• Title/Summary/Keyword: Chemical Detection

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SEC/Light Scattering Analysis of Multicomponent Polymer Systems

  • 이희정;장태현
    • Bulletin of the Korean Chemical Society
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    • v.17 no.7
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    • pp.648-653
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    • 1996
  • We have shown several examples of characterization of multicomponent polymer systems by size exclusion chromatography coupled with a light scattering detector. Although SEC cannot provide a complete information for such systems due to its intrinsic limitation, one can extend its capability by combining multiple detection in order to get relevant information to some extent.

Analysis of Residual Organic Solvent in Environmentally-friendly Farming Materials with Headspace Method (Headspace 법을 사용한 유기농업자재 중 잔류 유기용매 분석)

  • Choi, Geun Hyoung;Kong, Seung-Heon;Park, Byung-Jun;Moon, Byeong-Cheol;Kim, Jin-Hyo
    • The Korean Journal of Pesticide Science
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    • v.20 no.2
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    • pp.128-132
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    • 2016
  • Volatile organic solvents are used to extract the bioactive materials from raw materials for environmentally-friendly farming materials (EFFM), but the solvent should not remain in EFFM for the safety reasons. Thus qualitative and quantitative analysis method for the solvents using Headspace-GC were evaluated. Water content depleted the detection ratio of hydrophilic solvents and disturbing the hydrophilic interaction with solvents by DMSO might be helped to increase the detection ratio (up to 715%). Surfactant concentration affected to the detection ratio (68.5-179.1%) while surfactant type was not deeply involved the solvent detection. On the other hand, matrix-matched calibration method was accepted the minimum requirements for the quantitative analysis of the solvents in EFFM.

Prevention of Soil Contamination from Underground Storage Facilities of Petroleum Product and Hazardous Chemical Compounds (유류 및 유해화학물질 저장시설에서의 토양오염 방지대책)

  • 배우근;홍종철;정진욱;김종호
    • Journal of Soil and Groundwater Environment
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    • v.7 no.4
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    • pp.40-47
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    • 2002
  • The practices of the construction and management of the petroleum and hazardous chemical compound storage facilities in Korea were investigated extensively, and the problems were identified. The advanced technologies in the U.S.A were comparatively studied. Considering the effectiveness of leak prevention and applicability, the following measures were suggested. To prevent corrosion of a tank, a clad tank, an interior lining tank, or a double-wall tank were thought to be the most cost effective. For piping. use of non-metalic materials was suggested. A catchment basin seemed to be effective for preventing spills. For monitoring of leaks, constructions of more than one of detection systems, such as an automatic leak detection device. a vapor detection system, a groundwater monitoring system, or a double-wall monitoring system, were recommended.

Rapid Detection Methods for Biogenic Amines in Foods (식품 내 바이오제닉아민 신속검출기술 개발 동향)

  • Lee, Jae-Ick;Kim, Young-Wan
    • Korean Journal of Food Science and Technology
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    • v.44 no.2
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    • pp.141-147
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    • 2012
  • Biogenic amines have been used as chemical indicators to estimate bacterial spoilage of foods, particularly fish and fish products, cheese, and fermented foods. So far many chromatography methods have been developed to detect biogenic amines in foods. Although these instrumental analyses exhibit good sensitivity, they cannot be used as rapid detection methods due to the chemical treatment of the samples and the time-consuming process involved. For the rapid and simple detection of biogenic amines, enzyme linked immunosorbent assay kits are commercially available. In addition, analytical systems with enzyme-based amperometric biosensor detection have been increasingly developed. The biosensors used to detect the biogenic amines are based on the action of either amine oxidases or amine dehydrogenases that catalyzes the oxidative deamination of biogenic amines to the corresponding aldehydes and ammonia. This review mainly focused on the principle, development, and applications of the detection methods for rapid detection of biogenic amines in foods.

Quantitative Analysis of Ethyl Carbamate in Korean Alcoholic Beverages by Chromatography with Mass Selective Detection (GC/MS 를 이용한 한국 주류 중의 Ethyl Carbamate 정량)

  • Park, Gyo-Beom;Lee, Sueg-Geun
    • Analytical Science and Technology
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    • v.15 no.1
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    • pp.26-30
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    • 2002
  • In order to determine the contents of ethyl carbamate in Korean traditional alcoholic beverages and general beverages, GC/MS-SIM method was used after extraction of beverages with dichloromethane. The contents of ethyl carbamate in Korean traditional alcoholic beverages, non-distilled alcohol, and whisky were detected in the range of $4.6-50.2{\mu}g/L$, $27.8-45.4{\mu}g/L$, and $24.8-55.1{\mu}g/L$, respectively. The recoveries were ranged from 83.3 to 104.8 %. The values of relative standard deviation were ranged from 1.8 to 14.8 % and the detection limit was $0.3{\mu}g/L$.