• 대한치과교정학회지
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• 제19권1호
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• pp.245-256
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• 1989

Translational movement along an arch wire requires sufficient force to overcome frictional forces between bracket and arch wire. The orthodontist must appreciate the importance of friction in this process, and study out the influencing factors on the level of friction. The purpose of this study was to evaluate the effect of artificial saliva on frictional resistances generated between the bracket and arch wire. Independent variables of this study were arch wire material, angulation and environment. Static frictional forces of cobalt-chromium, heat-treated cobalt-chromium, beta-titanium, stainless steel wires were measured under non-angulated dry, angulated dry, non-angulated saliva, angulated saliva conditions. The results were as follows: 1. Stainless steel wires showed lower friction values in non-angulated dry condition, and heat-treated cobalt-chromium wires showed higher friction values in angulated dry condition. Higher friction values were showed in order of cobalt-chromium. stainless steel, heat-treated cobalt-chromium and beta-titanium wires in non-angulated saliva condition. and were showed in order of stainless steel, cobalt-chromium, heat-treated cobalt-chromium, beta-titanium wires in angulated saliva condition. 2. Angulation increased friction for stainless steel wires under dry condition. 3. Artificial saliva decreased friction for cobalt-chromium wires and increased friction for stainless steel wires under non-angulated condition. 4. Artificial saliva decreased friction for all wires except beta-titanium wires under angulated condition. 5. Regardless of angulation or environment. heat-treated cobalt-chromium and beta-titanium wires showed higher friction values, and stainless steel wires showed lower friction values.

• 대한치과보철학회지
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• 제34권3호
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• pp.475-488
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• 1996

The opaque porcelain layer of porcelain-fused-to-metal(PFM) restoration is critical for the success of PFM restoration because it is the first layer placed over the treated alloy. But, the methods of opaquing technique have not been confirmed. Usually, the one layer method and two layer method have been used for the application of opaque porcelain. In the past, alloys with porcelain veneers which have been used successfully have contained various precious metals. Recent increase in the cost of precious metals stimulates considerable interest in nonprecious alloys. Although nickel-chromium alloys and nickel-chromium-beryllium alloys have been widely used, the use of cobalt-chromium alloys would be gradually increased with elimination of any potential risk of nickel-related allergic responses and/or beryllium-related toxic responses. This investigation examined one- and two-layer opaque porcelain applications to determine the effect on the bond strength of titanium added cobalt-chromium metal ceramic alloy. Bond strength of Ceramco II porcelain to titanium added cobalt-chromium alloy(2Dentitan) and gold-platinum-palladium alloy(Degudent H) were evaluated by direct shear bond strength test with Instron universal testing machine. The results were as follows; 1. When the mean shear bond strength of each experimental group were compared in $0.25cm^2$ unit area, the titanium added cobalt-chromium alloy/two layer method exhibited the greatest strength(79.7kg), followed by titanium added cobalt-chromium alloy/one layer method(76.2kg), gold-platinum-palladium alloy/two layer method(71.4kg), gold-platinum-palladium alloy/one layer method(64.2kg). 2. No significant differences in bond strength were recorded between the two opaquing techniques for gold-platinum-palladium alloy and titanium added cobalt-chromium alloy. 3. No significant differences in bond strength were recorded between the gold-platinum-palladium alloy and the titanium added cobalt-chromium alloy.

• 대한치과보철학회지
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• 제38권2호
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• pp.160-168
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• 2000

This study evaluated the effects of four adhesive metal primers on the shear bond strength of a heat curing denture base resin(Lucitone 199) to cobalt-chromium alloy(Biosil-f). The adhesive metal primers were Cesead Opaque Primer, Metal Primer, MR Bond, and Super-Bond liquid. The metal surface primed or nonprimed was filled with the heat-curing methyl methacrylate resin. The specimens were stored in water at $37^{\circ}C$ for 24 hours and the alternately immersed in water bath at $5^{\circ}C\;and\;55^{\circ}C$ for up to 2,000 thermal cycles. Shear bond strengths were measured using UTM at a crosshead speed of 0.5mm/min. Failure surface were examined under magnifying glasses. All the primers examined improved the shear bond strength between denture base resin and cobalt-chromium alloy compared with nonprimed specimens before thermal cycling. The bond strength of Cesead Opaque Primer was greatest. And after 2,000 thermal cycles, the bond strengths between resin and cobalt-chromium alloy were decreased but the difference between thermal cycling 0 and 2,000 at Cesead Opaque primer and Metal Primer were not significant. This study indicated that Cesead Opaque Primer & Metal Primer is effective primers to obtain higher bond strength between heat cured denture base resin and cobalt-chromium alloy.

