• Journal of Hydrogen and New Energy
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• v.17 no.1
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• pp.69-74
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• 2006

Thick film $H_2$ sensors were fabricated using $SnO_2$ loaded with $Ag_2O$ and $PtO_x$. The composition that gave the highest sensitivity for $H_2$ was in the weight% ratio of $SnO_2 : PtO_x : Ag_2O$ as 93 : 1 : 6. The nano-crystalline powders of $SnO_2$ synthesized by sol-gel method were screen printed with $Ag_2O$ and $PtO_x$ on alumina substrates. The fabricated sensors were tested against gases like $H_2$, $CH_4$, $C_3H_8$, $C_2H_5OH$ and $SO_2$. The composite material was found sensitive against $H_2$ at the working temperature $130^{\circ}C$, with minor interference of other gases. The $H_2$ gas as low as 100 ppm can be detected by the present fabricated sensors. It was found that the sensors based on $SnO_2-Ag_2O-PtO_x$ system exhibited the high performance, high selectivity and very short response time to $H_2$ at ppm level. These characteristics make the sensor to be a promising candidate for detecting low concentrations of $H_2$.

• Composites Research
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• v.15 no.2
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• pp.11-17
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• 2002

The piezoelectric thin film sensor can be used to interpret variations in structural and material properties, e.g. for structural integrity monitoring and assessment. To illustrate one of this potential benefit, PVDF (polyvinylidene fluoride) film sensors are used for monitoring impact damage in Gr/Ep composite panels. Both PVDF film sensors and strain gages are attached to the surface of Gr/Ep specimens. A series of impact tests at various impact energy by changing impact mass the height are performed on the instrumented drop weight impact tester. The sensor responses are carefully examined to predict the onset of impact damage such as indentation, matrix cracking, and delamination, etc. Test results show that the particular waveforms of sensor signals implying the damage initiation and development are detected above the damage initiation impact energy. As expected, the PVDF film sensor is found to be more sensitive to impact damage initiation event than the strain gage.

• Composites Research
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• v.13 no.3
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• pp.9-20
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• 2000

Free vibration characteristics of a cantilevered laminated composite beam with multiple non-propagating transverse open cracks are investigated. In the present analysis a special ply-angle distribution referred to as asymmetric stiffness configuration inducing the elastic coupling between chord-wise bending and extension is considered. The multiple open cracks are modelled as equivalent rotational springs whose spring constants are calculated based on the fracture mechanics of composite material structures. Governing equations of a composite beam with open cracks are derived via Hamilton's Principle and Timoshenko beam theory encompassing transverse shear and rotary inertia effect is adopted. The effects of various parameters such as the ply angle, fiber volume fraction, crack numbers, crack positions and crack depthes on the free vibration characteristics of the beam with multiple cracks are highlighted. The numerical results show that the existence of the multiple cracks in an anisotropic composite beam affects the free vibration characteristics in a more complex fashion compared with the beam with a single crack.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2005.04a
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• pp.146-149
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• 2005

The using of composite material is an aviation field but it changes into a general industry. Especially composites are expanding the use on transportation vehicles like automobiles, ships, and aircrafts. The main factor of this expansion is high specific strength. It can supply a high quality and efficiency of energy. But manufacturing of composite products requires many raw materials and tooling cost for special process, so we needs a reduction of these costs to achieve best efficiency. In the present study, we contrast the change of mechanical and physical properties between VaRTM(Vacuum Assisted Resin Transfer Molding) and hand lay-up process. VaRTM process can offer a high quality the same as autoclave products, and low cost like hand lay-up process. In the results of mechanical tests, VaRTM specimen is stronger than hand lay-up specimen and hand lay-up specimen became delamination. In the results of physical tests, the resin content of VaRTM specimen is lower than hand lay-up specimen. On micrograph, the strength of specimen by VaRTM between fiber and resin is stronger than that of one by hand lay-up. And the specimen by hand lay-up contains more defects than one by VaRTM. So, VaRTM process can practically apply for automobile engine hood. This paper shows that VaRTM process is one of the most suitable processes for composite parts of automobile.

• Composites Research
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• v.27 no.2
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• pp.72-76
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• 2014

This study is investigated by experiments and analyses at rates of 2.5m/s, 7.5m/s and 12.5m/s on the impact of tapered double cantilever beam specimens with aluminium alloy. It aims to examine the mechanical property of aluminum alloy by evaluating energy release rate and equivalent stress happened at the bonded part of specimen. Because bonding force remains after the separation of specimen, the energy release rate at the bonded part becomes highest. As crack propagates and the high stress happens at the end of the bonded part, the maximum equivalent stress becomes higher at the last stage, regardless of impact rate. These results of experiments and analyses are the data necessary to develop the safe design of composite material to prevent crack propagation due to impact.

