• Title/Summary/Keyword: Compound Pattern

Search Result 264, Processing Time 0.024 seconds

Content Comparative Analysis and Classification for Piniellia ternate, P. pedatisecta and Typhonium flagelliforme by HPLC-PDA analysis (HPLC-PDA를 이용한 반하, 호장남성, 수반하의 분류 및 함량분석)

  • Jo, Ji Eun;Lee, A Yeong;Kim, Hyo Seon;Moon, Byeong Cheol;Choi, Goya;Ji, Yunui;Kim, Ho Kyoung
    • The Korea Journal of Herbology
    • /
    • v.28 no.5
    • /
    • pp.95-101
    • /
    • 2013
  • Objectives : A quantitative method using high performance liquid chromatography with a photodiode array detector(HPLC-PDA) was established for the quantitative analysis of the four main compound and pattern analysis to classification Piiellia ternate, P. pedatisecta and Typhonium flagelliforme. Methods : The analytical procedure for the determination of P. ternata, together with the known main compounds uracil, uridine, guanosine and adenosine was established. Optimum HPLC-PDA separation of these P. ternata was possible on Luna C18(2) column material, using water and acetonitrile as mobile phase. The method was validated according to regulatory guidelines. In addition, this assay method were analyzed for the content of four main compound in P. ternata, P. pedatisecta and T. flagelliforme and by data obtained from the HPLC-PDA analysis was performed principal component analysis(PCA). Results : Validation results indicated that the HPLC method is well suited for the determination of the roots of P. ternata with a good linearity ($r^2$ > 0.999), precision and recovery rates. Analysis of HPLC-PDA, the average content of uracil, uridine, guanosine and adenosine was significantly higher in P. ternate>P. pedatisecta> T. flagelliforme order. The application of PCA to main compound data by HPLC-PDA permitted the effective discrimination among the three species. Conclusions : Analysis of both HPLC-PDA and PCA confirmed the fact that four main compound and pattern profiles of P. ternata, P. pedatisecta and T. flagelliforme were different from each other.

A Study on Iron Compounds Accompanied in Korean Kaolin Minerals (국산 Kaolin 광물에 수반된 철화합물의 종류 및 존재상태 구명에 관한 연구)

  • 박금철;최석진;박영갑
    • Journal of the Korean Ceramic Society
    • /
    • v.11 no.2
    • /
    • pp.22-30
    • /
    • 1974
  • This study was carried out to investigate the species of iron compounds in kaolin mineral and the bonding relation between the major kaolin and its subordinate iron compound existing as incidental mineral in common clay by means of chemical composition, X-ray diffraction, thermal differential and thermogravimetrie analysis for the application of clays in the field of ceramic raw material. The domestic clay are produced abounduntly in many places, but San-Cheong kaolin, Chu-An clay, and Yeong-Am clay were selected as samples in this experiment because of their frequent utilization in porcelain industry. Two kinds of samples with low and high iron content are picked up respectively from the place of production and elutriated under two micron size to determine the properties and concentration of iron compound very fine particles or colloidal substance of low crystalline grade. Therefore, hydrothermal treatment in autoclave was conducted considering the existence of low crystalline grade of iron compounds known as an amorphoue state in X-ray diffraction pattern furthermore, de-iron treatment of hydrothermal compound was done in order to identify the related iron compound before and after hydrothermal reaction and iron compound which is one of the samples was synthesized for the determination of their compounds state in more detail. The obtained results in this study are as follows: In San-Cheong kaolin, Chu-An clay and Yeong-Am clay 1) It is proved that species accompanying iron compound is $\alpha$-FeOOH form. 2) Iron compound is composed of very fine particles or colloidal substance. 3) The iron substance encircles the fine parts of clay minerals under 2 micron and acts as cementizing agent.

