• 제목/요약/키워드: Crucible

검색결과 317건 처리시간 0.024초

Floating Zone법에 의한 LiF 단결정 성장 (Growth of LiF Single Crystal by Floating Zone Method)

  • 오원석;신건철
    • 한국세라믹학회지
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    • 제27권5호
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    • pp.631-637
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    • 1990
  • Lithium fluolide single crystals were grown by a floating zone method, with infrared radiation convergence type heater, which is free of contamination from the crucible wall. The crystals grown by this apparatus are 5cm in length and 5-6mm in diameter. The grown cryatal was examined by an optical microscope, XRD, Laue camera, Vickers hardness tester, and FTIR.

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8인치 실리콘성장을 위한 커스프 MCZ계에서 축방향 산소분포에 대한 연구 (A numerical study on the optimum operation condition for axial oxygen concentration in 8 inch silicon growth by cusp MCZ)

  • 이승철;윤종규
    • 한국결정성장학회지
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    • 제7권3호
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    • pp.406-417
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    • 1997
  • 초크랄스키법들 의한 8인치 실리콘 단결정 성장계에 대칭과 비대칭 커스프 자장을 인가하여 결정을 성장시켰을 때 축방향으로 일정한 산소농도분포를 가질 수 있는 적절한 인가 자장의 크기와 비대칭도에 대한 수치해석적 연구를 수행하였다. 결정이 성장할 때 커스프 자장의 형태가 유지되는 방법으로 도가니의 위치를 변화시키는 방법과 인가코일의 위치를 변화시키는 방법을 비교하였다. 대칭 커스프 자장이 인가된 경우, 축방향으로 일정한 산소농도를 얻을 수 있는 자장의 강도변화는 결정이 성장함에 따라 아래로 볼록한 형태를 띠었다. 축밟향으로 일정한 산소농도분포를 갖기 위해 도가니의 위치를 변화시키는 방법과 코일의 위치를 변화시키는 방법을 비교한 결과 비슷한 산소농도의 표준편차값을 가짐을 알 수 있었다. 비대칭 자장이 인가된 경우, 축방향으로 일정한 산소농도 분포를 얻기 위해서는 비대칭도는 결정이 성장함에 따라 점차 증가하는 양상을 보였다.

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Theory and technology of growing striation-free crystals

  • Scheel, Hans J.
    • 한국결정성장학회지
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    • 제14권4호
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    • pp.174-186
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    • 2004
  • Striations are growth-induced inhomogeneities which hamper the applications of solid-solution crystals and of doped crystals in numerous technologies. Thus the optimized performance of solid solutions often can not be exploited. The inhomogeneity problem can be solved in specific cases by achieving a distribution coefficient one in growth from melts and from solutions. Macrostep-induced striations can be suppressed by controlling the growth mode, by achieving growth on facets thereby preventing step bunching. Thermal striations are commonly assumed to be caused by convective instabilities so that reduced convection by microgravity or by damping magnetic fields was and is widely attempted to reduce such inhomogeneities. Here it will be shown that temperature fluctuations at the growth interface cause striations, and that hydrodynamic fluctuations in a quasi-isothermal growth system do not cause striations. The theoretically derived conditions were experimentally established and allowed the growth of striation-free crystals of $KTa_{1-x}Nb_xO_3$"KTN" solid solutions. Hydrodynamic variations from the accelerated crucible rotation technique ACRT did not cause striations as long as the temperature was controlled within $0.03^{\circ}$ at $1200^{\circ}C$ growth temperature. Alternative approaches to solve or reduce the segregation and striation problems in growth from melts and from solutions are discussed as well.

