• Title/Summary/Keyword: Coarse size

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Effect of Solid Content and Particle Size on the Flow Properties of Molten Chocolate (고형성분의 농도와 입도가 액상 초코렛의 유동특성에 미치는 영향)

  • Kim, Do-Un;Yoo, Myung-Shik;Pyun, Yu-Ryang
    • Korean Journal of Food Science and Technology
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    • v.21 no.1
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    • pp.75-79
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    • 1989
  • The rheological properties of sugar and cocoa particle suspensions in cocoa butter under molten condition were analyzed with Haake rotationary viscometer. Both suspensions had yield value and showed rheopexy at low shear rate and thixotropy at high shear rate. Flow behaviors of the suspensions were analyzed with modified Casson model. Casson viscosity and yield value increased with increasing the concentration of sugar and cocoa particles. There was an obvious dependence of the Casson viscosity and yield value on the particle size distributions that was represented by the Sauter mean diameter of the particles. Casson viscosity and yield value of cocoa butter-sugar suspension increased with increasing the fineness of sugar particle crystal. With increasing the fineness of cocoa particle a decreasing Casson viscosity of cocoa butter-cocoa particle suspension was achieved, but the yield value did not change significantly with cocoa particle size. Therefore, it was predicted that the best rheological properties of chocolate could be obtained with the combination of coarse ground sugar $(d=36.30{\mu}m)$ and fine ground cocoa particle $(d=14.81{\mu}m)$ within the studied range.

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Analysis of the Corrosion Behavior According to the Characteristics of Sigma Phase Formed in Super Austenitic Stainless Steel (슈퍼 오스테나이트계 스테인리스강의 시그마상 특성에 따른 부식거동 분석)

  • Kim, Ye Eun;Park, Jin-seong;Cho, Dong Min;Hong, Seung Gab;Kim, Sung Jin
    • Corrosion Science and Technology
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    • v.19 no.4
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    • pp.203-210
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    • 2020
  • The corrosion behavior of super austenitic stainless steel was studied by examining the characteristics of the sigma phase formed in the steel. A range of experimental and analytical methods was employed, including potentiodynamic polarization tests, critical pitting temperature tests, transmission electron microscopy, and energy-dispersive spectroscopy. Three steel samples with different sigma phase levels were obtained by intentionally adjusting the manufacturing process. The results showed that the corrosion resistance of the samples was strongly dependent upon the size and distribution of the sigma phase precipitated in the samples. The larger the size of the sigma phase, the higher the Mo content in the sigma phase and the higher the depletion level of Mo at the interface between the matrix/sigma phase, the more samples with a coarse-sized sigma phase were susceptible to localized pitting corrosion at the interface. These results suggest that various manufacturing processes, such as welding and the post-heat treatment of the steel, should be optimized so that both the size and fraction of the sigma phase precipitated in the steel are small to improve the resistance to localized corrosion.

Synthesis of Bi Nanoparticles Using a Modified Polyol Method (변형 폴리욜법에 의한 Bi 나노입자의 제조)

  • Cho, Hye-Jung;Lee, Jong-Hyun
    • Journal of the Microelectronics and Packaging Society
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    • v.19 no.2
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    • pp.61-66
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    • 2012
  • Bismuth(Bi) nanoparticles were synthesized at room temperature by a modified polyol process using bismuth(III) carbonate basic as precursor. In addition, some characteristics of the synthesis with respect to the exchange of a capping agent/surface stabilizer and solvent type were observed. When polyvinylpyrroldone was added, the finest Bi nanoparticles were synthesized in diethylene glycol(DEG), while the coarsest nanoparticles were formed in polyethylene glycol(PEG). The particle size immediately after synthesis was proportionate to final particle size which was determined by particle growth through coalescence and aggregation during drying. As a result, the finest Bi particles with the diameter range of several tens of nanometers - 300 nm were finally obtained in DEG. Regardless of the type of capping agent/surface stabilizer, extensive coalescence and aggregation behavior occurred in PEG, resulting in final products agglomerated with coarse particles.

