• Title/Summary/Keyword: Copper particle

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Detection of PED virus by the immunoelectron microscopy and immunogold conjugate immunoelectron microscopy (면역전자현미경(免疫電子顯微鏡)(IEM) 기법(技法) 및 immunogold conjugate 면역전자현미경(免疫電子顯微鏡)(IGC-IEM) 기법(技法)을 이용(利用)한 돼지 분변내 PED 바이러스의 검출(檢出))

  • Kim, Jae-hoon;Hwang, Eui-kyung;Bae, You-chan;Son, Hyun-joo;Park, Jung-won;Yoon, Yong-dhuk
    • Korean Journal of Veterinary Research
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    • v.35 no.3
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    • pp.575-581
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    • 1995
  • Both immunoelectron microscopy(IEM) and immunogold conjugate immunoelectron microscopy (IGC-IEM) techniques were developed for the detection of porcine epidemic diarrhea virus(PEDV) from the feces. Fecal samples were incubated sequentially with anti-PEDV monoclonal antibody(MoAb) and immunogold conjugated goat anti-mouse IgG+IgM. Then negatively stained, mounted on the formvar carbon-coated copper EM grids and observed by the transmission electron microscope. By the direct electron microscopy(DEM), coronavirus particles were observed from 17 cases of total 33 fecal samples of grower pigs and sows. The virons of coronavirus were moderately pleomorphic but mostly spherical, with a diameter ranged from 90 to 190nm. PED virus particles were identified from 15 cases of 17 DEM positive samples by the IEM and IGC-IEM techniques. Aggregates of PED virus coated with specific antibody were seen in fecal samples incubated with homologous anti-PED virus MoAb but not in control samples incubated with anti-TGE virus MoAb. Following incubation with immunogold-conjugated secondary antibody, the gold granules were usually distributed around and among the virus particles and soluble and viral particle-associated antigen. So, IEM and IGC-IEM techniques were proved a rapid and sensitive methods for detection and identification of PED virus from fecal and intestinal contents.

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A Comparative Study for Grinding Media Behavior and DEM Simulation at Actual Grinding Zone on a Traditional Ball Mill (매체형 전동밀의 실제 분쇄장에서 분쇄매체의 거동과 DEM 시뮬레이션의 비교연구)

  • Bor, Amgalan;Jargalsaikhan, Battsetseg;Lee, Jehyun;Choi, Heekyu
    • Korean Chemical Engineering Research
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    • v.57 no.6
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    • pp.804-811
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    • 2019
  • This study was performed the real motion and DEM simulation of ball motion using three different types of grinding media with different size and materials in media formation for optimization of process conditions in a traditional ball mill (media ball mill). In the simulation, the rotational speed of the mill, the material of the medium, the velocity of the medium, and the coefficient of friction between the media and the wall of pot were fixed into the actual experimental conditions. The motion of various kinds of grinding media was quantitatively measured by setting the grinding zone defined in the present study on the photographs taken and the snapshot images analyzed in the simulation. In addition, we observed the quantitatively measured value and the changed morphology of the sample and examined the correlation. Therefore, it is suggested to optimize the grinding media which has the greatest influence on the grinding zone under specific experimental conditions.

Comparative Evaluation of Shielding Performance according to the Characteristics of Eco-friendly Shielding Material Tungsten (친환경 차폐재료 텅스텐 특성에 따른 차폐성능 평가)

  • Kim, Seon-Chil
    • Journal of the Korea Convergence Society
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    • v.12 no.10
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    • pp.129-136
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    • 2021
  • Radiation shields used in medical institutions mainly use lead to manufacture products and fitments. Although lead has excellent processability and economic efficiency, its use is being reduced due to environmental issues when it is disposed of. In addition, when used for a long time, there is a limit to using it as a shielding film, shielding wall, medical device parts, etc. due to cracking and sagging due to gravity. To solve this problem, copper, tin, etc. are used, but tungsten is mostly used because there is a difficulty in the manufacturing process to control the shielding performance. However, it is difficult to compare with other shielding materials because the characteristics according to the type of tungsten are not well presented. Therefore, in this study, a medical radiation shielding sheet was manufactured in the same process using pure tungsten, tungsten carbide, and tungsten oxide, and the particle composition and shielding performance of the sheet cross-section were compared.As a result of comparison, it was found that the shielding performance was excellent in the order of pure tungsten, tungsten carbide, and tungsten oxide.

