• 제목/요약/키워드: Combined standard uncertainty

검색결과 61건 처리시간 0.019초

엔진 고도 시험의 측정 신뢰성 평가 (Reliability of Measurement Estimation in Altitude Engine Test)

  • 이진근;양인영;양수석;곽재수
    • 한국항공운항학회지
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    • 제14권3호
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    • pp.1-6
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    • 2006
  • The altitude engine test is a sort of engine performance tests carried out to measure the performance of a engine at the simulated altitude and flight speed environments prior to that at the flight test. During the performance test of a engine, various values such as pressures and temperatures at different positions, air flow rate, fuel flow rate, and the load by thrust are measured. These measured values are used to derive the representative performance values such as the net thrust and the specific fuel consumption through a momentum equation. Hence each of the measured values has certain effects on the total uncertainty of the performance values. In this paper, the combined standard uncertainties of the performance variables at the engine test were estimated by the uncertainty analysis of the measurement values and the repeatability and reproducibility of the altitude test measurement were assessed by the analysis of variation on the repeated test data with different operator groups.

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2,4-DNPH와 가스크로마토그래프를 이용한 포름알데히드 분석방법 (Analytical method for analyzing formaldehyde using 2, 4-DNPH and gas chromatography/FID, NPD)

  • 정지연;박승현;이광용;오세민
    • 한국산업보건학회지
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    • 제10권1호
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    • pp.126-146
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    • 2000
  • To develop and evaluate formaldehyde measurement method using 2,4-dinitro-phenylhydrazine (2,4-DNPH) coated sampler and gas chromatography, laboratory test and field test were conducted. Results of this study are as follows. Limit of detection(LOD) of measurement methods, HPLC-UVD, GC-NPD and GC-FID, is $0.008{\mu}g/m{\ell}$ $0.060{\mu}g/m{\ell}$, $0.472{\mu}g/m{\ell}$ respectively. Coefficiency of measurement methods, HPLC-UVD, GC-NPD and GC-FID, is 0.008, 0.009, 0.020 respectively. Desorption efficiency of sep-pak xposure aldehyde sampler and sorbent sample tube is 1.05(range : 0.99 - 1.12), 1.02(range : 0.99 - 1.06) respectively. Samples of sorbent sample tube and sep-pak xposure aldehyde sampler turned out to be stored at refrigerator, according to storage test results. Measurement methods of HPLC-UVD, GC-NPD, GC-FID, according to results of precision for the combined sampling and analytical procedure, became acceptable to OSHA evaluation standard. Field test using exposure chamber met the NIOSH overall uncertainty recommendation(less than 25%). Overall uncertainty of Sepak-HPLC(UVD), Tube-GC(NPD), Tube-GC(FID) is 11.0% - 17.0%. Consequently gas chromatography(GC-NPD, GC-FID) and high performance liquid chromatography(EPA TO-11) using 2,4-DNPH coated sampler for formaldehyde measurement turned out to be suitable to measure personal formaldehyde exposure at workplaces.

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왕수분해와 결합한 자동분석법의 토양 중 불소시험 유효성 연구 (The Validation Study of Auto Anlysis Method Combined with Aqua Regia Digestion for Fluorine of Soil)

  • 나경호;윤인철;이정복
    • 한국지하수토양환경학회지:지하수토양환경
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    • 제15권5호
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    • pp.8-15
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    • 2010
  • The purpose of this research is to check the validation of an auto-analysis method combined with aqua regia digestion apparatus for improvement of water distillation method used as a fluorine test of soil. Fluorine contents of CaO used in the pretreatment course of water distillation method were 120 mg/kg ~ 5,064 mg/kg at the blank test, which was exceeded up to maximum 12.5 times of the soil standard, so it was estimated due to a effect of fluorine existing as impurities of CaO. The recovery test of the same samples indicated that water distillation method and auto-analysis method were 134.5mg/kg and 161.7mg/kg respectively, the recovery ratio of the latter was 16.8% higher than the formal. The validation test of two methods satisfied the standard, but auto analysis method was excellent more than distillation method. Also, auto analysis method could save a analysis time up to maximum 4.7 times by comparison with water distillation method.

