• 제목/요약/키워드: Coating solution

Search Result 1,322, Processing Time 0.03 seconds

Effects of Coating Conditions on the Thickness and Morphology of Alumina- or Carbon-Coated Layers on SiC Whiskers (알루미나 또는 카본 코팅 SiC 휘스커의 코팅층 두께 및 형상에 미치는 코팅조건의 영향)

  • 배인경;장병국;조원승;최상욱
    • Journal of the Korean Ceramic Society
    • /
    • v.36 no.5
    • /
    • pp.513-520
    • /
    • 1999
  • Alumina-coated SiC whiskers wee prepared by the calcination (1150$^{\circ}C$, 1h, Ar) of the alumina hydrate layer which was precipitated homogeneously on whisker surface from a solution of Al2(SO4)3 and urea as a precipitant. In addition carbon coated SiC whiskers were prepared by the pyrolysis (1000$^{\circ}C$, 4h Ar) of phenolic resin coated whisker. The effects of coating conditions on the thickness and morphology of the coated layers were examined by SEM and TEM. It was found that Al2O3-coating layers become thinner and more uniform with decreasing the Al2(SO4)3 concentration. Thin (0.075-0.1$\mu\textrm{m}$) and uniformly alumina-coating layers were obtained at the Al2(SO4)3 concentration 0.010mol/l. On the other han carbon-coating layers were uniform but very thin (5-16 nm) in thickness. For thicker carbon-coating layers ethanol as a disperse medium was found to be more efficient compared tousing acetone.

  • PDF

Protein-Coating Evaluation Method of Colloidal Gold Nanoparticles (콜로이드 골드 나노입자의 단백질 수송성 평가법)

  • Kim, Mi-Young;Noh, Sang-Myoung;Kim, Jung-Mogg;Choi, Han-Gon;Kim, Jung-Ae;Oh, Yu-Kyoung
    • Journal of Pharmaceutical Investigation
    • /
    • v.34 no.6
    • /
    • pp.465-469
    • /
    • 2004
  • Colloidal gold nanoparticles might be of use as nano scale delivery systems of various therapeutic materials in the future. Recent studies have reported the feasibility of colloidal gold nanoparticles as gene delivery systems or protein delivery systems. In this study, we aimed to develop a short-step method useful for screening the optimal coating conditions of colloidal gold nanoparticles with proteins. We observed that colloidal gold nanoparticles have properties of changing its unique color when they were exposed to NaCl solution. Taking advantage of the color changing properties of colloidal gold nanoparticles, we applied the color testing method of colloidal gold nanoparticles solutions for evaluating the protein coating nature. Using bovine serum albumin as a model protein, we tested the protein coating of colloidal gold nanoparticles via the color change upon NaCl addition. The optimal coating concentration and coating conditions of colloidal gold nanoparticles with bovine serum albumin were fixed using the color testing methods. We suggest that the color testing method might be applied to optimize the coating condition of colloidal gold nanoparticles with other therapeutic proteins.

Coating of ZnS phosphor by $SiO_2$ sol-gel

  • Lee, You-Hui;Han, Sang-Do;Han, Chi-Hwan;Yang, Hua;Singh, Ishwa
    • 한국정보디스플레이학회:학술대회논문집
    • /
    • 2004.08a
    • /
    • pp.719-723
    • /
    • 2004
  • Silica coating on ZnS particles with buffer solution has been investigated. Diluted sodium silicate in water was used as the precursor material and it was diluted in water. Sodium silicate was added drop-wise in the continuously stirred suspension of ZnS in the buffer solution at room temperature. Smooth and evenly distributed silica coated ZnS phosphors has been obtained when the pH of buffer solution was 10, the concentration of sodium silicate in water was 20 wt%, firing temperature was 500 $^{\circ}C$.

  • PDF

Effect of Electrolyte Concentration on Water Permeation in Protective Coatings (방식도막에 있어서 물의 침투에 대한 전해질 용액의 영향)

  • 박진환
    • Journal of the Korean Society of Safety
    • /
    • v.13 no.4
    • /
    • pp.206-212
    • /
    • 1998
  • The water permeation in protective coatings, which may greatly influence the corrosion protective property of these coatings, was studied using the electrochemical impedance spectroscopy technique. During the absorption of water in protective coatings immersed in electrolyte solution, the change of coating capacitance with concentration of electrolyte was determined from impedance measurements. When water absorption or desorption of coatings occured by exposing the coatings to electrolyte solutions of different concentration, increase in impedance caused by desorption of water was found to be higher in the case of thicker film. The amount of water absorbed in coatings changed with concentration of electrolyte. The water taken up in coatings from the solution of lower electrolyte concentration was deserted by contact with the solution of higher concentration. The uptake of water in protective coatings varied depending on the type of coating ingredient especially binder.

  • PDF

Hydration of Granulated Blast Furnace Slag in the Presence of NaOH (NaOH 자극에 의한 고노수쇄 슬래그의 수화반응)

  • 송종택;대문정기(大門正機);근등련일(近藤連一)
    • Journal of the Korean Ceramic Society
    • /
    • v.17 no.3
    • /
    • pp.158-162
    • /
    • 1980
  • The experiments of suspension hydration were performed in the mixtures of slag and water or NaOH solutions which were made up with a liquid/solid ratio of 10. The liquid phase of the suspension was chemically analysed and discussed. When slag was in contact with water, CaO component was released from slag grains into the solution. The amounts of $SiO_2$ and $Al_2O_3$ liberated in the solution were very low as compared with CaO, for the impermeable coating of $SiO_2$, $Al_2O_3$-rich gel was formed on the surface of slag grains. The hydration was considered to be inhibited by this impermeable coating. The weak hydraulic property of slag was based on slowly released CaO and dissolved Na, K components which increased pH in the solution.

