• Title/Summary/Keyword: Coating Time

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The Influence of Process Variables on the Thin Film Growth of Metal-Halide Perovskites by the Solution Shear Coating (전단코팅 공정으로 제조하는 금속-할라이드계 페로브스카이트의 박막성장에 미치는 공정변수의 영향 고찰)

  • Choe, Jihye;Song, Jiho;Jeong, Jiyoung;Chung, Choong-Heui;Kim, Jaekyun;Hong, Ki-Ha
    • Journal of the Korean institute of surface engineering
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    • v.52 no.1
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    • pp.6-15
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    • 2019
  • Metal-halide perovskite (MHP) solar cell is a promising candidate for next-generation flexible devices and the BIPV (Building-integrated photovoltaics) because it can exhibit high power conversion efficiencies over 23%, good bendability and low processing cost. However, MHP solar cells are commonly fabricated by the spin coating that is not a reliable method to produce large-scale commercial solar cells. A shear coating can be one of the potential candidates for the large-scale deposition method of MHP films. In this work, the influences of the process parameters such as solvents of precursor solution, substrate temperature, concentrations of precursor solution, and annealing time on the thin film growth of MHP were investigated for the shear coating process. This study presents the possibility of the shear coating process for large-scaled perovskite film fabrication and reveals the role of process condition in the thin film growth of perovskites.

Performance of Membrane Electrode Assembly for DMFC Prepared by Bar-Coating Method (Bar-Coating 방법으로 제조한 직접메탄올 연료전지 MEA의 성능)

  • Kang, Se-Goo;Park, Young-Chul;Kim, Sang-Kyung;Lim, Seong-Yop;Jung, Doo-Hwan;Jang, Jae-Hyuk;Peck, Dong-Hyun
    • Journal of the Korean Electrochemical Society
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    • v.11 no.1
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    • pp.16-21
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    • 2008
  • The key component of a direct methanol fuel cell (DMFC) is the membrane electrode assembly (MEA), which comprises a polymer electrolyte membrane and catalyst layers (anode and cathode electrode). Generally the catalyst layer is coated on the porous electrode supporter (e.g. carbon paper or cloth) using various coating methods such as brushing, decal transfer, spray coating and screen printing methods. However, these methods were disadvantageous in terms of the uniformity of catalyst layer thickness, catalyst loss, and coating time. In this work, we used bar-coating method which can prepare the catalyst layer with uniform thickness for MEA of DMFC. The surface and cross-section morphologies of the catalyst layers were observed by SEM. The performances and resistance of the MEAs were investigated through a single cell evaluation and impedance analyzer.

Effects of Polymer Coating on Seed Vigour in Rice (벼 종자의 Polymer 피복처리가 종자세에 미치는 영향)

  • 이성춘;정춘화;김진희;송동석
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.41 no.3
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    • pp.274-285
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    • 1996
  • These experiments were conducted to evaluate the effects of seed coating with ten environmentally acceptable polymers, on germination percentage, water uptake, respiration, emergence and seedling growth characteristics. The water absorption of polymer-coated seeds in saturation condition was highest in klucel and lowest in polyvinyl pyrrolidone(PVP), and that in water was highest in klucel and lowest in maltrin. Respiration rates of polymer-coated seeds in Hwayoungbyeo and Ilpumbyeo were lower than those of none-coated seeds, and those in Daecheongbyeo and Jinmibyeo were higher than that of none-coated seeds, and those of sepiret coated seeds were higher than PVP coated seeds. The germination polimer-coated seed was reduced by one percentage by coating with seed coating machine. Germination percentage was not affected by any of polymer coating in high quality seed, but there were significant effects in low quality seed coating with waterlock, surelease 46 and sepiret significantly reduced germination some cultivars. Germination percentage after accelated ageing treatment were slightly higher most of polymer-coated seeds than in none-coated seeds, but those of sepiret-and klucel-coated seeds were lower significantly. Germination percentage of seeds coated with daran 8600, rnaltrin, sacrust and opadry were enhanced slightly under cold test other polimers reduced germination. The seedling height of polymer-coated seeds were longer than those of none-coated seeds, but those of waterlock, PVP and maltrin coating seeds were shorter, seedling hight was shortened by polimer coating under cold test. Polymer-coated seeds showed higher emergence percentage, shorter emergence time in field condition. The highest emergence percentage and the shortest emergence time was shown at 90% soil moisture content.

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Evaluation of the Wear Resistance of PVD Coatings on Drills by Using a Slurry Jet Impact Test

  • Iwai, Y.;Ueno, Y.;Suehiro, T.;Honda, T.;Hogmark, S.
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2002.10b
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    • pp.141-142
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    • 2002
  • In this paper, we propose a slurry jet (water containing $1\;{\mu}m$ alumina particles) impact test in order to quickly evaluate the wear properties of physical vapor deposited (PVD) coatings on commercial cutting tools. Linear wear was obtained for bothe coating and substrate material, and the penetration through the coating into the substrate was signified by a sharp increase in slope of the wear versus time curve. The PVD coatings deposited on the tools showed the same wear rates as those on reference plate specimens produced by the same coating methods. We conclude that our proposed evaluation technique for coatings is considerably useful as a screening test when evaluating coated tools like twist drills, taps, end mills, gear hobs, etc.

