• Title/Summary/Keyword: Continuous Extraction

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디젤오염토양복원을 위한 고온공기 주입/추출 공정의 토양 파일 공법에의 적용 연구

  • 박민호;박기호;홍승모;고석오
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2004.09a
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    • pp.63-67
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    • 2004
  • A field pilot study on remediation of diesel-contaminated soil by hot air injection/extraction process constructing soil piling system was conducted to evaluate the effects of hot air on the removal of diesel and each constituent. After the heating process of 2 months, the equilibrium temperature of soil reached to 10$0^{\circ}C$ and soil TPH concentration was reduced to about 72% against the initial concentration. Additional extraction process of 2 months induced the continuous extraction of residual diesel and the increment of microbial activity, which made soil TPH concentration reduced to 95%. In addition biological removal of non volatile constituents in diesel was verified indirectly and the removal pattern of each DRO(diesel range organic) as soil temperature was explained.

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Vertical Stripes Extraction By Using The Gabor Filter for 3D Face Acquisition (3차원 얼굴정보 획득을 위한 가버필터를 이용한 세로줄무늬 패턴 추출)

  • 김인범;김재희
    • Proceedings of the IEEK Conference
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    • 2002.06d
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    • pp.133-136
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    • 2002
  • In this paper, we propose a method to extract vertical stripes projected on human face using Gabor filter, Previous work cannot extract continuous vertical stripes in the eye and mouth region due to their horizontal lines, Proposed method use Gator filter adaptively according to main frequencies and directions of stripes in each block. Experimental results show that Proposed method can extract continuous vertical stripes in the eye and mouth region

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Studies on the Formation of Copper Complexes of Sulfa-Drug II.Study on Chemical Constisuent of Copper Sulfa-Drug Complex by Continuous Variation Method. (Sulfa제-Cu착화합물의 형성에 관하여 II Spectrophotometry 에 의한 Copper Sulfa-Drug Complex 의 화학조성결정)

  • 이왕규
    • YAKHAK HOEJI
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    • v.8 no.4
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    • pp.96-99
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    • 1964
  • In the previous study, the composition ratios of the Cu-sulfa drugs complexes determined by gravimetric and solvent extraction method reported. In this paper, the continuous variations method has been used to know whether the complexes are simple complexes or chelates, and to recertify the composition ratios of the complexes at pH 7-8. It has been certified that the ratio of $Cu^{+2}$ ion to sulfa drugs in 1:2 from the result of this experiment.

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Continuous methanol synthesis directly from methane and steam over Cu(II)-exchanged mordenite

  • Lee, Sae Ha;Kang, Jong Kyu;Park, Eun Duck
    • Korean Journal of Chemical Engineering
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    • v.35 no.11
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    • pp.2145-2149
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    • 2018
  • The formation of methanol directly from methane and steam was observed over Cu ion-exchanged mordenite. Furthermore, the continuous production of methanol was achieved by co-feeding methane and steam over Cumordenite. The methanol production rate was comparable to that reported in the stepwise process in which activation, methane reaction, and extraction of methanol were carried out separately.

Solvent Extraction for the Recovery of Copper from Hydrochloric Etching Solutions by Alamine336 (염산에칭폐액으로부터 Alamine336에 의한 구리의 용매추출에 관한 연구)

  • 안재우;염재웅
    • Resources Recycling
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    • v.6 no.3
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    • pp.9-14
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    • 1997
  • A study has been made of the rccovery of copper (11) by solvent extraction with Alamine336 (Tri-n-oclylamine) as a extractant from hydrochloric etching solutions. The effect of extractant concentrations, hydrochloric acid, chloride Ion concentrations and phase ratio (organiclaqueaus) on copper extraction were studied. Experimental results showed that the concenl~atiano f extractant and the phase ratio strongly influenced the copper extraction, and the extraction percent of capper Increased at higher hydrochloric acid and chloride ion mncmhation. We proposed that the optimum extrachon stages of copper for continuous extraction process by analysidng thc McCabe-Thielc diagram. Stripping of copper from the loaded organic phases wn be accomplished by pure water (H, O) as a dripping reagent effectively. As the tcmpcrature is increased, thc stripping of copper is enhanced.

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Solidification Analysis for Evaluation of Cooling Pattern in Bloom Type Continuous Caster (Bloom type 연주기의 냉각패턴 평가를 위한 응고해석)

  • 정영진;김영모;조기현;강충길
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2003.10a
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    • pp.51-54
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    • 2003
  • The continuous casting is primarily a heat-extraction process in which the heat transfer at various cooling zones profoundly influences quality of products. So development of numerical model is necessarily needed for more specific and clear investigations upon heat transfer mechanism at mold and secondary cooling zones. In this study, heat transfer coefficients which shows the characteristic of heat transfer mechanism in mold are calculated for more exact analysis with temperatures measured in bloom mold using optimal algorithm, and finally the validity of cooling conditions at secondary cooling zone which is actually used at field for 30 Ton bloom type continuous casting of 0.187%C is investigated. From the results of solidification analysis, the characteristic of bloom mold shows good agreements with that of previously studies by other authors and optimized cooling conditions for 0.187%C are presented.