• Composites Research
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• v.27 no.2
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• pp.66-71
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• 2014

This study carried out finite element vibration analysis of pole structures made of GFRP, which is based on the micro-mechanical approach for different fiber-volume fractions. The finite element (FE) models for composite structures using multi-scale approaches described in this paper is attractive not only because it shows excellent accuracy in analysis but also it shows the effect of the material combination. The FE model is used for studying free vibrations of laminated composite poles for various fiber-volume fractions. In particular, new results reported in this paper are focused on the significant effects of the fiber-volume fraction for various parameters, such as fiber angles, layup sequences, and length-thickness ratios. It may be concluded from this study that the combination effect of fiber and matrix, largely governing the dynamic characteristics of composite structures, should not be neglected and thus the optimal combination could be used to design such civil structures for better dynamic performance.

• Composites Research
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• v.27 no.2
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• pp.37-41
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• 2014

Fiber reinforced composite materials have outstanding specific strength and specific stiffness. So the use of composite materials increases in various kinds of industrial fields including sports goods such as bicycles. Composite materials are used to make structural parts with various kinds of shapes. Specially, rectangular composite tubes are used to make a few of composite bicycle frames, but there has been a few of research on this issue. Rectangular composite tubes are designed to have appropriate radius of curvature and endure bending and torsional loads. In this research, nine kinds of rectangular composite tubes having aspect ratios 1:1, 1:1.5, 1:2 and radius of curvatures R5, R10, R15 were fabricated. The carbon fiber reinforced composite material was used to make tubes having same cross sectional areas. The stacking sequence of tubes is $[0/90/{\pm}45]s$. Experimental evaluation was accomplished to apply bending and torsional load to the tubes. Experimental results show that bending and torsional characteristics depend on radius of curvature and aspect ratio of rectangular composite tubes.

• Composites Research
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• v.27 no.4
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• pp.174-181
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• 2014

This study describes viscoelasticity analysis of carbon-fiber reinforced polymer matrix composite material. One of the most important problem during high temperature molding process is residual stress. Residual stress can cause warpage and cracks which can lead to serious defects of the final product. For the difference in thermal expansion coefficient and change of resin property during curing, it is difficult to predict the final deformed shape of carbon-fiber reinforced polymer matrix composite. The consideration of chemical shrinkage can reduce the prediction errors. For this reason, this study includes the viscoelasticity and chemical shrinkage effects in FE analysis by creating subroutines in ABAQUS. Analysis results are compared with other researches to verify the validity of the subroutine developed, and several stacking sequences are introduced to compare tested results.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.37 no.7
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• pp.627-633
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• 2009

Composite has become one of the most frequently used material for a tube of satellite camera due to its attractive characteristics. However, laminated composites can be weakened by delamination which comes from interlaminar stress. Such failure mode cause structural instability of the camera as well as degradation of optical quality. Therefore composite tube should be robust in delamination. Also, composite tube should have high stiffness, sufficient high natural frequency and small coefficient of thermal expansion. The design procedures presented in this paper are based on design of experiments. The experiments for mechanical analysis are designed by the tables of orthogonal arrays. In order to manipulate the various mechanical properties systematically, multiple-attribute decision making(MADM) is employed. Through analysis of variance and F-test, the critical design variables which have dominant influences on mechanical performance are determined. Finally improved ply angles for composite tube are determined.

• Korean Journal of Materials Research
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• v.19 no.10
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• pp.517-521
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• 2009

Si-C composite with hollow spherical structure was synthesized using ultrasonic treatment of organosilica powder formed by hydrolysis of phenyltrimethoxysilane. The prepared powder was pyrolyzed at various temperatures ranging from 900 to 1300 $^{\circ}C$ under nitrogen atmosphere to obtain optimum conditions for Li-ion battery anode materials with high capacity and cyclability. The XRD and elemental analysis results show that the pyrolyzed Si/C composite at 1100 $^{\circ}C$ has low oxygen and nitrogen levels, which is desirable for increasing the electrochemical capacity and reducing the irreversible capacity of the first discharge. The solid Si-C composite electrode shows a first charge capacity of $\sim$500 mAhg$^{-1}$ and a capacity fade within 30 cycles of 0.93% per cycle. On the other hand, the electrochemical performance of the hollow Si-C composite electrode exhibits a reversible charge capacity of $\sim$540 mAhg$^{-1}$ with an excellent capacity retention of capacity loss 0.43% per cycle up to 30 cycles. The improved electrochemical properties are attributed to facile diffusion of Li ions into the hollow shell with nanoscale thickness. In addition, the empty core space provides a buffer zone to relieve the mechanical stresses incurred during Li insertion.