cold stop to eliminate thermal background emission from the telescope structures. From the test observation, limiting magnitudes are J=17.6, H=17.5, Ks=16.1 and L(narrow)=10.0 mag at a signal-to-noise ratio of 10 in an integration time of 100 s. MIRIS (Multi-purpose InfraRed Imaging System) is the main payload of the STSAT-3 in Korea. MIRIS Space Observation Camera (SOC) covers the observation wavelength from $0.9{\mu}m$ to $2.0{\mu}m$ with a wide field of view $3.67^{\circ}{\times}3.67^{\circ}$. The PICNIC HgCdTe detector in a cold box is cooled down below 100K by a micro Stirling cooler of which cooling capacity is 220mW at 77K. MIRIS SOC adopts passive cooling technique to chill the telescope below 200K by pointing to the deep space (3K). The cooling mechanism employs a radiator, a Winston cone baffle, a thermal shield, MLI of 30 layers, and GFRP pipe support in the system. Opto-mechanical analysis was made in order to estimate and compensate possible stresses from the thermal contraction of mounting parts at cryogenic temperatures. Finite Element Analysis (FEA) of mechanical structure was also conducted to ensure safety and stability in launching environments and in orbit. MIRIS SOC will mainly perform the Galactic plane survey with narrow band filters (Pa $\alpha$ and Pa $\alpha$ continuum) and CIB (Cosmic Infrared Background) observation with wide band filters (I and H) driven by a cryogenic stepping motor.

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Opto - Mechanical Design of IGRINS Slit-viewing Camera Barrel

  • Oh, Hee-Young;Yuk, In-Soo;Park, Chan;Lee, Han-Shin;Lee, Sung-Ho;Chun, Moo-Young;Jaffe, Daniel T.
    • Bulletin of the Korean Space Science Society
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    • 2011.04a
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    • pp.31.2-31.2
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    • 2011
  • IGRINS (Immersion GRating INfrared Spectrometer) is a high resolution wide-band infrared spectrograph developed by Korea Astronomy and Space Science Institute (KASI) and the University of Texas at Austin (UT). The slit-viewing camera is one of four re-imaging optics in IGRINS including the input relay optics and the H- and K- band spectrograph cameras. Consisting of five lenses and one Ks-band filter, the slit viewing camera relays the infrared image of $2'{\times}2'$ field around the slit to the detector focal plane. Since IGRINS is a cryogenic instrument, the lens barrel is designed to be optimized at the operating temperature of 130 K. The barrel design also aims to achieve easy alignment and assembly. We use radial springs and axial springs to support lenses and lens spacers against the gravity and thermal contraction. Total weight of the lens barrel is estimated to be 1.2 kg. Results from structural analysis are presented.

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Development of primary reference gas mixtures of 18 volatile organic compounds in hazardous air pollutants (5 nmol/mol level) and their analytical methods

  • Kang, Ji Hwan;Kim, Yong Doo;Lee, Jinhong;Lee, Sangil
    • Analytical Science and Technology
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    • v.34 no.5
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    • pp.202-211
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    • 2021
  • Volatile organic compounds (VOCs) in hazardous air pollutants (HAPs) have been regulated by the Air Pollution Control Act (1978) and their atmospheric concentrations have been monitored in 39 monitor sites in Korea. However, measurement standards of volatile organic compounds (VOCs) in HAPs at ambient levels have not been established in Korea. Primary reference gas mixtures (measurement standards) at ambient levels are required for accurately monitoring atmospheric VOCs in HAPs and managing their emissions. In this study, primary reference gas mixtures (PRMs) at 5 nmol/mol were developed in order to establish primary national standards of VOCs in HAPs at ambient levels. Primary reference gas mixtures (PRMs) were prepared in pressurized aluminum cylinders with special internal surface treatment using gravimetric method. Analytical methods using gas chromatography-flame ionization detector (GC-FID) coupled with a cryogenic preconcentrator were also developed to verify the consistency of gravimetrically prepared HAP VOCs PRMs. Three different columns installed in the GC-FID were evaluated and compared for the retention times and separation of eighteen target components in a chromatogram. Results show that the HAP VOCs PRMs at 5 nmol/mol were consistent within a relative expanded uncertainty (k=2) of less than 3 % except acrylonitrile (less than 6 %) and the 18 VOCs were stable for 1 year within their associated uncertainties.