Evaluation of measurement uncertainty for quantitative determination of chlorite and chlorate in fresh-cut vegetables using ion chromatography

  • Jung, Sungjin;Kim, Dasom;Lee, Gunyoung;Yun, Sang Soon;Lim, Ho Soo;Jung, Young Rim;Kim, Hekap
    • 한국식품과학회지
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    • 제49권6호
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    • pp.591-598
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    • 2017
  • This study aimed to evaluate the measurement uncertainty for the quantitative determination of chlorite and chlorate in ready-to-eat fresh-cut vegetables using ion chromatography with a hydroxide-selective column. One gram of the homogenized sample in deionized water was sonicated and centrifuged at 8,500 rpm. The supernatant was purified by passing it through a Sep-Pak tC18 cartridge, followed by chromatographic determination using a Dionex IonPac AS27 column. The linearity of the calibration curves, recovery, repeatability, and reproducibility of the method were satisfactory. The method detection limit was estimated to be approximately 0.5 mg/kg. Each uncertainty component was evaluated separately, and the combined and expanded uncertainty values were calculated at the 95% confidence level. The measured concentrations for 3 mg/kg of chlorite and chlorate standard materials were $3.18{\pm}0.32$ and $3.10{\pm}0.42mg/kg$, respectively. These results confirmed the reliability of the developed method for measuring the two chlorine-based oxyanions in fresh-cut vegetables.

초음파간섭 수은주압력계와 정적법 중진공 국가표준기 상호비교 (Inter-comparison between ultrasonic interferometer manometer and medium vacuum standards by static expansion method)

  • 홍승수;임인태;신용현;정광화
    • 한국진공학회지
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    • 제14권3호
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    • pp.103-109
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    • 2005
  • 정적법을 이용하여 새로운 중진공 국가표준기를 개발하였다. 이 장치의 성능평가를 위해 측정범위가 각각 133pa과 1,333pa인 두 개의 용량혈 진공게이지를 전달표준기로 사용하여 초음파간섭 수은주압력계와 중진공 표준을 상호비교하였다. Error normalized (En) 값으로 분석한 결과 교정압력 $3pa\;\sim\;100pa$에서 두 표준기는 합성불확도 범위 내에서 잘 일치하고 있음을 알 수 있었다.

별 측광을 통한 야간 에어로졸의 광학적 두께 산출 (Retrieval of Nighttime Aerosol Optical Thickness from Star Photometry)

  • 오영록
    • 대기
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    • 제25권3호
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    • pp.521-528
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    • 2015
  • In this study star photometry was applied to retrieve aerosol optical thickness (AOT) at night. The star photometry system consisted of small refractor, optical filters, CCD camera, and driving mount and was located in Suwon. The calibration constants were retrieved from the astronomical Langley method but standard deviations of these were more than 10% of the mean values. After the calibration the nighttime AOT was retrieved and cloud-screened in clear six days from 25 Nov. 2014 to 17 Jan. 2015. To estimate the quality of the measurements the nighttime AOT was combined with daytime AOT retrieved from sky-radiometer that was located in Seoul and 17 km away from the star photometry system. In spite of the uncertainty of the calibration constants and the spatial difference of two observation systems, the temporal changes of the nighttime AOT coincided with the daytime. The nighttime ${\AA}ngstr{\ddot{o}}m$ exponent was about 20% lower and more variable than the daytime because of the uncertainty of the calibration constants. If the calibration process is more precise, the combination of star and sun or sky photometry system can monitor the air pollution day and night constantly.

SPR 기법을 이용한 회전 블레이드의 변형 및 모션 측정 (Measurement of Rotor Blade Deformation and Motions using Stereo Pattern Recognition Method)

  • 박재원;김홍일;한재흥;김도형;송근웅
    • 한국항공우주학회지
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    • 제39권5호
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    • pp.442-450
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    • 2011
  • 회전 블레이드의 모션을 측정하기 위해 스테레오 패턴 인식 (stereo pattern recognition, SPR) 기법을 적용한 측정 시스템을 구성하고 실험을 수행하였다. 시스템 요구사항을 만족시키는 스테레오 카메라를 확보하여 SPR 기반의 측정 시스템을 준비하였다. 시스템의 측정불확도를 계산하기 위한 일련의 실험을 통해, 본 SPR 시스템이 2m~4.2m의 측정 거리에서 0.2mm 이내의 표준불확도를 가짐을 확인하였다. 이를 이용하여 계산한 블레이드 모션의 합성표준불확도는, 리드-래그, 플래핑, 비틀림 운동에 대해 각각 0.296mm, 0.209mm, $0.238^{\circ}$ 이었다. 본 SPR 시스템을 한국항공우주연구원의 소형로터 시험장치에 설치하고 회전속도와 콜렉티브 피치각을 각각 360rpm, 589rpm, 그리고 $0^{\circ}$, $4^{\circ}$, $6^{\circ}$로 바꾸어가며, 지상 제자리비행 조건에서 블레이드의 모션과 탄성 변형을 성공적으로 측정하였다. Higher Harmonic Control Aeroacoustic Rotor Test -II 에서 사용한 측정 시스템과의 비교를 통하여 본 시스템의 장점을 분석하였다.

