• Title/Summary/Keyword: Compound Surface

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A Study on the kinetics of Aluminizing of Cold rolled Steel Sheets (冷間壓廷鋼板의 Aluminizing에 對한 速度論的인 硏究)

  • Yoon, Byung-Ha;Kim, Young-Ki
    • Journal of the Korean institute of surface engineering
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    • v.12 no.2
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    • pp.75-83
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    • 1979
  • The Rates of formation and heats of activation for the intermatallic Compound Layers between Cold rolled sheet and molten aluminium &ath (adding small amounts of silicon) has been determined by Continous aluminizing method in the temperature range of 680$^{\circ}$ to 760$^{\circ}C$ and with immerssion time. The structure of the intermetallic Compound Layers was the shape of "Tongues" in pure Al-Bath and Al-Bath Containing 1% Si, But in Al-5% Si Bath was "Band" the Composition of the intermetallic Compound Layers were checked by microhardness measurements and X-Ray probe micro analyzer. FeAl intermetallic Compound layer was found to be uniform in pure Al-Bath and Al-5% Si Bath, But Fe Al intermetallic Compound Layer was shown in Al-1% Si Bath. The growth Rates of the intermetallic Compound Layers was most rapidly increased at Temperatures from 720$^{\circ}$ to 760$^{\circ}C$, at the immorsion time above 60 Second in pure Al-Bath, But in Al-1% Si Bath was solwly increased for the same conditions, and then in Al-5% Si Bath was hardly effected by these experimental condition. Heasts of activation of 29, 46 Kcal per mole which calculuted from Layer growth experiments were found in pure Al-Bath, Al-1% Si Bath respectively.

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Effects of Iron, Silicon and Zinc Contained in Molten Aluminum on Aluminizing of Cast Iron (주철 소지상에 용융알루미늄 도금시 철 규소 및 아연의 영향)

  • Choi, Chong-Sool;Moon, Sung-Wuck
    • Journal of the Korean institute of surface engineering
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    • v.20 no.4
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    • pp.144-153
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    • 1987
  • In the case of dipping the Ni-Resist cast iron into molten aluminum with iron content, the thickness of intermetallic compound was remarkably increased with increasing iron content. The thickness was shown by following equation in the range of 1-3% iron content; $x=22.5t^{1/2}+4.47{\cdot}t{\cdot}(Fe%)$. where, x is thickness(${\mu}m$), t the time (minute), Fe% the iron w/o. When the Ni-Resist cast iron was dipped into the molten aluminum containing zinc content, the intermetallic compound thickness was also increased with increasing zinc contents. And thickness was represented by the following equation in the range of 2-10% zinc content; $x=3.46t^{1/2}+0.27{\cdot}t{\cdot}(Zn%)$. However, in the case of dipping the Ni-resist cast iron into molten aluminum with silicon content, the thickness of intermetallic compound was decreased with increasing silicon content, as shown in the following equation; $x=7.17t^{1/2}-0.15{\cdot}t{\cdot}(Si%)$. The intermetallic compound formed onto Ni-Resist cast iron was identified to be $FeAl_3\;and\;Fe_3Al$. As the result of hardness measurement, the peak hardness appeared in the intermetallic compound at near interface of the cast iron and the compound.

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A Study on Mechanical and Electrical Properties at Interfaces Between Epoxy and ifs Molded Metal (에폭시 매입금구 표면거칠기에 따른 전기적, 기계적 특성 연구)

  • 김수연;하영길;이성진;김영성;박완기;김성진
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.05a
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    • pp.226-229
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    • 1999
  • Epoxy compound has been used as insulation material in electrical equipment for a long time because of its excellent electrical, mechanical and chemical properties. Nowdays, becoming higher voltage system, the properties of interface between epoxy and metal insert become more important. The breakdown voltage of epoxy compound for electric material is variable according to the surface roughness of metal insert. Generally, with metal insert sanding, the adhesion strength is enhanced and the breakdown strength is reduced. But in this study, we knew that the adhesion strength became enhanced but the breakdown strength didn\`t reduced with metal insert sanding. So in this study sanding. So in this study, we suggest the optimum interface condition by adjusting the surface roughness.