Assessment of The Above-Ground Carbon Stock and Soil Physico-Chemical Properties of an Arboretum within The University of Port Harcourt, Nigeria

  • Akhabue, Enimhien Faith;Chima, Uzoma Darlington;Eguakun, Funmilayo Sarah
    • Journal of Forest and Environmental Science
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    • v.37 no.3
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    • pp.193-205
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    • 2021
  • The importance of forests and trees in climate change mitigation and soil nutrient cycling cannot be overemphasized. This study assessed the above-ground carbon stock of two exotic and two indigenous tree species - Gmelina arborea, Tectona grandis, Khaya grandifoliola and Nauclea diderrichii and their litter impact on soil nutrient content of an arboretum within the University of Port Harcourt, Nigeria. Data were collected from equal sample plots from the four species' compartments. Tree growth variables including total height, diameter at breast height, crown height, crown diameter and merchantable height were measured for the estimation of above-ground carbon stock. Soil samples were collected from a depth of 0-30 cm from each compartment and analyzed for particle size distribution, organic carbon, total nitrogen, available phosphorus, exchangeable bases, exchangeable acidity, cation exchange capacity, base saturation, pH, Manganese, Iron, Copper and Zinc. Analysis of Variance (ANOVA) was used to test for significant difference (p<0.05) in the carbon contents of the four species and the soil nutrient contents of the different species' compartments. Pearson correlation was used to assess the relationships between the carbon contents, growth parameters and soil parameters. The highest and lowest carbon stock per hectare was observed for G. arborea (151.52 t.ha-1) and K. grandifoliola (45.45 t.ha-1) respectively. Cation exchange capacity and base saturation were highest and lowest for soil under G. arborea and K. grandifoliola respectively. The pH was highest and lowest for soil under G. arborea and T. grandis respectively. Carbon stock correlated positively with dbh, crown diameter, merchantable height and Zn and negatively with base saturation. The study revealed that G. arborea and N. diderrichii can effectively be used for reforestation and afforestation programmes aimed at climate change mitigation across Nigeria. Therefore, policies to encourage and enhance their planting should be encouraged.

Effect of Friction Coefficient from DEM Simulation in Grinding Zone of the Ball Mill (볼 밀의 분쇄장에서 DEM 시뮬레이션을 통한 마찰계수 영향)

  • Jargalsaikhan, Battsetseg;Bor, Amgalan;Uranchimeg, Khulan;Lee, Jehyun;Choi, Heekyu
    • Korean Journal of Materials Research
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    • v.31 no.5
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    • pp.286-295
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    • 2021
  • This study attempts to find optimal conditions of the friction coefficient using a discrete element method (DEM) simulation with various friction coefficient conditions and three different grinding media with various ball sizes in a traditional ball mill (TBM). Using ball motion of the DEM simulation are obtained using the optimal friction coefficient compared with actual motion; photographs are taken by the digital camera and the snapshot images are analyzed. In the simulation, the rotation speed of the mill, the materials and velocity of the grinding media, and the friction coefficient between the balls and the wall of the pot are fixed as the actual experimental conditions. We observe the velocity according to the friction coefficient from the DEM simulation. The friction coefficient is found to increase with the velocity. Milling experiments using a traditional ball mill with the same experimental conditions as those of the DEM simulation are conducted to verify the simulated results. In addition, particle morphology change of copper powder is investigated and analyzed using scanning electron microscopy (SEM) for the milling experiment.