• 대한치과기공학회지
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• 제32권3호
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• pp.195-207
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• 2010

Purpose: The purpose of this study was to observe the microstructural changes of surface in the specimens, performing the shear bond strength testing. The currently most used non-precious alloys are nickel-chromium based alloys with or without beryllium. However, their biocompatibility has been questioned concerning possible damages to the health of the patient and professionals involved in the fabrication of prosthesis caused by long exposure to Ni and Be. An option to nickel-chromium alloys is the cobalt-chromium alloy, an alternative that does not sacrifice the physical properties of the metal porcelain systems. Studies in the animals substantially show that the cobalt-chromium alloys are relatively well tolerated, being therefore more biocompatible than the nickel-chromium alloys. Methods: Non-addition Be to nickel-chromium based alloy(Bellabond plus) and cobalt-chromium alloy which has been widely used(Wirobond C) fused with ZEO light porcelain classified control group and cobalt-chromium alloy which is developing alloy of Alphadent company in Korea(Alphadent alloy) fused with ZEO light porcelain classified experimental group. The specimens of $4mm{\times}4mm{\times}0.5mm$ were prepared as-cast and as-opaque to cast body to analyze the mechanical characteristic change, the microstructure of alloy surface. The phase change was used to observe through XRD analysis and OM/SEM was used to observe the surface of specimens as-cast and as-opaque to cast body. Chemical formation of their elements was measured with EDS. Then hardness was measured with Micro Vicker's hardness tester. Shear bond strength test thirty specimens of $10mm{\times}10mm{\times}2mm$ was prepared, veneered, 3mm high and 3mm in diameter, over the alloy specimens. The shear bond strength test was performed in a universal testing machine(UTM) with a cross head speed of 0.5mm/min. Ultimate shear bond strength data were analyzed with one-way ANOVA and the Scheffe's test (P<0.05). Within the limits of this study, the following conclusions were drawn: The X-ray diffraction analysis results for the as-cast and as-opaque specimens showed that the major relative intensity of Bellabond plus alloy were changed smaller than Wirobond C and Alphadent Co-Cr based alloys. Results: Microstructural analysis results for the opaque specimens showed all the alloys increased carbides and precipitation(PPT). Alphadent Co-Cr based alloy showed the carbides of lamellar type. The Vickers hardness results for the opaque specimens showed Wirobond C and Alphadent Co-Cr based alloys were increaser than before ascast, but Bellabond plus alloy relatively decreased. The mean shear bond strengths (MPa) were: 33.11 for Wirobond C/ZEO light; 25.00 for Alphadent Co-Cr alloy/ZEO light; 18.02 for Bellabond plus/ZEO light. Conclusion: The mean shear bond strengths for Co-Cr and Ni-Cr based alloy were significantly different. But the all groups showed metal-metal oxide modes in shear bond strengths test at the interface.

• The Journal of Advanced Prosthodontics
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• 제9권2호
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• pp.124-129
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• 2017

PURPOSE. This study evaluated the effect of span length on the adaptation of implant-supported cobalt chromium frameworks fabricated by three techniques. MATERIALS AND METHODS. Models with two solid abutment analogs at different inter-abutment distances were digitized using a laboratory scanner. Frameworks of two-, three-, and four-unit fixed prostheses were designed by a computer. Six dots with a diameter of 0.2 mm were preset on the surface of each framework. A total of 54 implant-supported cobalt chromium frameworks were fabricated by milling, selective laser melting (SLM), and cast techniques. The frameworks were scanned and exported as Stereolithography files. Distances between two dots in X, Y, and Z coordinates were measured in both the designed and fabricated frameworks. Marginal gaps between the framework and the abutments were also evaluated by impression replica method. RESULTS. In terms of distance measurement, significant differences were found between three- and four-unit frameworks, as well as between two- and four-unit frameworks prepared by milling technique (P<.05). Significant differences were also noted between two- and three-unit frameworks, as well as between two- and four-unit frameworks prepared by cast technique (P<.05). The milling technique presented smaller differences than the SLM technique, and the SLM technique showed smaller differences than the cast technique at any unit prostheses (P<.05). Evaluation with the impression replica method indicated significant differences among the span lengths for any fabrication method (P<.05), as well as among the fabrication methods at any unit prostheses (P<.05). CONCLUSION. The adaptation of implant-supported cobalt chromium frameworks was affected by the span length and fabrication method.