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Study on the preparation of electrochemical exfoliated graphene/Fe oxide compound according to synthetic conditions (합성 조건 변화에 따른 전기화학적 박리 그래핀/철 산화물 복합체 제조 연구)

  • Park, Eunjin;Kim, Yong-Tae;Choi, Jinsub
    • Journal of the Korean institute of surface engineering
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    • v.55 no.2
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    • pp.84-90
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    • 2022
  • With the growing interest in energy storage and conversion systems including secondary batteries, capacitors, and water electrolysis, various electrode materials are being developed to improve the energy efficiency. Among them, graphene is regarded as one of the promising candidates owing to its exceptional properties - large surface area, and excellent electrical conductivity. Herein, we report a facile one-step electrochemical approach to synthesize exfoliated graphene/Fe oxide compound. The effect of experimental conditions - the types of applied voltage, kinds of counter electrodes, acidity of electrolyte on the synthesis of graphene/Fe oxide compound is investigated.

CHARACTERIZATION AND ANALYSIS OF SHEAR TEST WITH TESTING CONDITIONS ON BGA PACKAGE

  • Koo, Ja-Myeong;Kim, Dae-Up;Jung, Seung-Boo
    • Proceedings of the KWS Conference
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    • 2002.10a
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    • pp.463-468
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    • 2002
  • This study investigates the variations of shear force, displacement, and fracture surface with the shear speed and the number of reflows. The experimental data of shear tests indicate that the shear force increases as increasing the number of reflows and the shear speed due to the formation of a kind of intermetallic compound, Ni$_3$Sn$_4$, on Au/Ni/Cu pad, and the work-hardening. However, general trends show that the shear force decreases due to increasing the thickness of the intermetallic compound over 4x reflow. It is observed that the intermetallic compound which is formed between solder and pad increases according to increasing the number of reflows, and the growth rate of the intermetallic compound at central region on the interface is faster than one at edge part. The general tendencies of shear force and displacement with different shear speeds are almost identical as an increase of the number of reflows.

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Angle-sensitive Pixels Based on Subwavelength Compound Gratings

  • Meng, Yunlong;Hu, Xuemei;Yang, Cheng;Shen, Xinyu;Cao, Xueyun;Lin, Lankun;Yan, Feng;Yue, Tao
    • Current Optics and Photonics
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    • v.6 no.4
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    • pp.359-366
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    • 2022
  • In this paper, we present a new design for angle-sensitive pixels (ASPs). The proposed ASPs take advantage of subwavelength compound gratings to capture the light angle, which enables pixel size to reach the wavelength scale of 0.7 ㎛ × 0.7 ㎛. The subwavelength compound gratings are implemented by the wires of the readout circuit inherent to the standard complementary metal-oxide-semiconductor manufacturing process, thus avoiding additional off-chip optics or post-processing. This technique allows the use of two pixels for horizontal or vertical angle detection, and can determine the light's angle in the range from -45° to +45°. The proposed sensor enables surface-profile reconstruction of microscale samples using a lensless imaging system.

A Study on the Tool Interference Detection and Tool Path Correction in Compound Surface Machining (복합곡면 가공시 공구간섭의 탐지와 공구경로 수정에 관한 연구)

  • 조명우
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.8 no.6
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    • pp.105-112
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    • 1999
  • In this paper we deal with tool interference problem in the case of compound surface machining. A new tool interference detection and correction method based on the envelope of the tool path is suggested to identify and correct the tool interference - not only within the local path of tool movement, but also outside of the tool path. Therefore, the developed strategy can be used to check the possible interference in any region of the surface. In order to analyze quantitatively the milled surface error produced by the tool interference, improved surface prediction model is also suggested in cutting process by general cutters. The effectiveness of the proposed method is demonstrated through simulation study.

