• 한국건설순환자원학회논문집
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• 제10권4호
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• pp.577-583
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• 2022

본 연구에서는 고로슬래그 미분말, 팽창재 및 무수석고로 이루어진 무기계 자기치유 소재를 사용하여 제조한 자기치유 모르타르의 특성을 조사하였다. 무기계 치유재료의 사용량이 다른 3종류의 자기치유 모르타르를 대상으로 압축강도를 측정하고 정수위 투수시험를 통하여 치유성능을 평가하였다. 치유성능 평가지표로 균열유도재령애 따른 치유율과 등가균열폭을 활용하였다. 자기치유 모르타르의 압축강도 발현, 치유재령에 따른 치유율 변화와 경제성을 고려하여 무기계 혼합재의 최적 사용량을 시멘트 질량 대비 20 %로 제안하였다.

• 대한기계학회논문집A
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• 제31권11호
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• pp.1108-1114
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• 2007

The low kinds of $Al_2O_3$ composite ceramics were prepared using a mixture of 85 wt.% $Al_2O_3$ (mean size $0.5\;{\mu}m$), 15 wt.% SiC Powder with $Y_2O_3$, as an additive powder (0, 1, 3 and 5 wt.%). The crack-healing strengths were studied as functions of crack-healing temperature and amount of $Y_2O_3$. The in-situ crack-healing behavior was observed at 1,573 K for 1 h in the air. The heat treated specimen with 3 wt.% of $Y_2O_3$ showed better crack-healing ability than specimen with 1 or 5 wt.% of $Y_2O_3$. In case of specimen with 3 wt.% of $Y_2O_3$, the bending strength of the crack-healed specimen at 1,473 K was recovered to the bending strength of smooth specimen treated at 1573 K. The heat-resistance limit temperature of $Al_2O_3$ composite ceramics was 1,073 K, 1,373 K, 873 K for the specimen with 1, 3, 5 wt.% of $Y_2O_3$.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2009년도 춘계 학술대회 제21권1호
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• pp.441-442
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• 2009

Concrete has some self-healing ability if the crack is occurred. Concrete with a inorganic-organic chemical compound, self-healing ability is increased at the surface of the crack. In this study, we investigate self-healing performance of concrete using admixutre by performing permeability test.

• 한국건설순환자원학회논문집
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• 제9권3호
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• pp.375-382
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• 2021

자기치유 콘크리트는 직접적인 보수보강 없이도 스스로 구조물의 균열을 치유하여 효율적으로 콘크리트 구조물의 수명연장이 가능하다는 측면에서 각광받고 있다. 현재 자기치유 콘크리트는 전 세계적으로 활발히 연구가 진행되고 있는 분야이지만 대부분의 연구는 치유 성능의 향상에 초점을 맞추고 있기 때문에 객관적으로 치유성능을 평가하는 방법은 부족한 실정이다. 자기치유 콘크리트의 성능평가에 활용하기 위해 기체확산실험 방법이 개발된 바가 있지만, 시편의 포화도 및 실험시의 온습도 등과 같은 환경조건의 통제가 필요하다는 단점이 있다. 따라서 본 연구에서는 기체 확산 실험시에 필요한 환경조건을 대폭 완화하여 적용성을 향상시키고자 하였다. 아울러 실험시간을 단축시키고자 사전 안정화 과정을 도입하였고, 약 20분이내의 실험시간에서 3%이내의 오차 수준으로 균열폭의 추정이 가능하였다.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2003년도 춘계학술대회 논문집
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• pp.1495-1498
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• 2003

Recently, self-healing methods of a cracked matrix, especially polymeric composite materials, became the center of engineering researchers. In this paper, we summarized the self-healing concept for polymeric composite materials and investigated the effect of microparticle on the crack growth behavior in colorless and transparent matrix by experimental observation to describe the crack propagation around the microparticle inside epoxy matrix composite. Compression splitting test for the specimen involving microparticle was conducted. In addition, FE analysis was pursued to present the stress contour around microparticle in the matrix. Through the experiments and FE analysis, we found that the size. relative position, bonding condition and relative stiffness of microparticle are important parameters to decide the direction of crack propagation, which is related to the rupture of microparticle for self-healing

• 한국세라믹학회지
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• 제54권6호
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• pp.492-498
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• 2017

A thermal barrier coating (TBC) with self-healing property for cracks was proposed to improve reliability during gas turbine operation, including structural design. Effect of healing agent on crack propagation behavior in TBCs with and without buffer layer was investigated through furnace cyclic test (FCT). Molybdenum disilicide ($MoSi_2$) was used as the healing agent; it was encapsulated using a mixture of tetraethyl orthosilicate and sodium methoxide. Buffer layers with composition ratios of 90 : 10 and 80 : 20 wt%, using yttria stabilized zirconia and $MoSi_2$, respectively, were prepared by air plasma spray process. After generating artificial cracks in TBC samples by using Vickers indentation, FCTs were conducted at $1100^{\circ}C$ for a dwell time of 40 min., followed by natural air cooling for 20 min. at room temperature. The cracks were healed in the buffer layer with the healing agent of $MoSi_2$, and it was found that the thermal reliability of TBC can be enhanced by introducing the buffer layer with healing agent in the top coat.

