• 제목/요약/키워드: Composite Degree

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Prediction Method of Dispersion Condition for Reinforced Epoxy in Nano SiC Particles Using Capacitance Measurement (Capacitance 측정법을 이용한 나노 SiC 에폭시 복합재료의 내부 강화재 분산 예측방법)

  • Kwon, Dong-Jun;Wang, Zuo-Jia;Kim, Je-Jun;Jang, Key-Wook;Park, Joung-Man
    • Composites Research
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    • v.26 no.6
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    • pp.337-342
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    • 2013
  • The good dispersion of nano-materials in epoxy matrix was important parameter for the reinforcement effect, and the evaluation of dispersion degree was to prove it. This work was studied to predict the dispersion condition of nano-SiC powders in SiC/epoxy composites using capacitance measurement. Capacitance was defined to be the electric capacity in proportional to electron charge of the measuring section. In case of nano-SiC powders, the electron charge of SiC/epoxy composites was higher than that of neat epoxy resin. Capacitance was evaluated for each section of SiC/epoxy composites. The prediction of dispersion condition was verified by using capacitance measurement. Dispersion condition of nano-SiC powders in epoxy matrix was evaluated with two different dispersion methods, i.e., sonication and stirring methods. The dispersion degree was also verified with the tensile strength correlating to capacitance.

Hydrophilization of a Porous Polytetrafluoroethylene Supporter by Radiation Grafting Poly(Acrylonitrile-co-Sodium Allylsulfonate) (Acrylonitrile/Sodium Allylsulfonate 공중합체 방사선 접목을 이용한 다공성 Polytetrafluoroethylene 지지체의 친수화)

  • Park, Byeong-Hee;Sohn, Joon-Yong;Yoon, Ki-Suk;Shin, Junhwa
    • Polymer(Korea)
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    • v.38 no.3
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    • pp.293-298
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    • 2014
  • We prepared hydrophilic porous supporters for the reinforced composite fuel cell membrane by radiation grafting of acrylonitrile (AN) and hydrophilic sodium allylsulfonate (SAS) into a porous polytetrafluoroethylene (PTFE) supporter. The physicochemical properties of the supporters prepared under various reaction conditions such as molar ratio of SAS/AN, monomer concentration, and irradiation dose were evaluated. FTIR was utilized to confirm the successful introduction of SAS/AN copolymer chains into the porous PTFE. The pores of the porous PTFE film were found to be decreased with an increase in the degree of grafting by using FE-SEM and gurley number. Furthermore, by analyzing the degree of grafting, contact angle, and TBO (toluidine blue O) uptake, the hydrophilicity of the prepared supporters was found to increase with an increase in the degree of grafting.

MICROLEAKAGE OF MICROFILL AND FLOWABLE COMPOSITE RESINS IN CLASS V CAVITY AFTER LOAD CYCLING (Flowable 및 microfill 복합레진으로 충전된 제 5급와동에서 load cycling 전,후의 미세변연누출 비교)

  • Kang, Suk-Ho;Kim, Oh-Young;Oh, Myung-Hwan;Cho, Byeong-Hoon;Um, Chung-Moon;Kwon, Hyuk-Choon;Son, Ho-Hyun
    • Restorative Dentistry and Endodontics
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    • v.27 no.2
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    • pp.142-149
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    • 2002
  • Low-viscosity composite resins may produce better sealed margins than stiffer compositions (KempScholte and Davidson, 1988: Crim, 1989). Plowable composites have been recommended for use in Class V cavities but it is also controversial because of its high rates of shrinkage. On the other hand, in the study comparing elastic moduli and leakage, the microfill had the least leakage (Rundle et at. 1997) Furthermore, in the 1996 survey of the Reality Editorial Team, microfills were the clear choice for abfraction lesions. The purpose of this study was to evaluate the microleakage of 6 compostite resins (2 hybrids, 2 microfills, and 2 flowable composites) with and without load cycling. Notch-shaped Class V cavities were prepared on buccal surface of 180 extracted human upper premolars on cementum margin. The teeth were randomly divided into non-load cycling group (group 1) and load cycling group (group 2) of 90 teeth each. The experimental teeth of each group were randomly divided into 6 subgroups of 15 samples. All preparations were etched, and Single bond was applied. Preparations were restored with the following materials (n=15) : hybrid composite resin [Z250(3M Dental Products Inc. St. Paul, USA), Denfil(Vericom, Ahnyang, Korea)], microfill [Heliomolar RO(Vivadent, Schaan, Liechtenstein), Micronew(Bisco Inc. Schaumburg, IL, USA)], and flowable composite[AeliteFlo(Bisco Inc. Schaumburg, IL, USA), Revolution(Kerr Corp. Orange, CA, USA)]. Teeth of group 2 were subjected to occlusal load (100N for 50,000 cycles) using chewing simulator(MTS 858 Mini Bionix II system, MTS Systems Corp. Minn. USA). All samples were coated with nail polish 1mm short of the restoration, placed in 2% methylene blue for 24 hours, and sectioned with a diamond wheel. Enamel and dentin/cementum margins were analyzed for microleakage on a sclale of 0 (no leakage) to 3 (3/3 of wall). Results were statistically analyzed by Kruscal-Wallis One way analysis, Mann-Whitney U-test, and Student-Newmann-Keuls method. (p = 0.05) Results : 1. There was significantly less microleage in enamel margins than dentinal margins of all groups (p<0.05) 2. There was no significant between six composite resin in enamel margin of group 1. 3. In dentin margin of group 1, flowable composite had more microleakage than others but not of significant differences. 4. there was no significant difference between six composite resin in enamel margin of group 2. 5. In dentin margin of group 2, the microleakage were R>A =H=M>D>Z. But there was no significant differences. 6. In enamel margins, load cycling did not affect the marginal microleakage in significant degree. 7. In enamel margins, load cycling did affect the marginal microleakage only in Revolution. (p<0.05).