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Influence of LPPS Spraying Parameters on Deposition Efficiency of Zirconia Powder

  • Shi, Jian-Min;Hu, Zhong-Yin;Huang, Jing-Qi;Ding, Chuan-Xian
    • Journal of the Korean Vacuum Society
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    • v.6 no.S1
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    • pp.160-165
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    • 1997
  • Yttria stabilized zirconia coating is an attractive material for several engineering applications. In order to produce coatings with consistent and reliable performance it is important to understand the influence of spraying parameters on the coating properties and optimize the spraying parameters. In this paper the low pressure plasma spray(LPPS) deposition of as-received zirconia powder has been investigated using simple one-factor-at-a-time approach. The deposition efficiency was chosen to evaluate the melting characteristics of the as-received zirconia powder. The results obtained indicated that the deposition efficiency of zirconia powder is very sensitive to the spraying parameters such as plasma gas flow rate and ranges from 24% to 57% The microstructure and the phase composition of zirconia coating deposited with the different plasma spraying parameters were also examined by SEM and XRD respectively. The relationship between deposition efficiency and the microstructure of zirconia coating was discussed.

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A Study on the Contact Stress Analysis of the Coating Layer Using Finite Element Method (유한요소법을 이용한 Coating Layer의 접촉응력 해석에 관한 연구)

  • 김청균;오병택
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1996.10a
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    • pp.183-188
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    • 1996
  • Films and coatings are used for an enormous and diverse set of applications including mechanical, electronic and optical devices, protection at high temperature, cutting tools enhancement and automotive use. Many of these applications require the various properties associated with inorganic and metallic / non-metallic materials; i.e., with ceramics. Therefore, a large number of coatings have been developed and used for a long time in the various fields, especially in mechanical one. As one of the mutual surface actions, the problems of contact stresses are complex. The relationship between load and stress are nonlinear. Besides, the material is often apt to deform plastically under low load. However, analytical solutions exist only for some simple problems. If a material has a complicated shape or inhomogeneous properties, numerical method must be used. In this paper, the analysis of the contact stress of the coating layer was solved, using the finite element method.

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Oxidation Resistance of Al Diffusion Coating Layer on TiAl (TiAl합금의 Al 피복시 Al확산 피복층의 내고온산화성)

  • Lee, C.H.;Choe, J.I.
    • Journal of the Korean Society for Heat Treatment
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    • v.10 no.2
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    • pp.150-156
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    • 1997
  • The effect of variation of pack activators, compositions, temperature and time on the thickness and structure of aluminide coatings formed on the TiAl alloy was studied in one-step packs and two-step packs containing aluminum for the purpose of improvement of oxidation resistance. The thickness of coating layer was increased with increasing $NH_4Cl$ content up to 3wt% and then it was saturated. Oxidation resistance of coating layers carried out at one step pack was superior to that of ones through of two step pack. The improvement of high temperature oxidation resistance was due to the formation of a protective $Al_2O_3$ surface layers and coating the alloys with $TiAl_3$ phase.

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Development of Post-process for Improving the Surface Roughness of Stereolithography parts - Using Wax Coating and Grinding Post-process - (RP part 표면정도 향상을 위한 후처리 공정 개발 -왁스 코팅과 연삭 후처리 공정 이용-)

  • 안대건;김호찬;최홍태;이석희
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2002.10a
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    • pp.659-662
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    • 2002
  • SL(Stereolithography) part is made by piling up thin layers which causes the stair stepping effect at the surface of SL parts. This effect brings about excessive surface roughness and requires additional post-process finishing such as abrasive techniques that are detrimental to part geometry and time consuming. Hence a wax coating and grinding post-process is proposed to improve the surface quality of SL part. The wax that has suitable properties for the proposed post-process is coated all over the part surface. By grinding the thin layer of coated on the SL part only, the surface roughness can be improved without any damage on the part. From the experimental results, This approach is considered to be very practical fur die casting with RT(Rapid Tooling) techniques.

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Moist Corrosion and Surface Protection of YBCO HTS

  • Lim, Byong-Jae;Soh, Dea-Wha;Fan, Zhanguo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.11a
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    • pp.256-259
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    • 2002
  • The critical currents of sintered $YBa_{2}Cu_{3}O_{6.5+\delta}$ were measured as the variables with the corrosive time in the humid air. The corrosive process was studied by means of the current changes. Ag coating on the textured YBCO and polytetrafluoroethylene (PTFE) coating on the sintered YBCO were prepared. The critical current densities of different YBCO samples with and without coatings were compared. Both Ag coating and PTFE coating can well protect YBCO from moisture and $CO_{2}$.

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Optimization of Plasma Spray Coating Parameters of Alumina Ceramic by Taguchi Experimental Method (실험계획법에 의한 알루미나 세라믹의 플라즈마 용사코팅 최적화)

  • 이형근;김대훈;윤충섭
    • Journal of Welding and Joining
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    • v.18 no.6
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    • pp.96-101
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    • 2000
  • Sintered alumina ceramic substrate has been used for the insulating substrate for thick Hybrid IC owing to its cheapness and good insulating properties. Some of thick HIC's are important to eliminate the heat emitted from the parts that are mounted on the ceramic substrate. Sintered ceramic substrate can not transfer and emit the heat efficiently. It's been tried to do plasma spray coating of alumina ceramic on the metal substrates that have a good heat emission property. The most important properties to commercialize this ceramic coated metal substrate are surface roughness and deposition efficiency. In this study, plasma spray coating parameters are optimized to minimize the surface roughness and to maximize the deposition efficiency using Taguchi experimental method. By this optimization, the deposition efficiency was greatly improved from 35% at the frist time to 75% finally.

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