• 한국안전학회지
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• 제27권6호
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• pp.109-114
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• 2012

This study is the things to experiment and evaluate the performance of self-healing water-proofing on the concrete to be using the crystal growth composite waterproofing admixture. The cylinder to be making on the concrete by ${\varnothing}150{\times}300$ mm for evaluating the performance of self-healing water-proofing was aging 90 days and cut on a 50 mm. So, it prompted the crack and applied. After it measured the quantity of water to be flow the water throughout the crack part of the cylinder, it applied the basic formular of Darcy's law and calculated the coefficient of water permeability. So, it verified the performance of self-healing water-proofing on the basis of the changing shape of the water permeability. This experiment is the thing to be applied the general evaluation of the structure to demand the real watertightness on doing for the evaluating of performance of the quantity of water leak and self-healing water-proofing about the various penetration crack.

• 한국건설순환자원학회논문집
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• 제10권4호
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• pp.600-608
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• 2022

이 연구는 전기영동확산시험을 이용하여 이중층수산화물(LDH)을 혼입한 균열이 있는 자기치유 시멘트 모르타르의 염화물 침투 저항성을 평가하여 LDH가 자기치유 콘크리트의 치유 효과에 미치는 영향을 고찰하였다. 실험결과에 따르면 자기치유물질만 혼입한 경우와 자기치유물질과 Ca-Al LDH를 함께 혼입한 경우 균열 발생 직후 영동확산계수는 대부분 OPC 배합에 비해 더 컸지만, 치유재령이 경과할수록 OPC 보다 더 큰 폭으로 영동확산계수가 감소하며, Ca-Al LDH를 함께 혼입한 경우가 자가치유 물질만 혼입한 경우보다 영동확산계수 감소가 더 크게 나타나 더 높은 자기치유 성능을 보였다. 이는 균열면에 자기치유 반응생성물이 증가하면서 균열 내부에서 LDH에 의한 염소이온의 구속작용이 더 커진다는 것을 시사한다.

• 한국해양공학회지
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• 제22권3호
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• pp.71-75
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• 2008

This paper illustrates haw $Y_2O_3$ contributes to crack-healing strengths as a function of crack-healing temperature and the additive amount. In investigating mechanical properties, the indentation fracture method is very simple and useful, but careful attention must be paid to the statistical data processing because data may be scattered excessively, especially for brittle materials. To estimate accurate AE signal properties we applied the useful time-frequency method with a discrete wavelet analysis algorithm. In experiments, three kinds of specimens were prepared. After the specimens were indented by a Vickers indentor, they were heat-treated and crack-healed to evaluate bending strength and the AE signal. With higher amounts of the additive powder, as 1, 3, or 5% wt. of $Y_2O_3$, the concentrative tendency of dominant frequency trended toward lower frequency groups. The $Al_2O_3$ ceramic with 3% wt. of $Y_2O_3$ was judged most suitable because it demonstrated superior crack-healing ability and relative concentration on the highest frequency group.

• 한국해양공학회:학술대회논문집
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• 한국해양공학회 2004년도 학술대회지
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• pp.337-341
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• 2004

Engineering ceramics have superior heat resistance, corrosion resistance, and wear resistance. Consequently, these art significant candidates for hot-section structural components of heat engine and the inner containment of nuclear fusion reactor. Besides, some of them have the ability to heal cracks and great benefit can be anticipated with great benefit the structural engineering field. Especially, law fracture toughness of ceramics supplement with self-healing ability. In the present study, we have been noticed some practically important points for the healing behavior of silicon nitride, alumina, mullite with SiC particle and whisker. The presence of silicon carbide (SiC) in ceramic compound is very important for crack-healing behavior. However, self-healing of SiC has not been investigated well in detail yet. In this study, commercial SiC was selected as sample, which can be anticipated in the excellent crack healing ability. The specimens were produced three-point bending specimen with a critical semi-circular crack of which size that is about $50-700{\mu}m$. Three-point bending test and static fatigue test were performed cracked and healed SiC specimens. A monotonic bending load was applied to cracked specimens by three-point loading at different temperature. The purpose of this paper is to report Strength Properties and Elastic Waves Characteristics of Silicon Carbide with Crack Healing Ability.