• Applied Microscopy
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• v.43 no.4
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• pp.164-172
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• 2013

In this work, microstructural and hardness evolution of the X20 steel upon short-term creep test ($550^{\circ}C$ to $650^{\circ}C$, $180^{\circ}C$ to 60 MPa) was studied by using scanning electron microscope, electron backscattered diffraction, and transmission electron microscope, microhardness tester. After creep rupture, gauge and grip part of the specimens were microstructurally analyzed. Creep at the $650^{\circ}C$/60 MPa resulted in a rupture at 1,460 hours with growth of lath width from 1.31 to $2.87{\mu}m$ and a grain growth with a more equiaxed feature. There is a close relationship between Microhardness and lath width. The formation and coarsening of Laves phase, which was observed up to $600^{\circ}C$ of creep temperature, was accelerated by the applied stress. Slight coarsening of the $M_{23}C_6$ was observed in the $550^{\circ}C$ and $600^{\circ}C$ crept or aged specimens. The coarsening of $M_{23}C_6$ depended on the temperature, where specimens crept at $650^{\circ}C$ showed higher growth rate. The microstructural evolution of X20 after short-term creep test was extensively discussed in relation to the long-term creep/aging test reported in literatures.

• Geotechnical Engineering
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• v.9 no.4
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• pp.55-64
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• 1993

The Undrained creep tests on the normally consolidated clays with four different consolication ratios(c3c'/clc': 1.0, 0.7, 0.5, 0.4) were performed to investigate the effects of avisotropic consolidation on the undrained creep rupture behavior. The elapsed time to a certain minimum strain rate is decreased with decreasing the value of the consolidation pressure ratio, and the elapsed time to rupture for a certain minimum strain rate is also decreased with decreasing the ratio. The upper yield strength obtained from the equation suggested by Finn and Shead(1.) is coincided well with the creep strength irrespective of the magnitude of the consolidation pressure ratio, and the normallised upper yielding strength by mean confining pressure is decreased with increasing the consolidation pressure ratio. The critical strain for creep rupture, the strain at min. strain rate, is constant irrespective of the magnitude of creep stress, but it increased exponentially with increasing the ratio, It accordingly is dangerous that the potential of in-situ creep rupture is estimated only by the creep rupture test on the isotropically consolidated clay in case of K0-value below 1.0.

• Korean Journal of Materials Research
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• v.33 no.10
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• pp.406-413
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• 2023

This study used optical and scanning electron microscopy to analyze the surface oxidation phenomenon that accompanies a γ'-precipitate free zone in a directional solidified CM247LC high temperature creep specimen. Surface oxidation occurs on nickel-based superalloy gas turbine blades due to high temperature during use. Among the superalloy components, Al and Cr are greatly affected by diffusion and movement, and Al is a major component of the surface oxidation products. This out-diffusion of Al was accompanied by γ' (Ni₃Al) deficiency in the matrix, and formed a γ'-precipitate free zone at the boundary of the surface oxide layer. Among the components of CM247LC, Cr and Al related to surface oxidation consist of 8 % and 5.6 %, respectively. When Al, the main component of the γ' precipitation phase, diffused out to the surface, a high content of Cr was observed in these PFZs. This is because the PFZ is made of a high Cr γ phase. Surface oxidation of DS CM247LC was observed in high temperature creep specimens, and γ'-rafting occurred due to stress applied to the creep specimens. However, the stress states applied to the grip and gauge length of the creep specimen were different, and accordingly, different γ'-rafting patterns were observed. Such surface oxidation and PFZ and γ'-rafting are shown to affect CM247LC creep lifetime. Mapping the microstructure and composition of major components such as Al and Cr and their role in surface oxidation, revealed in this study, will be utilized in the development of alloys to improve creep life.

• Korean Journal of Materials Research
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• v.14 no.8
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• pp.558-564
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• 2004

In order to improve the low hardness and low wear resistance of Ti-6Al-4V alloy, plasma carburization treatment and CrN film coating were carried out. Effects of the plasma carburization and CrN coating were analyzed and compared with the non-treated alloy by mechanical and creep tests. After plasma carburization and CrN coating treatments, the carburized layer was about 150 ${\mu}m$ in depth and CrN coated layer was about 7.5 ${\mu}m$ in thickness. Hardness value of about $H_{v}$ 402 of the non-treated alloy was improved to $H_{v}$ 1600 and 1390 by plasma carburization and CrN thin film coating, respectively. Stress exponent(n) was decreased from 9.10 in CrN coating specimen to 8.95 in carburized specimen. However, the activation energy(Q) was increased from 242 to 250 kJ/mol. It can be concluded that the static creep deformation for Ti-6Al-4V alloy is controlled by the dislocation climb over the ranges of the experimental conditions.