A COMPARATIVE STUDY OF WATER ABSORPTION AND RELATED CHANGES OF COMPRESSIVE STRENGTH IN THREE RESTORATIVE MATERIALS (치과용 수복재의 수분흡수도와 압축강도의 변화에 관한 연구)

  • Chang, Woo-Hyuck;Choi, Yeong-Chul
    • Journal of the korean academy of Pediatric Dentistry
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    • v.30 no.1
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    • pp.161-170
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    • 2003
  • The aesthetic restorative materials are widely used in recent dentistry, showed not only the different quality between each component but also showed that the environment of the material has important effect on the physical properties of the material. Especially, when the restoratives are restored in the mouth, and since saliva is existing, the restoratives are always exposed to water and affected by the saliva. The purpose of this study was to research and compare the change of the degree of water sorption after water immersion of three types of the resin-based materials and the compressive strength, and observe the relation between the change of the water absorbing degree and the compressive strength. Z-100(3M, U.S.A) as a composite resin, F-2000(3M, U.S.A) as a compomer and Vitremer Restoratives(3M, U.S.A) as a resin-modified GIC were used, and each specimen was made to measure the water sorption and to evaluate the compressive strength. The specimens for measurement of the water sorption and the compressive strength were divided into 4 groups(1 day, 2 weeks, 4 weeks, and 8weeks). Each specimen was filled in the 30cc vial with 20cc of distilled water during the fixed amount of period in $37^{\circ}C$. The water sorption is decided by dividing the difference of weight before and after the immersion by the volume, and the compressive strength was measured by using the instron after the immersion. The following results were obtained ; 1. The more the water sorption increased, the more the immersion period of three restorative materials was long. And the most of water sorption was obtained during the first 2 weeks(P<0.001). 2. The water sorption of resin-modified GIC was higher than composite resin and compomer. 3. The more the compressive strength decreased, the more the immersion period of three restorative materials increased(composite resin and compomer: P<0.001, resin-modified GIC: P<0.05). Especially, the amount of the reduction in compressive strength of the composite resin was the highest. 4. The more the water sorption of all materials increased, the more the compressive strength decreased(P<0.05).

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Studies on Evaluation for Long-term Loading of Composite Wood-joint and Characteristics of Joint Strength (I) - The strength properties of mechanical joints of Pinus densiflora with drift pin and bolt - (목재 접합부의 강도특성 및 장기 내력 평가 (I) - 소나무재의 Bo1t 및 Drift pin 접합부 능력(耐力) 성능 평가 -)

  • Hong, Soon-Il;Hwang, Won-Jung;Kim, Eun-Sam;Jin, Kwang-Sung
    • Journal of the Korean Wood Science and Technology
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    • v.29 no.4
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    • pp.1-8
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    • 2001
  • This study was carried out to investigate the strength and stiffness of drift pinned and bolted joints with steel-plates by the tension-type lateral strength tests. Specimens were solid wood of Pinus densiflora. Bolt and drift pin were jointed with inserted steel plates. Tests were conducted with combinations of two loading directions (parallel to the grain : 0 degree, perpendicular to the grain : 90 degree) and three diameters of fasteners (d = 6 mm, 10 mm, 12 mm). The results obtained were as follow: 1. In the test of the parallel to the grain, maximum loads were increased with increasing of the diameter of bolt and drift pin in the same end distance. In the test of perpendicular to the grain with diameter 10 mm and 12 mm, specimens mostly were failed with horizontal splits in woods reaching the yield load of drift pinned and bolted joints. 2. The ratio of maximum load to the yield load determined by the so-called "5% offset method", was great in bolted joints in the parallel to the grain This trend become more remarkable as the slenderness ratio was increased. 3. The calculated yield strength was agreed well with the experimental results of drift pinned joint(0 degree).