  • PDF

Constituents of Paulownia tomentosa Stem(III): The Crystal Structure of Methyl 5-Hydroxy-dinaphtho[1,2-2',3]furan-7,12-dione-6-carboxylate

  • Park, Il-Yeong;Kim, Bak-Kwang;Kim, Yang-Bae
    • Archives of Pharmacal Research
    • /
    • v.15 no.1
    • /
    • pp.52-57
    • /
    • 1992
  • The molecular structure of a natural compound was determined by single crystal X-ray diffraction analysis. The compound was isolated by methanol extraction and repeated chromatography from the stem of Paulownia tomentosa. Yellow prismatic crystals of the compound, which were recrystallized from tetrahydrofuran, are triclinic, with a = 7.310 (6), b = 10.753(6), c = 11.586(5) ${\AA}.\;\alpha= 93.30(6),\;\beta=105.62(10),\;\gamma=109.49(7)^\circ,\;D_x=1.514,\;D_m=1.51 g/cm^3$, space group P1 and Z = 2. The structure was solved by direct method, and refined by least-squares procedure to the final R-value of 0.032 for 1271 independent reflections $(F\le3\sigma{(F))}$. The compound is one of new furanquinone analogue. The molecule has a nearly planar conformation with an intramolecular hydrogen bond. In the crystal, the planar molecules are arranged as a prallel sheet-like pattern, and these stackings are stabilized by the O-H...O type intermolecular hydrogen bonds. The other intermolecular contacts appear to be the normal van der Waals interactions.

  • PDF

The Effect of N-Substituted Alkyl Groups on the Anticonvulsant Activities of N-Cbz-${\alpha}$-amino-N-alkylsuccinimides

  • Lee, Jae-Won;Son, Ki-Chun;Jung, Kyung-Im;Choi, Jong-Won;Park, Min-Soo
    • Archives of Pharmacal Research
    • /
    • v.20 no.1
    • /
    • pp.53-57
    • /
    • 1997
  • For the purpose of defining the effects of the N-substituted alkyl groups on the anticonvulsant activities of N-Cbz-.alpha.-aminosuccinimides, various (R)- and (S)-N-alkyl substituted N-Cbz-.alpha.-aminosuccinimides (1 and 2) were prepared from the corresponding (R)- and (S)-N-Cbz-aspartic acid by using known reaction and were evaluated the anticonvulsant activies in the MES and PTZ tests, including their neurotoxicities. The most active compound in the MES test was (R)N-Cbz-.alpha.-amino-N-methylsuccinimide (1b) $(ED_{50}=52.5 mg/kg, Pl=3.2)$. And in case of the PTZ test, (R)-N-Cbz-.alpha.-amino-N-ethylsuccinimide (1c) was the most active compound $(ED_{50}/=32.5mg/kg, Pl=3.1)$. The order of anticonvulsant activities of these compounds against the MES test, as judged from the ED_50values for the R series (1), was N-methyl > N-isobutyl > non-substituted > N-ethyl, N-allyl > N-benzyl compound; for the S series (2) N-methyl > N-altyl > non-substituted > N-isobutyl > N-ethyl > N-benzyl compound. The anticonvulsant activities in the PTZ tests of these compounds exhibited somewhat different pattern ; for the R series (1) Nethyl > N-methyl > N-isobutyl> non-substituted > N-allyl > N-benzyl compound in order of decreasing activity; for S series (2) N-ethyl > N-allyl, non-substituted > N-isobutyl > N-methyl > N-benzyl compound in order of decreasing activity.

  • PDF

A study on the design wax up technique for mandibular molar occlusion surface (하악구치 교합면의 design 조각법에 관한 연구)

  • Moon, Hee-Kyung
    • Journal of Technologic Dentistry
    • /
    • v.24 no.1
    • /
    • pp.107-126
    • /
    • 2002
  • The first function of occlusion is mastication. Therefore the functional restoration of occlusal surface is very important. The restoration of occlusal surface is three method as wax bite technique, F.G.P. technique, cone technique. Many dental technician is using compound method. I am using compound method of wax bite technique and cone technique. I have knew common point on each teeth during I have waxing up wax pattern. So I studied on the design waxup technique for mandible molar occlusion. The results of the study were as follows; 1. The dam wax up method can restore axial contour of teeth very easy and make short working time of wax pattern. 2. The height of dam must be same with cusp of adjacent teeth. 3. Automatically the contour of tooth is appeared if the contour of dam is relationship with cuspid line of adjacent teeth. 4. The height of contour of buccal, lingual surface is formed natural curve to add fluid wax by gravitation. 5. The development groove of mandible first premolar is appeared V form. 6. The development groove of mandible second premolar is appeared Y form. 7, The development groove of mandible first molar is appeared M form. 8. The development groove of mandible second molar is W form. 9. The embrasure is formed to carve around contact point area as round convex. It affects to axial form of tooth. 10. The buccal, lingual groove of molar is formed parallel with direction of teeth arrangement.

