• Title/Summary/Keyword: Co powder

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산화물 복합분말 첨가 Camphene 슬러리의 동결건조 공정에 의한 Cu-Co 복합계 다공체 제조 (Synthesis of Porous Cu-Co using Freeze Drying Process of Camphene Slurry with Oxide Composite Powders)

  • 이규휘;한주연;오승탁
    • 한국분말재료학회지
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    • 제27권3호
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    • pp.193-197
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    • 2020
  • Porous Cu-14 wt% Co with aligned pores is produced by a freeze drying and sintering process. Unidirectional freezing of camphene slurry with CuO-Co3O4 powders is conducted, and pores in the frozen specimens are generated by sublimation of the camphene crystals. The dried bodies are hydrogen-reduced at 500℃ and sintered at 800℃ for 1 h. The reduction behavior of the CuO-Co3O4 powder mixture is analyzed using a temperature-programmed reduction method in an Ar-10% H2 atmosphere. The sintered bodies show large and aligned parallel pores in the camphene growth direction. In addition, small pores are distributed around the internal walls of the large pores. The size and fraction of the pores decrease as the amount of solid powder added to the slurry increases. The change in pore characteristics according to the amount of the mixed powder is interpreted to be due to the rearrangement and accumulation behavior of the solid particles in the freezing process of the slurry.

Effects of Crystal Grain Size and Particle Size on Core Loss For Fe-Si Compressed Cores

  • Takemoto, Satoshi;Saito, Takanobu
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.1183-1184
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    • 2006
  • Core loss of soft magnetic powder cores have been focused on to achieve high efficiency of power supplies. In this study the effects of crystal grain size on core loss were investigated by changing heat treatment conditions. It was found that core loss is influenced by crystal grain size because eddy current loss decreased and hysteresis loss increased by making crystal grain size smaller, and it is also influenced by particle size.

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분무건조법에 의한 용사용 WC-17%Co 복합분말제조 및 HVOF(High Velocity Oxy-Fuel) 용사특성 (Fabrication of WC-17%Co Composite Powder for Thermal Spray by Spray-Drying Method and HVOF Thermal Spray Characteristics)

  • 설동욱;김병희;임영우;정민석;서동수
    • Journal of Welding and Joining
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    • 제14권6호
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    • pp.101-108
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    • 1996
  • In this study, WC-l7wt% Co composite powder for thermal spray was fabricated by spray drying method. The agglomerated composite powder had spheroidal morphology and the particle size distribution was 20~60${\mu}{\textrm}{m}$. WC and Co were distributed homogeneously. However, the strength of the spray-dried agglomerate was low due to the pores within the agglomerate. Therefore, the spray-dried agglomerate was broken down during HVOF thermal spray and the microstructure was inhomogeneous with many pores within the coating layer. And the decomposition of WC to W and $W_{6}$ $C_{2.54}$ was accelerated. The strength and flowability of the agglomerate were greatly improved by sintering heat treatment(110$0^{\circ}C$, 1 hour, hi atmosphere), and then the coating layer showed dense and homogeneous microstructure with well-developed splats. The hardness of the coating layer was H $v_{300}$ = 1072.2.2.

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텅스텐염의 액상법을 통한 초미립 WC-Co 분말의 합성 (Synthesis of Nano-sized Tungsten Carbide - Cobalt Powder by Liquid Phase Method of Tungstate)

  • 김종훈;박용호;하국현
    • 한국분말재료학회지
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    • 제18권4호
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    • pp.332-339
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    • 2011
  • Cemented tungsten carbide has been used in cutting tools and die materials, and is an important industrial material. When the particle size is reduced to ultrafine, the hardness and other mechanical properties are improved remarkably. Ultrafine cemented carbide with high toughness and hardness is now widely used. The objective of this study is synthesis of nanostructured WC-Co powders by liquid phase method of tungstate. The precursor powders were obtained by freezen-drying of aqueous solution of soluble salts, such as ammonium metatungstate, cobalt nitrate. the final compositions were WC-10Co. In the case of liquid phase method, it can be observed synthesis of WC-10Co. The properties of powder produced at various temperature, were estimated from the SEM, BET and C/S analyser.

WC-Co 초경합금의 마이크로파 소결 (Microwave Sintering of WC-Co Hard Metals)

  • 송강석;김석범
    • 한국분말재료학회지
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    • 제10권4호
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    • pp.249-254
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    • 2003
  • WC-6wt%Co hard metal powders were sintered by a 2.45 GHz multimode microwave applicator in Ar atmosphere. Microwave sintering of WC-6wt%Co powder lowered the sintering temperature and shortened the processing time in less than two hours than by a conventional method. Microstructures of the sintered specimen were studied with scanning electron microscope (SEM) and no abnormal grain growth was observed. Mechanical properties were similar to the values of the specimens sintered by a conventional method. Specimen sintered at 135$0^{\circ}C$ for 30 minutes ,hewed 99%, 20.5 GPa and 8.1 MPa$\sqrt{m}$ of theoretical density, hardness and fracture strength, respectively.

${\CO_2}$ 레이저에 의한 선택적 소결법 (Selective Laser Sintering by ${\CO_2}$ Laser)

  • 전병철;김재도
    • 한국정밀공학회지
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    • 제15권7호
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    • pp.18-25
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    • 1998
  • A prototyping process based on the technique of selective ${\CO_2}$ laser sintering has been carried out using bronze powder. The integration of a ${\CO_2}$ laser and a working table to create the opto-mechanical system has been constructed for making the multi-layer sintering. Three dimensional rapid prototyping process which has used the 40W ${\CO_2}$ laser and bronze powder has been investigated experimentally The optimal scanning method has been found to minimize the deflection and distortion by using the thermal strain method which the laser scans in the x and v directions repeatedly. The method of spreading powder has been improved by using the rubber knife of which the flexibility causes less wave of spreading powder.

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Research on Two Sintered Techniques of Nanometer WC-Co Powder

  • Sun, Lan;Jia, Chengchang;Tang, Hua
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.529-530
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    • 2006
  • This paper concerned with SPS (spark plasma sintering), hot pressing of sinter nanometer WC-Co powder and discussed the density, hardness, microstructures and grain sizes of the alloys sintered. The results showed that the two sintered techniques could produce high density alloys and play well on the grain growth, but SPS could lower the sintering temperature and shorten sintering time. Besides, the hardness of the sintered cemented alloys that was dependent on the grain size and densification could also be improved.

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폐미분말을 원료로 한 저탄소형 재생시멘트의 CO2배출량 저감평가 (Evaluation of Reduction of CO2 Emission Achieved by Using Low-carbon Recycled Cement with Cementitious Waste Powder)

  • 권은희;안재철;박동천
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2014년도 춘계 학술논문 발표대회
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    • pp.250-251
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    • 2014
  • With the recent movement toward sustainable development, many efforts have been made to reduce environmental loads in various domains of industry. In particular, a great deal of research and technology development has been underway on approaches to reducing industrial waste and the emission of greenhouse gases. For this reason, a quantitative analysis of the reduction in CO2 emission that could be achieved by replacing limestone material with cementitious waste powder was performed in this study. Through the analysis, it was found that CO2 emissions were reduced by up to 50 percent compared with the scenario in which OPC was used, which suggests that it is possible to reduce global CO2 emissions by approximately 5percent, or by 446.4 Tg of the 965 Tg of CO2 emissions generated by the cement industry, in the total global CO2 emissions of 19300Tg.

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