• Transactions of the Korean Society of Mechanical Engineers
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• v.17 no.6
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• pp.1321-1329
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• 1993

Long time creep strength and life prediction of 1% Cr-Mo-V and 12% Cr rotor steel were performed by using round-bar type specimens under static load at 500-600.deg. C TTP (time temperature parameter), MCM (minimum commitment method) and ISM (initial strain method newly devised) as life prediction methods were investigated, and the results could be summarized as follows. (1) The minimum parameter of SEE (standard error) by TTP was proved as LMP (larson-miller parameter), and the minimum parameter of RMS (root mean squares), by data less than 10$^{3}$hrs was MHP (manson-haferd parameter). (2) The parameters of the minimum and the maximum strength values predicted in $10^{5}$hrs creep life of 1% Cr-Mo-V steel by TTP were LMP and MSP, respectively. In case of 12% Cr steel above $550^{\circ}C$ OSDP (orr-sherby-dorn parameter) was minimum and MSP (manson-succop parameter) was maximum, but below $550^{\circ}C$, the inverse phenomena was observed. On the other hand the creep strengths before $10^{3}hrs$ life by MCM were similar to those by TTP, but the strengths after $10^{3}hrs$ life were 10-25% lower than those by TTP. (3) Creep strengths by ISM were maximum 5% lower than those by TTP. Because $10^{5}hrs$ strengths were similar to those of the lower band by TTP, the ISM was safer than the TTP.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.7 s.178
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• pp.1771-1778
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• 2000

The purpose of this study is to investigate the thermal embrittlement and the mechanical properties of 2.25Cr-1Mo steel aged at high temperature for the extended periods. Original, aged artificiall y and used material were tested to obtain the tensile strength, hardness and impact absorbed energy. Tensile strength, hardness and impact absorbed energy decreased with the increasing aging time. The carbide morphology with the thermal embrittlement was found to contribute to the mechanical property change by X-Ray diffraction method.

• Journal of Ocean Engineering and Technology
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• v.3 no.2
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• pp.125-137
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• 1989

To check technical improvement in the soundness and strength of 12% Cr steel rotor, a 25 tons of rotor with 65 tons of ingot was made in real size and was cut to pieces to take test samples, and the various mechanical tests such as impact, tensile, creep, and fatigue were carried out. The strengths are compared with those of 1% Cr-Mo-V rotor of same size. Microstructures of the samples are examined and reviewed. The results can be summarized as follows. 1) Fracture appearance transition temperatures are 80.deg. C at the center part and 60.deg. C near surface of 12% Cr rotor, and 8.deg. C near surface of 1% Cr-Mo-V rotor. 2) Comparative rapid softening occurs at higher temperatures above 600.deg. C for 12% Cr steel and 550.deg. C for 1% Cr-Mo-V steel in tension tests. 3) Fatigue crack propagation rate of 12% Cr steel is almost same as that of 1% Cr-Mo-V steel at the same corresponding surface part of the rotors. The crack growth rate of center part of 12% Cr rotor is faster than near surface part of the rotor, and the crack growth rate at the load condition of R=0.04 is slower than that of the load condition of R=0.5 for both 12% Cr steel and 1% Cr-Mo-V steel. 4) Crack growth rate of radial direction near surface of 12% Cr rotor is faster than that of transverse direction at the same part because of the difference in residual stresses. 5) Both creep and fatigue strengths of 12% Cr steel are superior to those of 1% Cr-Mo-V steel and the difference is thought the effect of climb and glide controlled creep by solid solution of alloying elements and dispersion of carbides.

• Journal of Ocean Engineering and Technology
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• v.3 no.2
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• pp.625-625
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• 1989

To check technical improvement in the soundness and strength of 12% Cr steel rotor, a 25 tons of rotor with 65 tons of ingot was made in real size and was cut to pieces to take test samples, and the various mechanical tests such as impact, tensile, creep, and fatigue were carried out. The strengths are compared with those of 1% Cr-Mo-V rotor of same size. Microstructures of the samples are examined and reviewed. The results can be summarized as follows. 1) Fracture appearance transition temperatures are 80.deg. C at the center part and 60.deg. C near surface of 12% Cr rotor, and 8.deg. C near surface of 1% Cr-Mo-V rotor. 2) Comparative rapid softening occurs at higher temperatures above 600.deg. C for 12% Cr steel and 550.deg. C for 1% Cr-Mo-V steel in tension tests. 3) Fatigue crack propagation rate of 12% Cr steel is almost same as that of 1% Cr-Mo-V steel at the same corresponding surface part of the rotors. The crack growth rate of center part of 12% Cr rotor is faster than near surface part of the rotor, and the crack growth rate at the load condition of R=0.04 is slower than that of the load condition of R=0.5 for both 12% Cr steel and 1% Cr-Mo-V steel. 4) Crack growth rate of radial direction near surface of 12% Cr rotor is faster than that of transverse direction at the same part because of the difference in residual stresses. 5) Both creep and fatigue strengths of 12% Cr steel are superior to those of 1% Cr-Mo-V steel and the difference is thought the effect of climb and glide controlled creep by solid solution of alloying elements and dispersion of carbides.