Removal of Anionic Dyes and Heavy Metal Ions Using Silica Nanospheres or Porous Silica Micro-particles Modified with Various Coupling Agents (다양한 커플링제로 표면 개질된 실리카들을 활용한 음이온성 염료 및 중금속의 제거)

  • Sung, Sohyeon;Lee, Minjun;Cho, Young-Sang
    • Korean Chemical Engineering Research
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    • v.59 no.4
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    • pp.596-610
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    • 2021
  • For application in adsorption process, we synthesized silica nanospheres by Stober method, and silica particles with wrinkled surface as well as macroporous silica particles were also fabricated by utilizing emulsion droplet as micro-reactors, followed by modification of the particle surface using suitable coupling agents containing amine groups. These particles exhibited improved adsorption capacity for heavy metal ions and anionic dyes, which were difficult to be removed by conventional silica particles without surface modification. Anionic dye, methyl orange could be removed almost completely by adsorption using porous silica particles modified using APTES. The adsorption efficiency of heavy metal like copper ions was close to 100%, when porous silica was used as adsorbent particles modified with AAPTS.

Hydrogen Production by Methanol Steam Reforming over Micro-channel Reactor (마이크로 채널 반응기에서 메탄올의 수증기 개질반응을 통한 수소 제조)

  • Lee, Jin-Woo;Jeon, Hye-Jeong;Hong, Sung-Chang
    • Clean Technology
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    • v.15 no.2
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    • pp.130-136
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    • 2009
  • Commercial catalyst (Cu-Zn/$Al_2O_3$, Johnson Matthey Co., 83-3 Catalyst) was applied to the hydrogen production by steam reforming of methanol in the micro-channel reactor (MCR). The steam reforming of methanol was tested over Cu-Zn catalyst at temperatures in the range of 200 and 300$^{\circ}C$, the catalyst size of 0.05${\sim}$2.2 mm, the space velocity of 3,000${\sim}$10,000 $hr^{-1}$ in a fixed bed continuous flow reactor. The conversion of methanol and the yield $H_2$ preferred high temperatures and low space velocities, and had optimal results with the particle size of 0.35 mm. Based on the results from experiments with fixed bed reactor, two types of MCR, boat bed and stacked bed MCRs, were studied. The stacked bed type MCR showed better methanol conversion compared with the boat type one.

Mineralogical Characteristics and Fundamental Study of Flotation for Molybdenum Ore (몰리브덴광의 광물학적 특성 및 부선 기초연구)

  • Oyunbileg Purev;Hyun Soo Kim;Chul-Hyun Park
    • Resources Recycling
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    • v.31 no.6
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    • pp.73-80
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    • 2022
  • This study investigated the mineralogical characteristics and basic flotation properties of domestic molybdenum ores. The source mineral of molybdenum was identified as molybdenite, and the main gangue minerals in the raw ore were silicate minerals. Copper, lead, and zinc were also found in trace amounts. Based on the results of basic flotation properties, molybdenite's zeta potential showed negative charges in all pH ranges. The contact angle of molybdenite increased with pH, reaching a maximum of 74° at pH 9. In optimal conditions, the grade and recovery of the concentrate by unit flotation were MoS2 82.4% and 92.04%, respectively. Further investigation of the impurities in the concentrate revealed a sulfide mineral with surface characteristics similar to molybdenite and silicate minerals combined with molybdenite, which may degrade the quality of the concentrate. To improve the concentrate quality, we intend to control silicate minerals through regrinding and liberation and use column flotation to improve fine particle separation efficiency.