  • PDF

Analysis of the Motifs on Traditional Cultural Goods in Seoul and Kwang-Ju (전통 문화상품에 나타난 문양 분석 - 서울 지역과 광주 지역을 중심으로 -)

  • Choi, Seung-Youn;Lee, Mi-Sook;Shin, Youn-Sook
    • Journal of the Korean Home Economics Association
    • /
    • v.44 no.1 s.215
    • /
    • pp.101-113
    • /
    • 2006
  • The purpose of this study was to investigate and compare the characteristics of the motifs on cultural goods in In-Sa-Dong Street, Seoul, with those in Art Street, City Hall, Kwang-ju. For this study, 607 cultural goods were collected from the two cities: 265 in Seoul and 342 in Kwang-ju. Total cultural goods were classified by accessories, decoration pieces, stationery and ceramics and were studied by repetition patterns, motifs types, representative techniques, and representative types. The results were as follows. First, for repetition patterns of motifs, there were 219 simple repetition patterns in Seoul, and 289 in Kwang-ju, and 46 compound repetition patterns in Seoul, and 53 in Kwang-ju. The ratio of simple repetition pattern was higher than that of compound repetition pattern in both cities. Second, for motif types, floral, animal, letter, and graphic motifs were used far more frequently than any other motif types. Third, for representative techniques, embroidery was far more frequently used than any other representative techniques. Metallic crafts, chil-bo and paper techniques were also favored. Fourth, for representative types, realistic types were more common than abstract types.

TOLERANT FUZZY PATTERN MATCHING : AN INTRODUCTION

  • DUBOIS, DIDIER;PRADE, HENRI
    • Journal of the Korean Institute of Intelligent Systems
    • /
    • v.3 no.2
    • /
    • pp.3-17
    • /
    • 1993
  • The fuzzy pattern matching technique has been developed in the framework of fuzzy set and possibility theory in order to take into account the imprecision and the uncertainty pervading values which have to be compared to requirements (which may be fuzzy) in a pattern matching process. This paper restates the basic principles and extends them to situations where (sub)patterns are only required to be satisfied up to a given tolerance (which may be fuzzy), or where the different subparts of a compound pattern may have various levels of importance. Both cases correspond to a weakening of elementary patterns. which can be expressed by a fuzzy relations modelling an approximate equality or an uncertain strict equality respectively. We also study the more sophisticated case where some elementary patterns have not to be satisfied with the highest priority provided that weaker requirements remain satisfied. The fuzzy pattern matching technique applies in a variety of problems including the evaluation of soft queries with respect to a fuzzy database, the evaluation of the fuzzy condition parts of rules in approximate reasoning, or the evaluation of the belonging of an ill-known object to a flexible class in classification problems.

  • PDF

Design of Compound Knowledge Repository for Recommendation System (추천시스템을 위한 복합지식저장소 설계)

  • Han, Jung-Soo;Kim, Gui-Jung
    • Journal of Digital Convergence
    • /
    • v.10 no.11
    • /
    • pp.427-432
    • /
    • 2012
  • The article herein suggested a compound repository and a descriptive method to develop a compound knowledge process. A data target saved in a compound knowledge repository suggested in this article includes all compound knowledge meta data and digital resources, which can be divided into the three following factors according to the purpose: user roles, functional elements, and service ranges. The three factors are basic components to describe abstract models of repository. In this article, meta data of compound knowledge are defined by being classified into the two factors. A component stands for the property about a main agent, activity unit or resource that use and create knowledge, and a context presents the context in which knowledge object are included. An agent of the compound knowledge process performs classification, registration, and pattern information management of composite knowledge, and serves as data flow and processing between compound knowledge repository and user. The agent of the compound knowledge process consists of the following functions: warning to inform data search and extraction, data collection and output for data exchange in an distributed environment, storage and registration for data, request and transmission to call for physical material wanted after search of meta data. In this article, the construction of a compound knowledge repository for recommendation system to be developed can serve a role to enhance learning productivity through real-time visualization of timely knowledge by presenting well-put various contents to users in the field of industry to occur work and learning at the same time.