• 대한치과보철학회지
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• 제35권1호
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• pp.78-94
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• 1997

The purpose of this experiment was to determine the effects of various treatments on denture base resin to metal bond for cobalt-chromium alloy. The metal surface was treated as follows. Group 1 : Sandblasted with $50{\mu}m$ aluminum oxide. Group 2 : Sandblasted with $250{\mu}m$ aluminum oxide. Group 3 : Sandblasted with $250{\mu}m$ aluminum oxide and followed by silicoating. Group 4 : Electrochemically etched. Group 5 : treated with oxidizing solution. Group 6 : Beaded with $200{\mu}m$ retention structure and followed by silicoating. All specimens were applied with 4-META resin and were thermocycled 1000 times at temperature of $5^{\circ}C$ to $55^{\circ}C$. The effects of various surface treatments on the bond strength between 4-META resin and metal interface were measured by using the universal testing machine. All specimens were observed with SEM. The results were as follows 1. The bond strength of 4-META resin were significantly higher to Co-Cr alloy. 2. The bond strength decreased in the following orders : group 6, group 3, groups 1 and 2, group 4, group 5 and there was no statistically significant difference in bond strength among groups 1 and 2.(p>0.05) 3. The bond strength of cobalt-chromium alloy to 4-META resin were not significantly different.(p>0.05) 4. The treated surface of groups 1, 2 and 3 has more fine undercut than that of groups 4 and 5 with SEM. 5. Stable adhesion can be achieved when mechanically roughened metal surface by sandblasting than treating in an electrochemical etching and an oxidizing solution with potassium manganate.

• 대한치과기공학회지
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• 제40권2호
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• pp.63-69
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• 2018

Purpose: The purpose of this study is to investigate the non-precious metal core materials used in the dental laboratory to fabricate the implant superstructure by CAD / CAM method. And to observe and compare the morphology and distribution of the osteoblasts in relation to implant osseointegration. Methods: In this study, the mandibular right first molar tooth model was selected as an international standard to produce a single core. Using this model, the impression was made with the silicone rubber, the tooth model was scanned, and a single core was designed and 5-axis milling was performed. The materials used were Cobalt-Chromium and Nickel-Chromium, and the cores for dental implant top structures were fabricated according to the procedures of the dental labs. After the fabrication, the marginal area of the core was separated and cell culture experiment was performed. The osteoblast cells used MC3T3-E1, which is currently widely used. For morphological analysis of osteoblasts, cells were posttreated and observed using CLSM (Confocal Laser Scanning Microscope) and compared. Results: The cell adhesion behavior of the specimen surface measured by CLSM was uniformly distributed in specimen A (Cobalt-Chromium) than in specimen B (Nickel-Chromium). The distribution and changes of the cells were different in the two specimens. Conclusion : It is possible to confirm that specimen A (Cobalt-Chromium) is suitable for the living body through adhesion and proliferation of osteoblasts related to implant osseointegration in the non-precious metal superstructure used after implantation. It is considered that it is preferable to use Co-Cr when fabricating the superstructure.

• 대한치과보철학회지
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• 제32권2호
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• pp.249-267
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• 1994

The purpose of this study was to compare the fatigue, physical properties, flexibility and surface roughness of titanium used in removable partial dentures with those of a type IV and alloy and a cobalt- chromium alloy. Fatigue testing subjected the test specimen to rapid cycling at a given stress until failure occurred by using a small-sized, electrodynamic type bending fatigue testing machine. The S-N curves for the framework materials were generated. For tensile testing, a tensile bar as described in the ADA Specification No.14 was subjected to tensile loading until failure occurred. Load-displacement curves were generated for 18 gauge round specimen and tapered half round specimen. Then the flexibilities were calculated. The surface roughnesses were compared by analyzer. Through analyses of the data, the following conclusions were obtained. 1. The fatigue property of titanium was higher than that of a type IV gold alloy$(p\leq0.05)$, but there was no significant difference between titanium and a cobalt-chromium alloy $(p\geq0.05)$. 2. The yield strength, the ultimate tensile strength and Victors hardness of titanium were higher than those of a type IV gold alloy but lower than those of a coalt-chromium alloy$(p\leq0.05)$. 3. The percentage of elongation and reduction of area of titanium were the highest $(p\leq0.05)$. 4. The surface roughness of titanium was the greatest$(p\leq0.05)$. 5. The flexibility of titanium was lower than that of a type IV gold alloy but higher than that of a cobalt-chromium alloy$(p\leq0.05)$.

• 대한치과보철학회지
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• 제9권1호
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• pp.91-99
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• 1969

• 대한치과의사협회지
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• 제12권9호
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• pp.667-677
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• 1974

A testing machine was devised and constructed for the purpose of measuring the retentive forces of maxillary complete denture bases in subjects. Forth complete denture bases were made for ten subjects with three different denture base materials, following the usual denture construction technique. Retentive forces of the forty dentures were determined at seven locations. The tests on each base were repeated three times at intervals of 5 minutes. Differences in retention values were evaluated statistically. 1) Differences in retention values were found by the differences of the denture base materials, but acrylic resin was similar to chromium cobalt alloy. 2) The chromium cobalt alloy and acrylic resin bases from master models revealed the best retention values, the gold alloy base from master model was the poor second and the acrylic resin base from snap model was the third. 3) The retention values for hook-1 revealed higher than that for hook-2 and the retention values for hook-3 revealed the lowest value.