• 제목/요약/키워드: Coated layer

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천연왁스를 이용한 화장품 첨가용 비타민 C의 코팅 (Coating of Vitamin C Using Natural Wax as a Cosmetic Additive)

  • 김복희;김동만;이상화;신현재
    • KSBB Journal
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    • 제27권5호
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    • pp.319-323
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    • 2012
  • Vitamin C or L-ascorbic acid, an essential nutrient for humans with antioxidative property, was coated with natural wax to be used as functional additives for cosmetics. Coating of vitamin C was performed using carnauba wax and olive wax in self-designed reaction chamber for 60 min. The yield of coated vitamin C with carnawuba wax and olive wax were up to $94.6{\pm}1.2%$ and $82.5{\pm}1.4%$, respectively. The stability of the carnauba wax-coated vitamin C in the lotion was improved 17.8% than that of uncoated vitamin C during 30 day storage at $25^{\circ}C$. Color and the layer separation of the lotion added with the coated vitamin C showed better property than with the uncoated vitamin C. The coated vitamin C can be applied to cosmetic ingredients as a stable additive.

RABiTS와 PLD를 이용한 YBCO coated conductor 제조 (Manufacturing of YBCO coated conductor using RABiTS as the texture template and pulsed laser for the multi-layer oxide film deposition)

  • 박찬;고락길;신기철;송규정;정준기;;유상임;염도준
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2003년도 하계학술대회 논문집 Vol.4 No.1
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    • pp.104-106
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    • 2003
  • 다층의 산화물 박막으로 이루어진 coated conductor의 제조를 위하여 각층의 증착조건이 최적화되어야 한다. 가공/열처리를 통하여 2축배향성을 가지는 Ni 금속 기판위에 $Y_2O_3$, YSZ, $CeO_2$ 등의 산화물 완충층을 증착한 후 초전도층인 YBCO를 증착하였다. 12도와 8도의 in-plane fwhm (full width at half maximum)과 out-of-plane fwhm을 가지는 Ni 기판을 이용하여 13도와 4.5도의 in-plane 및 out-of-plane fwhm을 가지는 YBCO coated conductor를 제조하였다. 임계온도 (Tc), 임계전류 (Ic), 및 임계전류밀도 (Jc) 는 각각 84K, 3.3A, 및 $310,000\;A/cm^2$ 이었다.

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알루미나 또는 카본 코팅 SiC 휘스커의 코팅층 두께 및 형상에 미치는 코팅조건의 영향 (Effects of Coating Conditions on the Thickness and Morphology of Alumina- or Carbon-Coated Layers on SiC Whiskers)

  • 배인경;장병국;조원승;최상욱
    • 한국세라믹학회지
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    • 제36권5호
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    • pp.513-520
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    • 1999
  • Alumina-coated SiC whiskers wee prepared by the calcination (1150$^{\circ}C$, 1h, Ar) of the alumina hydrate layer which was precipitated homogeneously on whisker surface from a solution of Al2(SO4)3 and urea as a precipitant. In addition carbon coated SiC whiskers were prepared by the pyrolysis (1000$^{\circ}C$, 4h Ar) of phenolic resin coated whisker. The effects of coating conditions on the thickness and morphology of the coated layers were examined by SEM and TEM. It was found that Al2O3-coating layers become thinner and more uniform with decreasing the Al2(SO4)3 concentration. Thin (0.075-0.1$\mu\textrm{m}$) and uniformly alumina-coating layers were obtained at the Al2(SO4)3 concentration 0.010mol/l. On the other han carbon-coating layers were uniform but very thin (5-16 nm) in thickness. For thicker carbon-coating layers ethanol as a disperse medium was found to be more efficient compared tousing acetone.

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저온소결 세라믹기판용 Cordierite계 결정화유리의 합성 및 특성조사에 관한 연구;(IV) Sol-Gel법으로 코팅한 Cu분말을 이용한 Metallizing (Synthesis and Characterization of Cordierite Glass-Ceramics for Low Firing Temperature Substrate; (IV) Metallizing by Using Cu Powder Coated by Sol-Gel Method)

  • 김병호;문성훈;이근헌;임대순
    • 한국세라믹학회지
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    • 제31권4호
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    • pp.427-435
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    • 1994
  • Cu-metallized low firing temperature substrates were synthesized by cofiring green sheet of cordierite-based glass with Cu. By Sol-Gel method, Cu powder was coated with borosilicate gel which should act as a glass frit in Cu paste during cofiring. Theoretical weight ratios of Glass/Cu were controlled to be 2.5, 5, 10 and 15% by varying alkoxide concentrations. Average particle size of coated Cu was 0.629~0.674 ${\mu}{\textrm}{m}$ in comparison to that of as-received Cu(0.596 ${\mu}{\textrm}{m}$), which increased with alkoxide concentration but did not increase above certain concentration. The weight ratios of coated layer were 2.11~5.37%. The properties of Cu-metallized low firing temperature substrate, cofired at 90$0^{\circ}C$ for 1h under H2/N2 atmosphere, were as follows; sheet resistance was 13~43 m{{{{ OMEGA }}/$\square$, adhesion strength was 1.0~2.1 kgf/$\textrm{mm}^2$. From the observations of SEM photographs, the gel coated on Cu performed excellently as a glass frit.

