• 연구논문집
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• s.33
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• pp.175-182
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• 2003

In this study, the wear resistance of the complex powder diffusion treated KS STD 61 has been investigatived. KS STD 61 tool steel was pretreated in quenching and tempering processes to obtain the tempered martensitic microstructure. The samples were packed with complex powder in steel pot($\Phi$90x60mm) and heated in a box furnace. the complex powder diffusion treatment are carried out at $540^{\circ}C$, $520^{\circ}C$, $500^{\circ}C$ for 40min, 1.5hr and 2.5hr. The microstructure, microhardness, wear resistance, and coating layer thickness of the complex powder diffusion treated samples were investigation. The weight loss of as heat treated sample was 0.4mg and that of the complex powder treated at $540^{\circ}C$ for 2.5hr was 0.17mg. These result means that the wear resistance of tool steels can be easily improved by the powder diffusion process at conventional tempering treatment temperature.

• Korean Journal of Plant Resources
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• v.20 no.3
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• pp.226-233
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• 2007

To develop a clinically available saponin- or sapogenin complex from Oriental medicines, the EtOH extract (KPRG-A) was obtained by extracting from the four crude drugs, Kalopanacis Cortex, Platycodi Radix, Rubi Fructus and Glycyrrhizae Radis. The BuOH fraction (KPRG-B), a crude saponin complex, was prepared by fractionating KPRG-A, which were further completely hydrolyzed to afford the sapogenin complex (KPRG-D). In an attempt to find the antinoicpetive effects of the saponin complex and sapogenin complex, KPRG-C, and -D, were assayed by writhing-, hot plate-, and tail-flick tests using mice or rats. The three samples were also subjected to antiiflammatory tests using serotonin-induced and carrageenan-induced hind paw edema mice and rats, respectively. The three samples significantly reduced inflammations and pains of the experimental animal. The potency were found in the order of KPRG-D> KPRG-C> KPRG-B. The most active sample, KPRG-D, caused no death, no body increase or no anatomical pathlogic change even at 2,000 mg/kg dose. These results suggest that a sapogenin complex, KPRG-D, which was found to contain mainly hederagenin, platycodigenin, polygalacic acid, 23-hydroxytormentic acid, glycyrrhetic acid together with minor triterpene acids, could be a potential candidate for antiinflammatory therapeutics.

• Journal of the Korean Ceramic Society
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• v.35 no.8
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• pp.801-806
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• 1998

$Eu^{3+}$ -doped $Y_2$$O_3$ phosphors has been prepared by a polymerized complex method and investigated their powder and luminescence properties. They were compared with phosphors prepared by a solid state reac-thion method. The phosphors synthesized have been characterized by X-ray diffraction low-voltage lu-minescent emission spectroscopy etc. Under low-voltage electron excitation $Eu^{3+}$-doped $Y_2$$O_3$ exhibited a strong narrow-band red emission peaking at 612nm. On the other hand the critical value for concentration quenching of sample prepared by the polymerized complex method fired at $1400^{\circ}C$ is x=0.05 for $(Y_{1-x}Eu_x__2O_3$ The emission intensity of phosphors prepared by the polymerized complex method was higher than that of phosphors prepared by the solid state reaction method.

• Bulletin of the Korean Chemical Society
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• v.21 no.11
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• pp.1090-1094
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• 2000

A reaction between germanium (Ge) and the ligand, o-chlorophenylfluorone (o-CPF) has been carried out. The reaction sensitive at pH 4.5 in the presence of triton x-100 was selective in the presence of EDTA. The spectral correction technique was ap plied to the analysis of the reaction instead of single wavelength spectrophotometry because the absorption of excess of o-CPF was not negligible. An updated determination of the properties of the Ge(IV)-o-CPF complex is given, which involved the complex ratio, stepwise absorptivity and stability constant of the complex. In present work, the results show that the complex $Ge(o-CPF)_3was$ formed and its cumulative stability constant was 1.09 ${\times}$1016 . For sample analysis, the detection limit of germanium was 0.01 mg/L, and the recoveries were between 96.4% and 102%, with relative standard deviations of less than 6.5%.