가중화된 GPS 정보와 지도정보를 활용한 실외 이동로봇의 위치추정 (Outdoor Localization of a Mobile Robot Using Weighted GPS Data and Map Information)

  • 배지훈;송재복;최지훈
    • 로봇학회논문지
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    • 제6권3호
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    • pp.292-300
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    • 2011
  • Global positioning system (GPS) is widely used to measure the position of a vehicle. However, the accuracy of the GPS can be severely affected by surrounding environmental conditions. To deal with this problem, the GPS and odometry data can be combined using an extended Kalman filter. For stable navigation of an outdoor mobile robot using the GPS, this paper proposes two methods to evaluate the reliability of the GPS data. The first method is to calculate the standard deviation of the GPS data and reflect it to deal with the uncertainty of the GPS data. The second method is to match the GPS data to the traversability map which can be obtained by classifying outdoor terrain data. By matching of the GPS data with the traversability map, we can determine whether to use the GPS data or not. The experimental results show that the proposed methods can enhance the performance of the GPS-based outdoor localization.

Development of Isotope Dilution LC-MS/MS Method for Accurate Determination of Arsenobetaine in Oyster Certified Reference Material

  • Lee, Woo Young;Yim, Yong-Hyeon;Hwang, Euijin;Lim, Youngran;Kim, Tae Kyu;Lee, Kyoung-Seok
    • Bulletin of the Korean Chemical Society
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    • 제35권3호
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    • pp.821-827
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    • 2014
  • An isotope dilution liquid chromatography tandem mass spectrometry (ID LC-MS/MS) method has been developed and applied to the determination of arsenobetaine (AsB, ${(CH_3)_3}^+AsCH_2COO^-$) from oyster candidate certified reference material (CRM). The exact matching isotope dilution approach was adopted for accurate determination of AsB using $^{13}C_2$-labeled AsB as an internal standard. Efficiencies of different AsB extraction methods were evaluated using a codfish reference material and a simple sonication method was selected as the method of choice for the certification of the oyster candidate CRM. The hydrophilic interaction liquid chromatography (HILIC) combined with electrospray ionization tandem mass spectrometry (ESI/MS/MS) in selected reaction monitoring (SRM) mode was optimized for adequate chromatographic retention and robust quantification of AsB from codfish and oyster samples. By analyzing 12 subsamples taken from each 12 bottles systematically selected from the whole oyster CRM batch, the certified value of AsB was determined as $6.60mg{\cdot}kg^{-1}{\pm}0.31mg{\cdot}kg^{-1}$ and it showed excellent between-bottle homogeneity of less than 0.42%, which is represented by relative standard deviation of 12 bottles from the CRM batch. The major source of uncertainty was the certified value of the AsB standard solution.

온톨로지와 군집분석을 이용한 지하공간 정보모델 개발 (Development of Subsurface Spatial Information Model with Cluster Analysis and Ontology Model)

  • 이상훈
    • 한국지리정보학회지
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    • 제13권4호
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    • pp.170-180
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    • 2010
  • 지하공간 개발의 증가에 따라 지층단면도 등 다양한 형태로 제공되는 지하공간 정보모델의 신뢰성이 요구되고 있다. 그러나 지반은 근본적으로 불확실하며, 이를 표현하는 정보모델도 자료부족, 해석표준 부재 등의 비통계적 요인과 외부환경 변수라는 통계적 요인으로 불확실성을 가진다. 따라서, 현재의 모델 생성은 고도로 훈련된 전문가에 의해 이뤄지고 있다. 본 연구는 지반공학 전문가의 경험과 지식에서 시맨틱을 추출하고, 이를 온톨로지 모델과 정보량으로 정량화하였다. 정량화한 온톨로지 모델은 군집분석의 클러스터간 거리계산에 적용하여 시맨틱을 고려한 군집분석 방법론을 제안하였다. 본 제안 방법을 실험지역에 적용한 결과 기존 K-Means 방법에 비해 전문가의 해석과 유사한 결과를 도출하였으며, 수작업으로는 어려운 대용량 데이터를 손쉽게 처리하고 3차원 GIS로 가시화가 가능하였다. 본 연구를 통해 지반공학 전문가의 도움 없이도, 그 경험을 고려하면서 대량의 지반정보 데이터를 효과적으로 처리하여 신뢰성 있는 지하공간 정보모델을 생성할 수 있을 것이다.