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Simulation of the Digital Image Processing Algorithm for the Coating Thickness Automatic Measurement of the TRISO-coated Fuel Particle

  • Kim, Woong-Ki;Lee, Young-Woo;Ra, Sung-Woong
    • Journal of Information Processing Systems
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    • 제1권1호
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    • pp.36-40
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    • 2005
  • TRISO (Tri-Isotropic)-coated fuel particle is widely applied due to its higher stability at high temperature and its efficient retention capability for fission products in the HTGR (high temperature gas-cooled reactor), one of the highly efficient Generation IV reactors. The typical ball-type TRISO-coated fuel particle with a diameter of about 1 mm is composed of a nuclear fuel particle as a kernel and of outer coating layers. The coating layers consist of a buffer PyC, inner PyC, SiC, and outer PyC layer. In this study, a digital image processing algorithm is proposed to automatically measure the thickness of the coating layers. An FBP (filtered backprojection) algorithm was applied to reconstruct the CT image using virtual X-ray radiographic images for a simulated TRISO-coated fuel particle. The automatic measurement algorithm was developed to measure the coating thickness for the reconstructed image with noises. The boundary lines were automatically detected, then the coating thickness was circularly by the algorithm. The simulation result showed that the measurement error rate was less than 1.4%.

전자선을 이용한 PVDF-HFP/Silylated Al2O3가 코팅된 리튬 이차 전지용 폴리에틸렌 분리막의 전기화학적 특성 연구 (Electrochemical Study on PVDF-HFP/Silylated Al2O3-coated PE Separators using the Electron Beam Irradiation for Lithium Secondary Battery)

  • 손준용;신준화;노영창
    • 방사선산업학회지
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    • 제4권4호
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    • pp.359-364
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    • 2010
  • PVDF-HFP (binder)/silylated alumina (inorganic particle)-coated PE (polyethylene) separators were with various compositions of binder and inorganic particle were prepared by a dip-coating process with humidity control (R.H. 25% and 50%) using electron beam irradiation. The morphology of the coated PVDF-$HFP/Al_2O_3$ layer with various compositions of PVDF-HFP and $Al_2O_3$, and humidity condition was found to be an important factor in determining ionic conductivity of the prepared separators. The PVDF-$HFP/Al_2O_3$ (5/5)-coated PE separator prepared at R.H. 50% followed by electron beam irradiation at 200 kGy was applied for lithium-ion polymer battery and the cell test results showed improved high-rate discharge performance and better cyclic stability compared to the cells with the bare PE and the PVDF-HFP-coated PE separators.

NI/$MgAl_2O_4$코팅된 금속 모노리스 촉매의 수소 생산을 위한 천연가스 수증기 개질 반응특성에 관한 연구 (The Performance of NI/$MgAl_2O_4$ Coated Metal Monolith in Natural Gas Steam Reforming for Hydrogen Production)

  • 최은정;구기영;정운호;이영우;윤왕래
    • 한국수소및신에너지학회논문집
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    • 제21권6호
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    • pp.500-506
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    • 2010
  • The metal monolith catalyst coated with 15wt% Ni/$MgAl_2O_4$ is applied to the natural gas steam reforming for hydrogen production. To address the improvement of adherence between metal monolith and catalyst coating layer, the pre-calcination temperature as well as the coating conditions of $Al_2O_3$ sol are optimized. When the Fe-Cr alloy monolith is pre-calcined at $900^{\circ}C$ for 6 h, $Al_2O_3$ layer was formed uniformly on the entire surface of the metal substrate. It is seen that the formation of $Al_2O_3$ layer on the monolith surface is essential for the uniform coating of $Al_2O_3$ sol onto the monolith substrate. The monolith catalyst coated with 10wt% $Al_2O_3$ sol shows high $CH_4$ conversion and good thermal stability as compared with the monolith catalyst without $Al_2O_3$ sol coating under severe reaction conditions with high GHSV of 30,000 $h^{-1}$ at $700^{\circ}C$. In addition, the metal monolith catalyst shows higher catalytic activity and better thermal conductivity than 15wt% Ni/$MgAl_2O_4$ pellet catalyst.