CU+ ION EXTRACTION FROM A MODIFIED BERNAS ION SOURCE IN A METAL-ION IMPLANTER

  • Hong, In-Seok;Lee, Hwa-Ryun;Trinh, Tu Anh;Cho, Yong-Sub
    • Nuclear Engineering and Technology
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    • 제41권5호
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    • pp.709-714
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    • 2009
  • An ion implanter, which can serve as a metal-ion supply, has been constructed and performance tested. Copper ions are generated and extracted from a Bernas ion source with a heating crucible that provides feed gases to sustain the plasma. Sable arc plasmas can be sustained in the ion source for a crucible temperature in excess of $350^{\circ}C$. Stable extraction of the ions is possible for arc Currents less than 0.3 A. Arc currents increase with the induced power of a block cathode and the transverse field in the ion source. $Cu^+$ ions in the extracted beam are separated using a dipole magnet. A $20{\mu}A$ $Cu^+$ ion current can be extracted with a 0.2 A arc current. The ion current can support a dose of $10^{16}ions/cm^2$ over an area of $15\;cm^2$ within a few hours.

마이크로 파를 이용한 현무암 용융과 섬유 제조 (Microwave Melting of the Basalt Rock and Fiber Spinning)

  • 허유;김형진;양희원;전경진
    • 한국정밀공학회지
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    • 제26권2호
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    • pp.78-85
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    • 2009
  • High performance functional fibers are demanded increasingly in the modern industries, while the inorganic fibers such as carbon fibers, glass fibers, and metal fibers are representative among them in that they have high strength, consistent properties in a broad temperature change, etc.. This paper reports on the experimental trial to apply the microwave furnace on melting the natural basalt rock that spreads overall on the global surface and is supposed to be used as the raw material for the inorganic high performance fiber. Results showed that the new method to use the microwave as the heating source to melt the basalt rock was feasible. The crucible spinning could effectively applied for producing the basalt fibers up to 10 micrometer diameter, when the crushed basalt rocks were used. For drawing the molten basalt the drawing roller surface feature was a very important factor.

새로운 이온화된 클라스터 빔원의 제작과 특성 조사 (Investigation of New Ionized Cluster Beam Source)

  • 고석근;장홍규;정형진;최원국
    • 한국진공학회지
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    • 제5권3호
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    • pp.251-257
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    • 1996
  • The present paper the results of development of first experimental tests of a new ionized cluster beam (ICB) source. The novelty of ICB source lies in the fact that the crucible and ionization parts are spaced in one cylincrical shell but are not divided inan electric circuit. The ICB source adapts permanent mannets to increase the ionixation efficiency. The maximum obtained Cu+ ion current density I s1.5μA/㎠ 이었으며, 증착율이 초당 0.4Å일 때 이온화율은 3% 이었으며, 증착율이 초당 0.2Å일때는 이온화율이 6%이었다. 증착율이 초당 0.2Å이고, 가속전압이 4kV에서는 Cu+ 이온빔의 균일성이 95%이상이었다.

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Misaligned된 비균일자장이 인가된 초크랄스키 실리콘 단결정성장에 대한 수치적 해석 (A NUMERICAL ANALYSIS OF CZOCHRALSKI SINGLE CRYSTAL GROWTH OF SILICON WITH MISALIGNED CUSP MAGNETIC FIELDS)

  • Kim, Chang Nyung
    • Journal of the Korean Society for Industrial and Applied Mathematics
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    • 제4권1호
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    • pp.121-131
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    • 2000
  • Melt flow, heat and mass transfer of oxygen have been analyzed numerically in the process of Czochralski single crystal growth of silicon under the influence of misaligned cusp magnetic fields. Since the silicon melt in a crucible for crystal growth is of high temperature and of highly electrical-conducting, experimentation method has difficulty in analyzing the behavior of the melt flow. A set of simultaneous nonlinear equations including Navier-Stokes and Maxwell equations has been used for the modelling of the melt flow which can be regarded as a liquid metal. Together with the melt flow which forms the Marangoni convection, a flow circulation is observed near the comer close both to the crucible wall and the free surface. The melt flow tends to follow the magnetic lines instead of traversing the lines. These flow characteristics helps the flow circulation exist. Mass transfer characteristics influenced by the melt flow has been analyzed and the oxygen absorption rate to the crystal has been calculated and turned out to be rather uniform than in the case of an aligned magnetic field.

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