  • PDF

Development of Higher Functional Coating Agents for Pulp Mold (III) Manufacture of starch derivatives for coating - (펄프몰드용 새로운 고기능 코팅제 제조기술개발(제3보) -코팅용 전분유도체 제조-)

  • Kang Jin Ha;Lim Hyun A
    • Journal of Korea Technical Association of The Pulp and Paper Industry
    • /
    • v.36 no.4 s.107
    • /
    • pp.49-59
    • /
    • 2004
  • This study was carried out to obtain the basic data for producing higher functional coating agents for pulp mold by evaluating various kinds of starch derivatives. At that time, four kinds of starch derivatives were manufactured for making coating agents respectively. Physical properties of coated paperboards were tested. Conclusions obtained from this results were as follows. The water and oil resistance of hydroxypropylated, cyanoethylated and carboxymethy­lated starch were high when degree of molar substitution(DS) of propylene oxide, acrylonitrile and sodium monochloroacetate were 0.18, 0.07 and 0.009, respectively. Also, the those of crosslinked starch were high when degree of crosslinking of epichlorohydrin was 0.02. Consequently, $8\%$ solution of carboxymethylated starch made with DS 0.009 of monochloroacetate was the best among coating agents from starch derivatives men­tioned above.

Extending Shelf-life of Rice Cake Using Coating Agent Containing Soy Protein Isolate (찹쌀떡의 보존기간 연장을 위한 대두단백질 코팅제의 특성)

  • 박상규;조지미;이유석;이종욱
    • Food Science and Preservation
    • /
    • v.8 no.2
    • /
    • pp.181-186
    • /
    • 2001
  • The objective of this study is to determine the effect of soy protein isolate (SPI) film coating on the color, firmness, viscosity and weight loss of Rice Cake stored at 15, 20 and $25^{\circ}C$ (RH 50%) for 30 days. Raw materials mixed with SPI and cocoa powder (10:0, 7:3, 5:5, 3:7, w/w) were prepared. After adding sugar and shortening to raw materials, the mixture were refined to 25 micron of particle size. Coating of Rice Cake were carried out at $65^{\circ}C$. SPI coated Rice Cake had higher internal and external firmness comparing to the control at $25^{\circ}C$. SPI coated Rice Cake showed smooth surface morphology and had 0.71-1.01 mm of thickness. SPI coated Rice Cake showed less weight loss for 30 days compared to controls. SPI coating solution was successfully coated on Rice Cake and extended shelf-life over 15 days at room temperature.

  • PDF

Derivation of Cubic and Hexagonal Mesoporous Silica Films by Spin-coating

  • Pan, Jia-Hong;Lee, Wan-In
    • Bulletin of the Korean Chemical Society
    • /
    • v.26 no.3
    • /
    • pp.418-422
    • /
    • 2005
  • By introducing spin-coating method to the evaporation induced self-assembly (EISA) process, a simple and reproducible route in controlling the mesophase of silica thin films has been developed for the first time in this work. When a comparatively solvent-rich Si-sol (The atomic ratio of TEOS : F127 : HCl : $H_2O$ : EtOH = 1 : 0.006 : 0.2 : 9.2 : 30) was used as coating solution, the mesophase of resultant silica films was selectively controlled by adjusting the spin-on speed. The cubic mesophase has been obtained from the coating at a low rpm, such as 600 rpm, while the 2-D hexagonal mesophase is formed at a high rpm, such as 2,500 rpm. At a medium coating speed, a mixture of cubic and hexagonal mesophase has been found in the fabricated films. The present results confirm that the evaporation rate of volatile components at initial step is critical for the determination of mesopore structures during the EISA process.

Study of Ni-coating on 316L Stainless Steel by Pulse Electroplating in Various Bath Conditions at Room Temperature (실온 펄스도금법을 이용한 STS 316L 표면의 Ni 도금 저가형욕 연구)

  • 정세진;조계현
    • Journal of the Korean institute of surface engineering
    • /
    • v.35 no.1
    • /
    • pp.53-63
    • /
    • 2002
  • Ni coating was carried out by pulse plating at room temperature. So, experimental conditions for Ni-coating were based on Watt's bath, and new additives(propionic acid) were introduced in the Watt's bath electrolyte as $H_3$$BO_3$ alternatives. By adding propionic acid, coating layer demonstrated a good adhesion and uniformity without special pre-treatment of the 316L stainless steel at room temperature. With a decrease of amount of propionic acid and applied average current density, cathode current efficiency increased. Also, edge effect was decreased with decreasing a peak current and increasing a pulse frequency in the same bath condition. It was found that the optimum condition for Ni coating was a current density of 10~20mA/$\textrm{cm}^2$ at below 500 mA peak current in the $5m\ell/\ell$ propionic acid solution.

Effect of Inlet Air Temperature and Atomizing Pressure on Fluidized Bed Coating Efficiency of Broken Peanut (흡입공기온도와 분무압력이 분쇄땅콩의 유동층 코팅효율에 미치는 영향)

  • Kang, Hyun-Ah;Shin, Myung-Gon
    • Korean Journal of Food Science and Technology
    • /
    • v.34 no.5
    • /
    • pp.924-926
    • /
    • 2002
  • The effects of inlet air temperature and atomizing pressure on the coating efficiency were evaluated using peanuts. Broken peanut pieces were coated with dextrin and sodium caseinate solution by a fluidized bed coater. The coating efficiency was significantly influenced by inlet air temperature and atomizing pressure, with the optimal efficiency achieved at $70^{\circ}C$ and 3 bar, respectively. The coating material consisting of dextrin and sodium caseinate could be used for preventing rancidity of broken peanut.