Evaluation of Radiation Dose for Dual Energy CBCT Using Multi-Grid Device (에너지 변조 필터를 이용한 이중 에너지 콘빔 CT의 선량 평가)

  • Ju, Eun Bin;Ahn, So Hyun;Cho, Sam Ju;Keum, Ki Chang;Lee, Rena
    • Progress in Medical Physics
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    • v.27 no.1
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    • pp.31-36
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    • 2016
  • The paper discusses radiation dose of dual energy CT on which copper modulation layer, is mounted in order to improve diagnostic performance of the dual energy CT. The radiation dose is estimated using MCNPX and its results are compared with that of the conventional dual energy CT system. CT X-ray spectra of 80 and 120 kVp, which are usually used for thorax, abdominal, head, and neck CT scans, were generated by the SPEC78 code and were used for the source specification 'SDEF' card for MCNPX dose modeling. The copper modulation layer was located 20 cm away from a source covering half of the X-ray window. The radiation dose was measured as changing its thickness from 0.5 to 2.0 mm at intervals of 0.5 mm. Since the MCNPX tally provides only normalized values to a single particle, the dose conversion coefficients of F6 tally for the modulation layer-based dual energy CBCT should be calculated for matching the modeling results into the actual dose. The dose conversion coefficient is $7.2*10^4cGy/output$ that is obtained from dose calibration curve between F6 tally and experimental results in which GAFCHORMIC EBT3 films were exposed by an already known source. Consequently, the dose of the modulation layer-based dual energy cone beam CT is 33~40% less than that of the single energy CT system. On the basis of the results, it is considered that scattered dose produced by the copper modulation layer is very small. It shows that the modulation layer-based dual energy CBCT system can effectively reduce radiation dose, which is the major disadvantage of established dual energy CT.

The Study of Dose Change by Field Effect on Atomic Number of Shielding Materals in 6 MeV Electron Beam (6 MeV 전자선의 차폐물질 원자번호와 조사야 크기에 따른 선량변화 연구)

  • Lee, Seung Hoon;Kwak, Keun Tak;Park, Ju Kyeong;Gim, Yang Soo;Cha, Seok Yong
    • The Journal of Korean Society for Radiation Therapy
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    • v.25 no.2
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    • pp.145-151
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    • 2013
  • Purpose: In this study, we analyzed how the dose change by field size effects on atomic number of shielding materials while using 6 MeV election beam. Materials and Methods: The parallel plate chamber is mounted in $25{\times}25cm^2$ the phantom such that the entrance window of the detector is flush with the phantom surface. phantom was covered laterally with aluminum, copper and lead which thickness have 5% of allowable transmission and then the doses were measured in field size $6{\times}6$, $10{\times}10$ and $20{\times}20cm^2$ respectively. 100 cGy was irradiated using 6 MeV electron beam and SSD (Source Surface Distance) was 100 cm with $10{\times}10cm^2$ field size. To calculate the photon flux, electron flux and Energy deposition produced after pass materals respectively, MCNPX code was used. Results: The results according to the various shielding materials which have 5% of allowable transmission are as in the following. Thickness change rate with field size of $6{\times}6cm^2$ and $20{\times}20cm^2$ that compared to the field size of $10{\times}10cm^2$ found to be +0.06% and -0.06% with aluminum, +0.13% and -0.1% with copper, -1.53% and +1.92% with lead respectively. Compare to the field size $10{\times}10cm^2$, energy deposition for $6{\times}6cm^2$ and $20{\times}20cm^2$ had -4.3% and +4.85% respectively without shielding material. With aluminum it had -0.87% and +6.93% respectively and with lead it had -4.16% and +5.57% respectively. When it comes to photon flux with $6{\times}6cm^2$ and $20{\times}20cm^2$ of field sizes the chance -8.95% and +15.92% without shielding material respectively, with aluminum the number -15.56% and +16.06% respectively and with copper the chance -12.27% and +15.53% respectively, with lead the number +12.36% and -19.81% respectively. In case of electron flux in the same condition, the number -3.92% and +4.55% respectively without shielding material respectively, with aluminum the number +0.59% and +6.87% respectively, with copper the number -1.59% and +3.86% respectively, with lead the chance -5.15% and +4.00% respectively. Conclusion: In this study, we found that the required thickness of the shielding materials got thinner with low atomic number substance as the irradiation field is increasing. On the other hand, with high atomic number substance the required thickness had increased. In addition, bremsstrahlung radiation have an influence on low atomic number materials and high atomic number materials are effected by scattered electrons.

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