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A Study on the Microstructures and Properties of Sulfnitrided SCM440 Steel by Micro-pulse Plasma (SCM440강에 형성된 플라즈마 침류질화층의 조직과 특성에 관한 연구)

  • 이재식
    • Journal of the Korean institute of surface engineering
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    • v.31 no.5
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    • pp.266-277
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    • 1998
  • The effects of $H_2S$ gas ratio, temperature and time on the case depth, hardness, and sulfide and nitride formation on the surface of sulfnitrided SCM440 steel have been studied by micro-pulse plasma technique. The thickness of compound layer of sulfide and nitride increased with the increase of time, temperautre and $H_2S$ gas ratio. But surface hardness decreased with the increase of soft sulfide layer because the hard nitride layer formed beneath the sulfide. The thickness of sulfide layer was about 10$\mu\textrm{m}$ abpve 0.0088% of $H_2S$ gas. The highest surface hardness of the compound layer was Hv835 at $530^{\circ}C$, 1hr and 0.06% of $H_2S$ gas. X-ray diffraction indicated that the surface products were $Fe_{1_x}S$, $Fe_{2.5}N$ and $Fe_4N$. It was confirmed by EPMA that sulfide only existed in the surface.

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Moisture-Related Properties of PET Fabrics treated with Quaternary Ammonium Compound/Alkaline Solution (사급(四級) 암모늄 화합물(化合物)과 알칼리 혼합액(混合液)으로 처리(處理)된 PET직물(織物)의 수분특성(水分特性) 연구(硏究))

  • Kim, Do-Hee;Jeon, Dong-Won;Kim, Jong-Jun
    • Journal of Fashion Business
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    • v.7 no.2
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    • pp.69-81
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    • 2003
  • Among the various properties of textile fabrics, the moisture-related properties are important for the textile processes or the apparel comfort characteristics. Alkaline hydrolysis results in pitting on the surface of fibers and increases the amount of hydroxyl and carboxyl end groups of the PET molecules on the fiber surface. The purpose of this study is to investigate the moisture-related properties of PET fabrics treated with quaternary ammonium compound/alkaline solution. The wetting and wicking properties of the PET fabrics were measured using the following experiments: contact angle, surface free energy, work of adhesion, vertical wicking height, moisture regain, and frictional static voltage. It was concluded that by the alkaline hydrolysis process, surface hydrophilicity and reactivity were considerably improved especially at lower levels of weight loss% and that the pitting of the fiber surface resulted in at higher levels of weight loss% was disadvantageous in moisture-related properties of PET.

Synthesis and Surface Relief Gratings of Three-Armed Star-Shaped Molecules Bearing 4-(N,N-Diphenyl)Amino-4'-Nitroazobenzene Chromophores

  • Lee, Jung-Eun;Jung, Kyung-Moon;Cho, Min-Ju;Kim, Kyung-Hwan;Choi, Dong-Hoon
    • Macromolecular Research
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    • v.16 no.5
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    • pp.434-440
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    • 2008
  • Three-armed, star-shaped molecules containing 4-(N,N-diphenyl)amino-4'-nitroazobenzene chromophores were synthesized to study the diffraction behavior after inscribing surface relief gratings. The two molecules differed in terms of their mode of chromophore attachment to the core. In compound 5, they were bound to the core laterally through alkylene spacers, whereas the chromophores were tethered perpendicularly to the core in compound 4. Although 60 wt% of the polar azobenzene chromophores was comprised of large molecules, no aggregation behavior was observed in the absorption spectra of the thin films. The surface relief gratings were elaborated on the surface of the molecular films by the two-beam interference method. The dynamics of grating formation were studied in terms of the diffraction efficiency using two different film samples made up of two star-shaped molecules. The maximum diffraction efficiency of D-$(ENAZ)_3$, compound 4, was measured to be about 30%, which was significantly high. The mode of chromophore attachment affected the dynamic properties of the diffraction gratings.