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Solidification Simulation for Optimal Cooling of Bloom Type Continuous Casting Machine (Bloom 연주기의 최적 냉각조건 도출을 위한 응고 시뮬레이션)

  • Jung, Young-Jin;Kim, Young-Mo;Cho, Kee-Hyeon;Kang, Chung-Gil
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.28 no.11
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    • pp.1629-1636
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    • 2004
  • The continuous casting is primarily a heat-extraction process in which the heat transfer at various cooling zones profoundly influences quality of products. So development of numerical model is necessarily needed for more specific and clear investigations upon heat transfer mechanism at mold and secondary cooling zones. In this study, heat transfer coefficients which show the characteristic of heat transfer mechanism in mold are calculated for more exact analysis with temperature measured in bloom mold using optimal algorithm, and finally the validity of cooling conditions at secondary cooling zone actually used at field fur 30 Ton bloom type continuous casting of 0.187%C is investigated. From the results of solidification analysis, the characteristic of bloom mold shows a similar tendency with that of previous studies, and optimized cooling conditions for 0.187%C are presented.

Separation of Nitric Acid and Gold from Gold Bearing Aqua Regia Solution by Solvent Extraction with TBP(tributyl phosphate) (금이 함유된 왕수용액으로부터 TBP(tributyl phosphate) 용매추출에 의한 질산과 금의 분리)

  • Bae, Mooki;Srivastava, Rajiv R.;Kim, Sookyung;Lee, Jae-chun
    • Resources Recycling
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    • v.26 no.1
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    • pp.51-58
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    • 2017
  • The present study to develop a process for extracting nitric acid and gold from aqua regia leach solution using TBP(tributyl phosphate) was conducted. The pure aqua regia was used to investigate the extractive behavior of nitric acid depending on the concentration of extractant, concentration ratio of nitric and hydrochloric acid. The extraction rate of nitric acid and gold from the gold bearing aqua regia was also examined. The theoretical extraction number was verified by counter current using the number of operations and the phase ratio obtained from McCabe-Thiele diagram. Stripping experiments were carried out for continuous recovery of nitric acid and gold in loaded organic. Considering the effect of extraction acid and gold, the simulation showed that greater than 99.9% extraction of $103.0mg{\cdot}L^{-1}$ gold and 98.0% of $151.2g{\cdot}L^{-1}$ nitric acid could be attained in a two and three-stage counter-current extraction at an O/A phase ratio of 1:0.85. Distilled water and sodium thiosulfate were used as the nitric acid and gold stripping solution. The stripping rates were 99.5% and 92.0%, respectively. The study revealed that the recovery of nitric acid and gold from gold bearing aqua regia was a plausible approach through simultaneous extraction and continuous stripping of nitric acid and gold.

Optimum Extraction Methods of Volatile Compounds in Beef Extract Powder (쇠고기 엑기스 분말 휘발성 성분의 최적 추출방법에 관한 연구)

  • Kim Hun;Cho Woo-Jin;Jeong Eun-Jeong;Ahn Jun-Suck;Lim Chi-Won;Yoo Young-Jae;Kim Kwang-Ho;Cha Yong-Jun
    • The Korean Journal of Food And Nutrition
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    • v.17 no.4
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    • pp.412-419
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    • 2004
  • In odor to select optimum extraction methods of volatile compounds in beef extract powder(BEP) as basic data for the development of a new detection method of irradiated BEP, four extraction methods, such as solid phase microextraction with polar fiber(S-PD) and non-polar fiber(S-CD), purge and trap(P&T) and liquid liquid continuous extraction(LLCE) methods, were tested with gas chromatography/mass spectrometry method. A total of 106 volatile compounds including 22 hydrocarbons, 7 aldehydes, 6 ketones, 13 alcohols, 6 sulfur-containing compounds, 19 nitrogen-containing compounds, 6 aromatic compounds, 17 terpenes, 8 furans and 2 miscellaneous compounds were detected in BEP by four detection methods. The most compounds(62 compounds) were detected by S-PD method, followed by P&T(43), LLCE(38) and S-CD method(30). Among these methods, S-PD and P&T methods showed a complementary interrelationship to detect volatile compounds as S-PD method showed high detectabiltiy to all compound groups except hydrocarbons and ketones, which had high volatility and low molecular weight(less than RI 1200), but P&T method showed the contrary pattern to that of S-PD method. Moreover, the most of volatile compounds detected by S-CD and LLCE methods were also detectable by S-PD or/and P&T methods. Therefore, the simultaneous application of S-PD and P&T methods were selected as the optimum volatile extraction methods of BEP.

Extraction and Identification of Volatile Isothiocyanates from Wasabi using Supercritical Carbon Dioxide (초임계 이산화탄소를 이용한 고추냉이로부터 휘발성 Isothiocyanates류 추출 및 동정)

  • Kim, Sung-Jin;Lee, Min-Kyung;Back, Sung-Sin;Chun, Byung-Soo
    • KSBB Journal
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    • v.22 no.3
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    • pp.174-178
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    • 2007
  • The aim of this study was to identifyisothiocyanates (ITCs) from wasabi (Wasabi japonica Matsum) using supercritical carbon dioxide ($SCO_2$) and to compare the composition in the extracts between $SCO_2$ and organic solvents extraction. A semi-continuous high pressure apparatus was used to extract wasabi (roots, stems and leaves) at following conditions pressure 80$\sim$120 bar, temperature $40\sim50^{\circ}C$. Ether, ethanol, chloroform and dichloromethane were used as organic solvents. The ITCs extracted by means of both separation technologies were analyzed by a gas chromatography system. As the results of study, AITC and ITCs were highly extracted at 40$^{\circ}C$ and 80 bar. To extract AITC from wasabi, $SCO_2$ extraction is more effective than organic solvents extraction, resulted in thermal degeneration and remaining of organic solvents.