• Journal of Power System Engineering
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• v.8 no.3
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• pp.18-22
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• 2004

Boiler is one of the most important utilities providing steam to turbine in order to supply mechanical energy in thermal power plant. It is composed of thousands of tubes for high efficient heat transfer. The material for boiler tubes is used in such high temperature and pressure condition as $540^{\circ}C$, 22MPa. The boiler tube material is required to resist creep damage, fatigue cracking, and corrosion damages. 2.25%Cr-1Mo steel is used for conventional boiler tubes, and austenitenite stainless steel is used for higher temperature boiler tubes. But the temperature and pressure of steam in power plant became higher for high plant efficiency. So, the property of boiler tube material must be upgaded to fit the plant property. Several boiler tube material was developed to fit such conditions. X20CrMoV12.1 steel is also developed in 1980's and used for superheater and reheater tubes in supercritical boilers. The material has martensite microstructures which is difficult to evaluate the degradation. In this thesis, degrade the X20CrMoV12.1 steel at high temperatures in electric furnace, and evaluate hardness with Vickers hardness tester and strengths with Indentation tester.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.25 no.12
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• pp.2109-2115
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• 2001

Miniaturized specimen technology is useful to characterize the mechanical behavior when it is difficult to sample the material enough for the test. In this study, two kinds of miniaturized Charpy impact specimens(i.e., miniaturized specimen with side groove and without side groove) of aged 1Cr- lMo-0.25V steel were prepared and tested. The relationship between the extent of degradation in terms of ductile brittle transition temperature(DBTT) and the fracture stress of 1Cr-1Mo-0.25V steel was established. The fracture stress obtained from miniaturized specimen without side groove turned out to be linearly related with the DBTT of standard specimen. Therefore the fracture toughness of aged turbine rotor steel might be evaluated by the fracture stress. In addition, the correlation between DBTT of standard specimen and that of miniaturized specimen was investigated. As the results of normalizing DBTT by maximum elastic tensile stress, the normalized DBTT of miniaturized specimen without side groove allows one to estimate that of standard specimen.

• Analytical Science and Technology
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• v.16 no.1
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• pp.82-89
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• 2003

Isotope dilution mass spectrometry (IDMS) was applied to the determination of Ni, Cr, Mo in low alloy steel reference materials. The Mo isotope ratio measurement was performed by dynamic reaction cell inductively coupled plasma mass spectrometry (DRC-ICP/MS) using ammonia as a reaction cell gas. In the case of Ni and Cr measurement, all data were obtained at medium resolution mode (m/${\Delta}m=3000$) of double focusing sector field high resolution inductively coupled plasma mass spectrometry (HR-ICP/MS). For the method validation of the technique was assessed using the certified reference materials such as NIST SRM 361, NIST SRM 362, NIST SRM 363, NIST SRM 364, NIST SRM 36b. This method was applied to the determination of Ni, Cr and Mo in low alloy steel sample (CCQM-P25) provided by NMIJ for international comparison study.

• Journal of the Korean institute of surface engineering
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• v.51 no.3
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• pp.149-156
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• 2018

The corrosion and strength degradation characteristics of 1.25Cr-0.5Mo steels were studied under $650^{\circ}C$ in $76%N_2+6%O_2+16%CO_2+2%SO_2$ gas condition up to 500 hrs. Corroded specimens were characterized by weight gain, scanning electron microscope(SEM), energy dispersive X-ray spectroscopy(EDS), and X-ray diffraction(XRD). The tensile test was conducted to evaluate the mechanical strength and fracture mode with corrosion at high temperature. As the results of the experiments, thick Fe-rich oxide layers over $200{\mu}m$ were formed on the surface within 500 hrs. The thick oxide layers are formed with reduction of the cross-sectional area of the specimens. Thus, the strength tended to decrease with reduction of the cross-sectional area.

• Proceedings of the KWS Conference
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• v.43
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• pp.118-120
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• 2004

Recently 9Cr-1Mo azzoy is used in the Nuclear power plant due to its special properties. This material has the merit of high-strength resistance and corrosion resistance. Therefore the demand for this alloy is dramatically increased in the Nuclear power, petro-chemical complex etc. Re various research has been conducted to improve the material properties of this alloy. In spite of this circumstance, detail research in the area of welding process of this alloy is yet to be expanded In this study the numerical non-linear heat transfer analysis of laser welding which may possibly replace the conventional SMAW fabrication of 9Cr-1Mo steel has been carried out.

• Proceedings of the KSME Conference
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• 2001.11a
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• pp.222-227
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• 2001

Nonlinear acoustic effect has been considered as an effective tool for the evaluation of material degradation. In this paper, the applicability of nonlinear acoustic effect to the evaluation of degradation of 2.25Cr-1Mo steel is investigated. Firstly, a number of 2.25Cr-1Mo steel samples were heat-treated, and their damage mechanism was examined. Secondly, Ultrasonic nonlinear parameter was measured. Nonlinear acoustic parameter was found to be clearly sensitive to the material degradation.