Exploratory research on ultra-long polymer optical fiber-based corrosion sensing for buried metal pipelines

  • Luo, Dong;Li, Yuanyuan;Yang, Hangzhou;Sun, Hao;Chen, Hongbin
    • Smart Structures and Systems
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    • 제26권4호
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    • pp.507-520
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    • 2020
  • In order to achieve effective corrosion monitoring of buried metal pipelines, a Novel nondestructive Testing (NDT) methodology using ultra-long (250 mm) Polymer Optical Fiber (POF) sensors coated with the Fe-C alloy film is proposed in this study. The theoretical principle is investigated to clarify the monitoring mechanism of this method, and the detailed fabrication process of this novel POF sensor is presented. To validate the feasibility of this novel POF sensor, exploratory research of the proposed method was performed using simulated corrosion tests. For simplicity, the geometric shape of the buried pipeline was simulated as a round hot-rolled plain steel bar. A thin nickel layer was applied as the inner plated layer, and the Fe-C alloy film was coated using an electroless plating technique to precisely control the thickness of the alloy film. In the end, systematic sensitivity analysis on corrosion severity was further performed with experimental studies on three sensors fabricated with different metal layer thicknesses of 25 ㎛, 30 ㎛ and 35 ㎛. The experimental observation demonstrated that the sensor coated with 25 ㎛ Fe-C alloy film presented the highest effectiveness with the corrosion sensitivity of 0.3364 mV/g at Δm = 9.32 × 10-4 g in Stage I and 0.0121 mV/g in Stage III. The research findings indicate that the detection accuracy of the novel POF sensor proposed in this study is satisfying. Moreover, the simple fabrication of the high-sensitivity sensor makes it cost-effective and suitable for the on-site corrosion monitoring of buried metal pipelines.

용융염을 이용한 다이아몬드 표면의 크롬카바이드 코팅 (Chromium Carbide Coating on Diamond Particle Using Molten Salts)

  • 정영우;김화정;안용식;최희락
    • 한국재료학회지
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    • 제28권7호
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    • pp.423-427
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    • 2018
  • For diamond/metal composites it is better to use diamond particles coated with metal carbide because of improved wettability between the diamond particles and the matrix. In this study, the coating of diamond particles with a chromium carbide layer is investigated. On heating diamond and chromium powders at $800{\sim}900^{\circ}C$ in molten salts of LiCl, KCl, $CaCl_2$, the diamond particles are coated with $Cr_7C_3$. The surfaces of the diamond powders are analyzed using X-ray diffraction and scanning electron microscopy. The average thickness of the $Cr_7C_3$ coating layers is calculated from the result of the particle size analysis. By using the molten salt method, the $Cr_7C_3$ coating layer is uniformly formed on the diamond particles at a relatively low temperature at which the graphitization of the diamond particles is avoided. Treatment temperatures are lower than those in the previously proposed methods. The coated layer is thickened with an increase in heating temperature up to $900^{\circ}C$. The coating reaction of the diamond particles with chromium carbide is much more rapid in $LiCl-KCl-CaCl_2$ molten salts than with the molten salts of $KCl-CaCl_2$.

Effects of Zn2+ concentration and pH on the formation and growth of zinc phosphate conversion coatings on AZ31 magnesium alloy

  • Van Phuong, Nguyen;Lee, Kyuhwan;Lee, Sangyeol;Moon, Sungmo
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2013년도 춘계학술대회 논문집
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    • pp.62-62
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    • 2013
  • Magnesium alloys exhibit many attractive properties such as low density, high strength/weight ratio, high thermal conductivity, very good electromagnetic features and good recyclability. However, most commercial magnesium alloys require protective coatings because of their poor corrosion resistance. Attempts have been made to improve the corrosion resistance of the Mg alloys by surface treatments, such as chemical conversion coatings, anodizing, plating and metal coatings. Among them, chemical conversion coatings are regarded as one of the most effective and cheapest ways to prevent corrosion of Mg alloys. In this study, the effects of various $Zn^{2+}$ concentrations and pH levels on the formation of zinc phosphate conversion coatings (ZPCCs) on AZ31 magnesium alloy were investigated, and corrosion resistances of the coated samples were evaluated by immersion test and potentiodynamic polarization experiment. The corrosion resistance of the coated AZ31 samples was found to increase with increasing $Zn^{2+}$ concentration and the lowest corrosion rate was obtained for the samples coated at pH of 3.07, independent of $Zn^{2+}$ concentration. The best coatings on AZ31 were obtained at [$Zn^{2+}$] = 0.068 M and pH 3.07. At the conditions of [$Zn^{2+}$] = 0.068 M and pH 3.07, the formation and growth processes of ZPCCs on AZ31 Mg alloy are divided into four stages: formation of a dense layer, precipitation of fine crystals on the dense layer, growths of the inner and outer layers, and reorganization of outer crystalline layer.

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