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PMM for Surface Treatment of Concrete with the Utilization of By-Products

  • Drochytka, Rostislav;Zizkova, Nikol
    • International Journal of Concrete Structures and Materials
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    • v.2 no.1
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    • pp.49-55
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    • 2008
  • The disadvantage of PMM's (polymer-modified mortars) that are currently on the market is the utilization of expensive polymer additives and also the cost of the other components. One of the possibilities how to decrease this price is the effective utilization of waste materials which are very inexpensive in spite of their good properties. The combinations of different degree in polymer adhesiveness and waste secondary raw materials - fly ash - are experimentally verified in the paper. The use of fly ash in adhesive materials for ceramic tiles is limited by unsatisfactory initial adhesiveness to sintered ceramic sherd as a result of a running pozzolanic reaction that lowers the efficiency of polymer additives. On the other hand, the use of adhesive and backfill coating materials for gluing ETICS board insulation materials has brought very good results.

MARGINAL LEAKAGE TEST ON 'Hi-Pol' ENAMEL BOND SYSTEM (국산 'Hi-Pol' Enamel Bond System의 변연누출에 관한 실험적 연구)

  • Kwon, Hyuk-Choon
    • The Journal of the Korean dental association
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    • v.16 no.12 s.115
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    • pp.935-940
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    • 1978
  • The purpose of this study was to evaluate the marginal sealing ability of 'Hi-Pol' Enamel Bond system. Using freshly extracted human teeth and 2% acquous methylene blue, the marginal leakage of dye in restorative materials such as 'Hi-Pol' Enamel Bond system, Hi-Pol, Adaptic, Nuva system, Epolite and Amalgam were investigated at 37℃ and under temperature cycling in range of 4℃-60℃. the results as follows; 1. All filling materials showed some degree of marginal penetration by 2% methylene blue dye. 2. 'Hi-Pol' Enamel Bond system revealed the least marginal penetration by 2% methylene blue as Nuva did at 37℃, but under temperature cycling in range of 4℃-60℃ it showed the greatest marginal penetration. 3. Hi-Pol restoration showed a tendency the similar to the other composite restoration. 4. Nuva system had the most effective marginal sealing ability either at 37℃ and under temperature cycling.

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Parametric study on energy demands for steel special concentrically braced frames

  • Dogru, Selcuk;Aksar, Bora;Akbas, Bulent;Shen, Jay
    • Steel and Composite Structures
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    • v.24 no.2
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    • pp.265-276
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    • 2017
  • Structures are designed in such a way that they behave in a nonlinear manner when subject to strong ground motions. Energy concepts have been widely used to evaluate the structural performance for the last few decades. Energy based design can be expressed as the balance of energy input and the energy dissipation capacity of the structure. New research is needed for multi degree of freedom systems (MDOFs)-real structures- within the framework of the energy based design methodology. In this paper, energy parameters are evaluated for low-, medium- and high-rise steel special concentrically braced frames (SCBFs) in terms of total energy input and hysteretic energy. Nonlinear dynamic time history analyses are carried out to assess the variation of energy terms along the height of the frames. A seismic energy demand spectrum is developed and hysteretic energy distributions within the frames are presented.

Truncated hierarchical B-splines in isogeometric analysis of thin shell structures

  • Atri, H.R.;Shojaee, S.
    • Steel and Composite Structures
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    • v.26 no.2
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    • pp.171-182
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    • 2018
  • This paper presents an isogeometric discretization of Kirchhoff-Love thin shells using truncated hierarchical B-splines (THB-splines). It is demonstrated that the underlying basis functions are ideally appropriate for adaptive refinement of the so-called thin shell structures in the framework of isogeometric analysis. The proposed approach provides sufficient flexibility for refining basis functions independent of their order. The main advantage of local THB-spline evaluation is that it provides higher degree analysis on tight meshes of arbitrary geometry which makes it well suited for discretizing the Kirchhoff-Love shell formulation. Numerical results show the versatility and high accuracy of the present method. This study is a part of the efforts by the authors to bridge the gap between CAD and CAE.

Connection stiffness and natural frequency of DuraGal lightweight floor systems

  • Zhao, X.L.;Taplin, G.;Alikhail, M.
    • Structural Engineering and Mechanics
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    • v.15 no.3
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    • pp.269-284
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    • 2003
  • This paper reports a series of component tests on a lightweight floor system and a method to predict the natural frequency of the floor using a frame analysis program. Full-scale floor tests are also briefly described. DuraGal steel Rectangular Hollow Sections (in-line galvanised RHS) are used as joists, bearers and piers in DuraGal lightweight floor systems. A structural grade particleboard is used as decking. Connection stiffness between different components (bearer, joist, pier and floor decking) was determined. A 40% composite action was achieved between the RHS joist and the particleboard. Both 2D and 3D models were developed to study the effect of connection stiffness on predicting the natural frequency of DuraGal lightweight floor systems. It has been found that the degree of shear connection between the bearer and the joist has a significant influence on the floor natural frequency. The predicted natural frequencies are compared with measured values from full scale floor testing.