Species Composition and Community Structure of Macrobenthos during Fall on the Dokdo Coast, Korea (가을철 독도 연안에 출현하는 대형저서동물의 종 조성 및 군집 구조)

  • Kang, Su Min;Lee, Hyung-Gon;Kim, Sang Lyeol;Choi, Jin-Woo;Park, Chan Hong;Yu, Ok Hwan
    • Ocean and Polar Research
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    • v.41 no.2
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    • pp.47-61
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    • 2019
  • The Dokdo coast is known for its high biodiversity. However, few studies have examined the biodiversity and macrobenthic community on the subtidal soft-bottom. Therefore, we collected macrobenthos (> 1 mm) using a Smith-McIntyre grab ($0.1m^2$) at 15 stations along the Dokdo coast in September 2016. The sediments consisted of badly sorted (1.7) coarse sand with gravel and the mean sediment grain size was $-0.4{\phi}$. In total, 177 macrobenthic species were collected; their mean density was $1,566ind./m^2$. The number of species and density of macrobenthic fauna decreased significantly with the mean grain size. The dominant species were the amphipods Melita denticulata (16.5%) and Melita shimizui (5.5%), polychaete Salvatoria clavata (5.4%), bivalve Glycymeris aspersa (4.4%), and ophiuroid Ophionereis dubia (4.3%). The dominant macrobenthos species on the subtidal soft-bottom differed from the coastal areas of the East Sea, suggesting that the difference in the sediment grain size affected the macrobenthos. Cluster analysis was performed to divide the study area into four groups, and environmental factors which correlated with species composition and distribution in the study area were the combination of the four parameters of salinity, dissolved oxygen, total organic carbon and depth. A future seasonal investigation is needed to understand the species composition and characteristics of the Dokdo macrobenthos.

A Study on the Granulometry and Chemical Composition of Psudo-Gleized Soil in Jeongdongjin Area (정동진 의사글레이층의 입도와 화학 조성에 대한 연구)

  • Kim, Jong Yeon
    • Journal of The Geomorphological Association of Korea
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    • v.24 no.3
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    • pp.27-45
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    • 2017
  • At the upper part of terrace deposits at Jeongdongjin area, there is a structure in which reddish brown and grayish white layers laying horizontally. Previous studies have reported the existence of these structures within the deposits and suggested the theoretical background related to the formation process. However, the analysis of physical properties and chemical composition such as particle size, classification, etc. of the materials constituting the reddish brown and grayish white layers is scarcely done. In this study, the physico - chemical properties of gray - white and reddish brown beds are investigated. The mean grain size of the particles was less than $4{\varphi}$ in both layers and the reddish brown layer was more coarse. The results shows that the sorting of the grayish white layer is better. The chemical composition of both layers shows that the average concentration of $SiO_2$, $Al_2O_3$ and $K_2O$ of the grayish white layer was higher than those of the reddish brown layer. The concentration of $Fe_2O_3$ of reddish brown lyaer was 3 times higher than those of the grayish white layer. The degree of chemical weathering (CIA) is 90 or so in both the reddish brown and grayish white layers, indicating a significant level of chemical weathering. In conclusion, reddish brown layers had been formed by the processes related to the migration of iron and the migration of water that induced aggregation after the formation of sediments (psudo-gleization). In this study area, a vertical layer of grayish white which cuts off horizontal reddish brown and grayish white color was found. The vertical layer or wedge similar to a ice-wedge or columnar structure that in a cold environment, and there is a difference in shape and size. The vertical layer appears to have occurred three or more cycles. The vertical layers begin to form at a certain height within the outcrop and descend downwards, which of course is difficult to see as directing certain times.