• Geotechnical Engineering
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• v.4 no.3
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• pp.53-62
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• 1988

When a ground soil is under the constant continuous stress less than the failure strength of that soil, its deformation, in some cases, will increase continuously as time goes on due to creep phenomena. Deformation of soil caused by creep behavior will appear in various types depending on the elastic, plastic, viscous properties of soil. Therefore in this study, visco-plastic characteristics of grouted soil was studied by analysing the result of uniaxial creep test on the grouted soil. As a result of this research, it was found that the rheological model of grouted soil can be decided as Vyalov model and the visco-plastic properties of grouted soil is influenced by the content of silicate in grout.

• Geomechanics and Engineering
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• v.7 no.3
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• pp.279-295
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• 2014

A series of one-dimensional consolidation tests and triaxial creep tests were performed on Nansha clays, which are interactive marine and terrestrial deposits, to investigate their time-dependent behaviour. Based on experimental observations of oedometer tests, normally consolidated soils exhibit larger secondary compression than overconsolidated soils; the secondary consolidation coefficient ($C_{\alpha}$) generally gets the maximum value as load approaches the preconsolidation pressure. The postsurcharge secondary consolidation coefficient ($C_{\alpha}$') is significantly less than $C_{\alpha}$. The observed secondary compression behaviour is consistent with the $C_{\alpha}/C_c$ concept, regardless of surcharging. The $C_{\alpha}/C_c$ ratio is a constant that is applicable to the recompression and compression ranges. Compared with the stage-loading test, the single-loading oedometer test can evaluate the entire process of secondary compression; $C_{\alpha}$ varies significantly with time and is larger than the $C_{\alpha}$ obtained from the stage-loading test. Based on experimental observations of triaxial creep tests, the creep for the drained state differs from the creep for the undrained state. The behaviour can be predicted by a characteristic relationship among axial strain rate, deviator stress level and time.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.35 no.6
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• pp.609-617
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• 2011

There is a trend towards the progressive use of higher operating temperatures and stresses to achieve improved efficiencies in power-generation equipment. It is important to perform the crack assessment under hightemperature and high-pressure conditions. The C(t)-integral is a key parameter in crack assessment for transient creep states. The estimation of the C(t)-integral is complex when considering the mechanical and thermal loads simultaneously. In this paper, we study estimation of C(t)-integral under combined mechanical and thermal load depending on loading conditions.

• Journal of the Korean Society for Heat Treatment
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• v.28 no.2
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• pp.68-74
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• 2015

The low cycle fatigue (LCF) and creep-fatigue (hold time tension fatigue, HTTF) tests were performed on the modified 25Cr-13Ni cast stainless steel, which was selected as a candidate material for exhaust manifold in automotive engine. The exhaust manifold is subjected to an environment in which heating and cooling cycle occur due to the running pattern of automotive engine. Several types of fatigue behaviour such as thermal fatigue, thermal mechanical fatigue and creep-fatigue are belong to the main failure mechanisms. High temperature tensile test was firstly carried out to compare the sample with the traditional cast steel for the component. The low cycle fatigue and HTTF tests were carried out under the strain controlled condition with the total strain amplitude from ${\pm}0.6%$ to ${\pm}0.7%$ at $800^{\circ}C$. The hysteresis loops of HTTF tests showed significant stress relaxation during tension hold time. With the increase of tension hold time, the fatigue life was remarkably deceased which caused from the formation of intercrystalline crack by the creep failure mechanism.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2002.10a
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• pp.693-696
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• 2002

This study examined the effects of the testing temperature on the mechanical properties of the carbon tool steel (SK4M) for flat spring. Hardness test and fatigue test were performed at room temperature ($20^{\circ}C$). Tensile test and creep test were performed at temperature range $20^{\circ}C$ ~$160^{\circ}C$. The micro-vickers hardness values of SK4M was Hv=584. The Elastic modulus, tensile strength and yield strength of SK4M at 160t test temperature were decreased 0.92 time, 0.97 time and 0.82 time those of SK4M at 2$0^{\circ}C$ test temperature, respectively. The maximum creep strain for 100hr at creep temperature ($80^{\circ}C$ ~$160^{\circ}C$) and creep stress ($37.4Kgf/\textrm{mm}^2$ ~$93.6Kgf/\textrm{mm}^2$) was 0.572%. The fatigue limit of SK4M was $94Kgf/\textrm{mm}^2$.

• Korean Journal of Metals and Materials
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• v.48 no.9
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• pp.791-797
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• 2010

The creep crack growth rate (da/dt) of the Cr-Mo steels tested by pre-crack and the voltage (or resistance) variables were related into fracture parameter (Ct), crack growth coefficient (H), and an exponent (q) in the parts of Base, weld and HAZ. The fracture parameter (Ct) has various variables relating to the specimen and crack shape, applied stress, and creep strain curve. The H and q was inferred by OLS regression (ordinary least square method), and the H values were solved in statistics and probability assessment, which were attained fromPDF's distributions (probability density function). The HAZ part has the highest value of q by OLS regression and the widest distribution of H by PDF of WEIBULL, which means that the crack sensitivity of HAZ should be cautioned against the creep crack growth and failure.