The empirical Analysis of compound woven silk fabrics of Cho-Sun Dynasty - focusing of 26 pieces of the fabrics which are in the Tong-Do Temple′s collection - (조선시대 중조직 견직물에 대한 실증적 고찰 -통도사 소장직물 26점을 중심으로-)

  • 장현주;권영숙
    • Journal of the Korean Society of Costume
    • /
    • v.50 no.8
    • /
    • pp.5-16
    • /
    • 2000
  • This study attempts to examine compound weave among silk fabrics of Cho-Sun Dynasty. These silk fabrics have colorful patterns. They can be classified into two types by their texture structure one is called polychrome woven silk of which structure is plain or twill fabric : another is called satan damask of which structure is stain fabric. Their texture structure consist of warp and weft. In addition. there are other types of warp and weft for pattern structure ; various twill structures were used for patterns. A variety of colorful threads, including gold and silver ones. are used fur patterns in them. The brocaded-type fabric was primarily developed during Won Era of China. It was most developed in Ko-Rye Kingdom. During that era flat strip was used the most but its length was usually not long enough to finish one pattern. However, wrapped thread was increasingly used during the middle and later period of Cho-Sun Dynasty due to the development of weaving technology for gold thread. The brocaded-type fabric was produced in Korea and it was also Imported from China according to some record. There are some domestic empirical documents that show the names of imported Satin Samite, Brocaded satin and these are good evidence to prove the nationwide use of the cloth during Cho-Sun Dynasty. The density ratio of warp and weft is almost same except Samite in the third and Satin with flower motif in the second period is most density among them. C·F of Brocaded satin with Mang motif in the third period values the highest price. Brocaded satin, used with both gold and silver threads, is thickest.

  • PDF

Relationship of Follow-through Movements to Target Accuracy in Compound Archers (컴파운드 양궁의 팔로우 스루 동작과 사격 정확도의 상관관계)

  • Junkyung Song;Kitae Kim
    • Korean Journal of Applied Biomechanics
    • /
    • v.34 no.1
    • /
    • pp.34-44
    • /
    • 2024
  • Objective: This study aimed to investigate how the movements occurring during the follow-through phase after releasing an arrow among elite compound archers, are associated with the arrow impact points on the target. Method: Nine elite archers performed consecutive compound archery shooting under conditions identical to actual competitions using their own bows and equipment. Motion capture system and force platform were utilized to record the changes in joint positions and center of pressure, respectively. Principal component analysis was employed to identify the patterns in which multidimensional joint positions and COP changes were organized with horizontal and vertical coordinates of arrow impact points. Subsequently, correlation analysis quantified the relationship between individual variables and the coordinates of arrow impacts on the target. Results: We found a common organizational pattern in which the two axes of the impact point coordinates were grouped into the first two principal components. The movements of the upper and lower limbs following release exhibited opposite patterns in the anterior-posterior axis, with significant correlations observed between the arrow impact points of the horizontal axis and the left shoulder, right elbow, left hip, and both knees. Additionally, the lateral movements induced by the reaction force upon arrow release showed significant associations with the vertical coordinates of the impact points. Particularly, the correlations between the movements of the left shoulder and elbow, as well as the bilateral hip and right knee, were consistently observed among all participants. Conclusion: These findings implied that the post-release movements could significantly influence the trajectory and impact points of the arrows in compound archery. We suggest that a consistent and controlled movement during the follow-through phase may be more beneficial for optimizing shooting accuracy and precision rather than minimizing movements.