Effects of Initial Nucleation Condition at the Start Block on the Grain Size and Growth Direction in Directionally Solidified CM247LC Superalloy (CM247LC 초내열합금에서 일방향응고 스타트 블록의 초기 핵생성 조건에 따른 결정립 성장)

  • Yoon, Hye-Young;Lee, Je-Hyun;Jung, Hyeong-Min;Seo, Seong-Moon;Jo, Chang-Young;Gwon, Seok-Hwan;Chang, Byeong-Moon
    • Korean Journal of Metals and Materials
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    • v.49 no.1
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    • pp.58-63
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    • 2011
  • The grain size and growth direction of a directionally solidified turbine blade were evaluated by the initial nucleation condition at the start block of directional solidification. The initial nucleation condition was controlled by inserting a Ni foil on the directional solidification plate of the directional solidification furnace. Fine grains with good orientation were obtained in the faster cooling condition at the start block. The nucleus number was compared with the cooling rate of the start block by electron back scattered diffraction (EBSD). DSC (differential scanning calorimeter) analysis was performed to compare the melting point and undercooling for nucleation of the coarse nuclei and fine nuclei of the start block. The faster cooling condition at the start block showed more undercooling for nucleation and smaller size of nuclei which resulted in a fine grain with good orientation in the directional turbine blade.

Microstructure and High-Cycle Fatigue Properties of High-Speed-Extruded Mg-5Bi-3Al Alloy (Mg-5Bi-3Al 마그네슘 고속 압출재의 미세조직과 고주기피로 특성)

  • Cha, J.W.;Jin, S.C.;Park, S.H.
    • Transactions of Materials Processing
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    • v.31 no.5
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    • pp.253-260
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    • 2022
  • In this study, the microstructural characteristics of a high-speed-extruded Mg-5Bi-3Al (BA53) alloy and its tensile, compressive, and high-cycle fatigue properties are investigated. The BA53 alloy is successfully extruded at a die-exit speed of 16.6 m/min without any hot cracking using a large-scale extruder for mass production. The homogenized BA53 billet has a large grain size of ~900 ㎛ and it contains fine and coarse Mg3Bi2 particles. The extruded BA53 alloy has a fully recrystallized microstructure with an average grain size of 33.8 ㎛ owing to the occurrence of complete dynamic recrystallization during high-speed extrusion. In addition, the extruded BA53 alloy contains numerous fine lath-type Mg3Bi2 particles, which are formed through static precipitation during air cooling after exiting the extrusion die. The extruded BA53 alloy has a high tensile yield strength of 175.1 MPa and ultimate tensile strength of 244.4 MPa, which are mainly attributed to the relative fine grain size and numerous fine particles. The compressive yield strength (93.4 MPa) of the extruded BA53 alloy is lower than its tensile yield strength, resulting in a tension-compression yield asymmetry of 0.53. High-cycle fatigue test results reveal that the extruded BA53 alloy has a fatigue strength of 110 MPa and fatigue cracks initiate at the surface of fatigue test specimens, indicating that the Mg3Bi2 particles do not act as fatigue crack initiation sites. Furthermore, the extruded BA53 alloy exhibits a higher fatigue ratio of 0.45 than other commercial extruded Mg-Al-Zn-based alloys.

Experimental study of welding effect on grade S690Q high strength steel butt joint

  • Chen, Cheng;Chiew, Sing Ping;Zhao, Mingshan;Lee, Chi King;Fung, Tat Ching
    • Steel and Composite Structures
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    • v.39 no.4
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    • pp.401-417
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    • 2021
  • This study experimentally reveals the influence of welding on grade S690Q high strength steel (HSS) butt joints from both micro and macro levels. Total eight butt joints, taking plate thickness and welding heat input as principal factors, were welded by shielded metal arc welding. In micro level, the microstructure transformations of the coarse grain heat affected zone (CGHAZ), the fine grain heat affected zone (FGHAZ) and the tempering zone occurred during welding were observed under light optical microscopy, and the corresponding mechanical performance of those areas were explored by micro-hardness tests. In macro level, standard tensile tests were conducted to investigate the impacts of welding on tensile behaviour of S690Q HSS butt joints. The test results showed that the main microstructure of S690Q HSS before welding was tempered martensite. After welding, the original microstructure was transformed to granular bainite in the CGHAZ, and to ferrite and cementite in the FGHAZ. For the tempering zone, some temper martensite decomposed to ferrite. The performed micro-hardness tests revealed that an obvious "soft layer" occurred in HAZ, and the HAZ size increased as the heat input increased. However, under the same level of heat input, the HAZ size decreased as the plate thickness increased. Subsequent coupon tensile tests found that all joints eventually failed within the HAZ with reduced tensile strength when compared with the base material. Similar to the size of the HAZ, the reduction of tensile strength increased as the welding heat input increased but decreased as the thickness of the plate increased.

