• Journal of the Korean Society of Fisheries and Ocean Technology
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• v.51 no.4
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• pp.561-566
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• 2015

In this study, the effect of temperature effect of the rubber matrix filled with nano sized silica particles composites with silica volume fraction of 19-25% was investigated by the Charpy impact test. The Charpy impact test was conducted in the temperature range from $-40^{\circ}C$ to $0^{\circ}C$. The critical energy release rate GIC of the rubber matrix composites filled with nano sized silica particles was considerably affected by temperature and it was shown that the maximum value was appeared at higher temperature between temperature tested and it was shown that the value of GIC increases as temperature tested increases. The major fracture mechanisms were matrix deformation, silica particle debonding and delamination, microcrack between particles and matrix, and/or pull out between particles and matrix which is ascertained by SEM photographs of Charpy impact surfaces fracture.

• Tunnel and Underground Space
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• v.20 no.5
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• pp.344-351
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• 2010

Slip along a frictional fracture can be approached as initiation and propagation of a mode II crack along its own plane. Fracture mechanics theories predict that under pure mode II loading initiation will occur when the energy release rate of the fracture attains a critical value ($G_{IIC}$), which is generally taken as a material property. For the past few years the rock mechanics group at Purdue University has investigated experimentally the dependence of $G_{IIC}$ on normal stress and on the frictional characteristics of a fracture. A number of experiments has been conducted first on acrylic, a material that, using photoelastic methods, allows visualization of the stress field ahead of the fracture tip; and later on gypsum, a rock model material with relatively low unconfined compression strength. The experimental investigation has been expanded to include other frictional materials with higher unconfined compression strength. Direct shear tests have been conducted on specimens made with cement paste. New observations together with previous experiments indicate that $G_{IIC}$ can only be considered a material property when the peak friction angle of the discontinuity is similar to the residual friction angle; otherwise the critical energy release rate increases with normal stress.

• Journal of Ocean Engineering and Technology
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• v.16 no.4
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• pp.42-47
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• 2002

This paper describes the effect of loading rate, specimen geometries and material properties for Mode II interlaminar fracture toughness of hybrid composite by using end notched flexure(ENF) specimen. In the range of loading rate 0.5~2mm/min, there is found to be no significant effect of loading rate with the value of critical energy release rate( $G_{IIc}$). there is no dependence of the interlaminar fracture energy upon the specimen width over the specimen widths examined. The value of $G_{IIc}$ for variation of initial crack length are nearly similiar values when material properties are CF/CF and GF/GF, however, the value of $G_{IIc}$ are highest with the increasing intial crack length at CF/GF. The values of $G_{IIc}$ for variation material properties are higher with the increasing moulding pressure when moulding pressures are 307, 431, 585㎪. The SEM photographs show good fiber distribution and interfacial bonding of hybrid composites when the moulding is the CF/GF.e CF/GF.

• Journal of the Korean Chemical Society
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• v.47 no.5
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• pp.472-478
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• 2003

In this work, the zeolite/diglycidylether of bisphenol A(DGEBA) systems were investigated in terms of the cure kinetics and mechanical interfacial properties of the composites. The 4, 4-diamino diphenyl methane(DDM) was used as a curing agent for epoxy. Two types of zeolite(PZ) were prepared with 15 and 35 wt% KOH treatments(15-BZ and 35-BZ, respectively) for 24 h, and their surface characteristics were studied by X-ray photoelectron spectroscopy (XPS) and X-ray diffraction(XRD). Cure kinetics of the composites were examined in the context of differential scanning calorimetry(DSC), and mechanical interfacial properties were investigated in critical stress intensity factor($K_{IC}$) and critical strain energy release rate($G_{IC}$). In the results of XPS and XRD, sodium ion(Na) of zeolite was exchanged for potassium ion(K), resulting from the treatment of KOH. Also, $Si_{2p}/Al{2p}$ composition ratios of the treated zeolite were increased, which could be attributed to the weakening of Al-O bond in framework. Cure activation energy($E_a$) of 15-BZ composites was decreased, whereas KIC and $G_{IC}$ were increased, compared with those of the pure zeolite/DGEBA composites. It was probably accounted that the acidity of zeolite was increased by surface treatments and the cure reaction between zeolite and epoxy was influenced on the increased acidity of zeolite.

• Korean Chemical Engineering Research
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• v.43 no.5
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• pp.632-636
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• 2005

In this work, the effect of chemical treatments on surface properties of SiC was investigated in thermal and mechanical interfacial behaviors of SiC/PMMA nanocomposites. The acid/base value, contact angles, and FT-IR analysis were performed for the study of surface characteristics of the SiC studied. The thermal stabilities of the SiC/PMMA nanocomposites were investigated by thermogravimetric analysis (TGA). Also the mechanical interfacial properties of the composites were studied in critical stress intensity factor ($K_{IC}$) and critical strain energy release rate ($G_{IC}$) measurements. As a result, the acidically treated SiC (A-SiC) had higher acid value than that of untreated SiC (V-SiC) or basically treated SiC (B-SiC). The acidic solution treatment led to an increase in surface free energy of the SiC, mainly due to the increase of its specific component. Thermal and mechanical interfacial properties of the SiC/PMMA nanocomposites, including initial decomposition temperature (IDT), $K_{IC}$, and $G_{IC}$ had been improved in the acidic treatment on SiC. This was due to the improvement in the interfacial bonding strength, resulting from the acid-base interfacial interactions between the fillers and polymeric matrix.