• Journal of the Korean Ceramic Society
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• v.28 no.2
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• pp.101-108
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• 1991

0.2 mo1% La doped BaTiO3 samples were prepared by a wet chemical process (Pechini process) and electrical conductivity were measured from annealing temperatures(800-110$0^{\circ}C$) to room temperature continuously. 2 probe I-V characteristics showed that Pt electrodes were non-ohmic below about 80$0^{\circ}C$ for Ladoped sample. I-V curves showed varistor behavior and breakdown voltages showed PTC-like behavior. AC complex impedance of 0.2 La and 0.05 Mn mo1% doped BaTiO3 samples with three different electrodes (electroless Ni, Pt, Ag electrodes) were measured with temperature variation. Complex impedance plots showed that the samples with electroless Ni electrodes have negligible electrode resistance. Samples with Ag or Pt paste electrodes showed large electrode resistance. PTC effect, which is defined as the ratio of maximum resistance to minimum resistance, was found to be less than 10 for 0.2 mo1% La doped dense sample however greater than 105 with codoping of 0.05 mo1% Mn and 0.2 mol% La.

• Asian-Australasian Journal of Animal Sciences
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• v.25 no.11
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• pp.1511-1514
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• 2012

Epistasis that may explain a large portion of the phenotypic variation for complex economic traits of animals has been ignored in many genetic association studies. A Baysian method was introduced to draw inferences about multilocus genotypic effects based on their marginal posterior distributions by a Gibbs sampler. A simulation study was conducted to provide statistical powers under various unbalanced designs by using this method. Data were simulated by combined designs of number of loci, within genotype variance, and sample size in unbalanced designs with or without null combined genotype cells. Mean empirical statistical power was estimated for testing posterior mean estimate of combined genotype effect. A practical example for obtaining empirical statistical power estimates with a given sample size was provided under unbalanced designs. The empirical statistical powers would be useful for determining an optimal design when interactive associations of multiple loci with complex phenotypes were examined.

• The korean journal of orthodontics
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• v.15 no.2
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• pp.279-289
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• 1985

This study was undertaken to find out the factor highly correlated to the depth of overbite among the skeletal factors of the craniofacial complex using lateral roentgenocephalograms. The subjects cconsited of fifty normal occlusions, sixty Class I malocclusions, sixty Class II division I malocclustions and sixty Class III malocclusions. The results were as follows: 1. Ans-Go-Me angle and lower genial angle showed high correlation to the depth of overbite in the total malocclusion sample. 2. The mean values of Ans-Go-Me angle and lower goinal angle for the normal sample were $49.8^{\circ}\;and\;75.6^{\circ}$, respectively. 3. Ans-Go-Me angle above $56^{\circ}$ or lower gonial angle above $84^{\circ}$ indicated a tendency toward an openbite. Conversely, Ans-Go-Me angle below $48^{\circ}$ or lower goinal angle below $73^{\circ}$ indicated a tendency toward a deepbite.

• Survey Research
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• v.1 no.1
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• pp.109-123
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• 2000

In order to make statistically valid inferences for survey data based on complex probability sample designs, survey researchers must incorporate the sample design in the data analysis If this in not the case the variance estimates of survey statistics derived under the usual simple random sampling assumptions from an infinite population generally underestimate the true variance, which results in high Type l error level. In this article we introduce new software packages dedicated to analyze complex survey data In particular, we summarize analysis capabilities on SUDAAN Version 7.5 and SAS Version 8.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.15 no.1
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• pp.93-101
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• 2002

In this study, the stator form-winding sample coils based on silicone resin and polyimide were made for fault prediction and reliability estimation on the C-Class(200$\^{C}$ ) insulation system of traction motors. The complex accelerative degradation was periodically performed during 10 cycles, which was composed of thermal stress, fast rising surge voltage, vibration, water immersion and overvoltage applying. After aging of 10 cycles, the condition diagnosis test such as insulation resistance '||'&'||' polarization index, capacitance '||'&'||' dielectric loss and partial discharge properties were investigated in the temperature range of 20 ∼ 160$\^{C}$. Relationship among condition diagnosis tests was analyzed to find a dominative degradation factor and an insulation state at end-life point.

• Journal of the Korean Data and Information Science Society
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• v.25 no.3
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• pp.523-531
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• 2014

Design effect is often used in designing and planning sample surveys and/or in evaluating the efficiency of complex design features of the surveys. In this study, we applied Gabler et al. (2006)'s design effect model to 2013 Consumer behavior survey for food that was carried out by stratified two-stage sampling. Usability and adequacy of the design model to a real survey data are discussed and evaluated.