A Comparative Analysis on Channel Forms and Landscapes at Naeseongcheon River and Wicheon River in Gyeongpook Province (경북 내성천과 위천의 하도 형상 및 경관 비교 분석)

  • Lee, Gwang-Ryul
    • Journal of The Geomorphological Association of Korea
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    • v.17 no.4
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    • pp.1-16
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    • 2010
  • Channel topography, sediment properties, channel landscapes and characteristics of land covers in Naeseongcheon and Wicheon River consisting of granites and sedimentary rocks, respectively, are compared and analyzed. Due to the differences of bedrocks, soils and characteristics of land covers in the basins, Wicheon River with the slow flow speed shows the larger variations in river stage than Naeseongcheon River. While Naeseongcheon River fed by the granite sediments throughout granular disintegration hs tthe regular grain size properties with coarse sand in the most of river, Wicheon River fed by sedimentary rocks indicates the dramatic decertses of grain size lower-ward. Naeseongcheon River with channel interferences such as sand-sized sediment transughoations, dredges, and aggregate collections is analyzed as poorer vegetation covers than Wicheon River due to the dramatic changes in channel surfaces.

A study of compaction ratio and permeability of soil with different water content (축제용흙의 함수비 변화에 의한 다짐율 및 수용계수 변화에 관한 연구)

  • 윤충섭
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.13 no.4
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    • pp.2456-2470
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    • 1971
  • Compaction of soil is very important for construction of soil structures such as highway fills, embankment of reservoir and seadike. With increasing compaction effort, the strength of soil, interor friction and Cohesion increas greatly while the reduction of permerbilityis evident. Factors which may influence compaction effort are moisture content, grain size, grain distribution and other physical properties as well as the variable method of compaction. The moisture content among these parameter is the most important thing. For making the maximum density to a given soil, the comparable optimum water content is required. If there is a slight change in water content when compared with optimum water content, the compaction ratio will decrease and the corresponding mechanical properties will change evidently. The results in this study of soil compaction with different water content are summarized as follows. 1) The maximum dry density increased and corresponding optimum moisture content decreased with increasing of coarse grain size and the compaction curve is steeper than increasing of fine grain size. 2) The maximum dry density is decreased with increasing of the optimum water content and a relationship both parameter becomes rdam-max=2.232-0.02785 $W_0$ But this relstionship will be change to $r_d=ae^{-bw}$ when comparable water content changes. 3) In case of most soils, a dry condition is better than wet condition to give a compactive effort, but the latter condition is only preferable when the liquid limit of soil exceeds 50 percent. 4) The compaction ratio of cohesive soil is greeter than cohesionless soil even the amount of coarse grain sizes are same. 5) The relationship between the maximum dry density and porosity is as rdmax=2,186-0.872e, but it changes to $r_d=ae^{be}$ when water content vary from optimum water content. 6) The void ratio is increased with increasing of optimum water content as n=15.85+1.075 w, but therelation becames $n=ae^{bw}$ if there is a variation in water content. 7) The increament of permeabilty is high when the soil is a high plasticity or coarse. 8) The coefficient of permeability of soil compacted in wet condition is lower than the soil compacted in dry condition. 9) Cohesive soil has higher permeability than cohesionless soil even the amount of coarse particles are same. 10) In generall, the soil which has high optimum water content has lower coefficient of permeability than low optimum water content. 11) The coefficient of permeability has a certain relations with density, gradation and void ratio and it increase with increasing of saturation degree.

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