• Composites Research
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• v.21 no.4
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• pp.7-14
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• 2008

Prediction of the load-bearing capacity of an adhesive-bonded Joint is of practical importance for engineers. This paper introduces interface fracture mechanics approach to predict the load-bearing capacity of composite metal bonded joints. The adhesion strength of composite/steel bonding is evaluated in terms of the energy release rate of an interfacial crack and the fracture toughness of the interface. Virtual track closure technique (VCCT) is used to calculate energy release rates, and hi-material end-notched flexure (ENF) specimens are devised to measure the interfacial fracture toughness. Bi-material ENF specimens gave consistent mode II fracture toughness $(G_{IIc})$ values of the composite/steel interface regardless of the thickness of specimens. The critical energy release rates of double-lap joints showed a good agreement with the measured fracture toughness. Therefore. the energy-based interfacial fracture characterization can be a practical engineering tool for predicting the load-bearing capacity of bonded joints.

• Composites Research
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• v.28 no.6
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• pp.361-365
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• 2015

The influence of MWCNTs on fracture toughness properties of MWCNTs/Nickel-Pitch Fibers/epoxy composites (MWCNTs/Ni-PFs/epoxy) was investigated according to MWCNTs content. Nickel-Pitch-based carbon fibers (Ni-PFs) were prepared by electroless nickel-plating. The surface properties of Ni-PFs were determined by scanning electron microscopy (SEM) and X-ray photoelectron spectrometry (XPS). The fracture toughness of MWCNTs/Ni-PFs/epoxy was assessed by critical stress intensity factor ($K_{IC}$) and critical strain energy release rate ($G_{IC}$). From the results, it was found that the fracture toughness properties of MWCNTs/Ni-PFs/epoxy were enhanced with increasing MWCNTs content, whereas the value decreased above 5 wt.%. MWCNTs content. This was probably considered that the MWCNTs entangled with each other in epoxy due to an excess of MWCNTs.

• Macromolecular Research
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• v.17 no.8
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• pp.585-590
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• 2009

The cure behaviors, dielectric characteristics and fracture toughness of diglycidylether of bisphenol-A (DGEBA)/poly(ethylene terephthalate) (PET) blend system were investigated. The degree of conversion for the DGEBA/PET blend system was measured using Fourier transform infrared (FTIR) spectroscopy. The cure kinetics were investigated by measuring the cure activation energies ($E_a$) with dynamic differential scanning calorimetry (DSC). The dielectric characteristic was examined by dielectric analysis (DEA). The mechanical properties were investigated by measuring the critical stress intensity factor ($K_{IC}$), critical strain energy release rate ($G_{IC}$), and impact strength test. As a result, DGEBAIPET was successfully blended. The Ea of the blend system was increased with increasing PET content to a maximum at 10 phr PET. The dielectric constant was decreased with increasing PET content. The mechanical properties of the blend system were also superior to those of the neat DGEBA. These results were attributed to the increased cross-linking density of the blend system, resulting from the interaction between the epoxy group of DGEBA and the carboxyl group of PET.

• Journal of the Korean Society of Fisheries and Ocean Technology
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• v.19 no.1
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• pp.79-84
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• 1983

The test specimen, designated the double cantilever beam, was employed for a fracture mechanics study of stress corrosion cracking (SCC) of type 5083 Al-alloy in seawater. Stress intensities for this DCB specimen were calculated by using compliance, strain energy release rate and relation between stress intensity and strain energy release rate. Analytical expression for compliance as a function of crack length was obtained by applying beam theory. It was investigated that the polarization potentials affected the growth rate and surface of stress corrosion cracking. The results are as follows, The critical stress intensity was 134.81-148.38kg/mm super(3/2) and K sub(Ii) under polarization potentials was 75.92-145.78kg/mm super(3/2). The minimum stress corrosion crack growth rate was occurred at-987mV SCE. Insoluble compound on $\beta$ phase was looked into through SCC. The greater anodic potential is, the larger insoluble compound on $\beta$ phase becomes.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.20 no.9
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• pp.2894-2900
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• 1996

The stream generator tubes represent an integral part of a major barrier against the fission product release to the environment. So, the rupture of these tubes could permit flow of reactor coolant into the secondary system and injure the safety of reactor coolant system. Therefore, if the crack was detected during In-Service Inspection of tubes the cracked tube should be evaluated by the pulgging criteria and plugged or not. In this study, the fracture mechanics evaluation is carried out on the thru-wall axial crack due to Primary Water Stress Corrosion Cracking in the roll transition aone of steam generator tube to help the assurence the integrity of tubes and estabilish the plugging criteria. Due to the Inconel which is used as tube material is more ductile than others, the plastic instability repture theory was used to calculate the critical and allowable crack length. Based on Leak Before Break concept the leak rate for the critical crack length and the allowable leak rate are compared and the safety of tubes was given.