• Title/Summary/Keyword: Characterization high school

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Synthesis and Characterization of Highly Fluorescent and Thermally Stable π-Conjugates involving Spiro[fluorene-9,4'-[4H]indeno[1,2-b]furan]

  • Kowada, Toshiyuki;Ohe, Kouichi
    • Bulletin of the Korean Chemical Society
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    • v.31 no.3
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    • pp.577-581
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    • 2010
  • Spiro[fluorene-9,4'-[4H]indeno[1,2-b]furan] was synthesized, and its $\pi$-conjugation was efficiently elongated using palladium-catalyzed C-H arylation of a furan moiety. The resulting $\pi$-conjugated compounds showed intense fluorescence and extremely high thermal stability.

Deposition and high temperature oxidation characterization of CrAlSiN thin films

  • Kim, Sun-Kyu;Lee, Dong-Bok
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2007.11a
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    • pp.7-9
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    • 2007
  • Thin films of CrAlSiN were deposited on SKD11 tool steel substrate using Cr and AlSi cathodes by a cathodic arc plasma deposition system. The influence of process parameters on the deposited film properties were investigated. The oxidation characteristics of the films were studied at temperatures ranging from 800 and 1000+C up to 50 h in air. The films showed superhardness and good oxidation resistance..

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Dynamic Characterization of Large-scale Structures through Mobile-phone Application (휴대폰 애플리케이션을 통한 초대형 구조물의 동적특성 분석)

  • Jung, Young-Seok;Yoon, Sung-Won
    • Journal of Korean Association for Spatial Structures
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    • v.15 no.4
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    • pp.99-105
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    • 2015
  • The serviceability design of the high-rise building is affected by the wind response vibration such as the acceleration, at this time it is important to calculate the natural frequency correctly. Since the suggestion equation of the natural frequency being used in the design phase is not the regression equation obtained from the vibration measurement of the high-rise building, the verification to use for the serviceability design of the high-rise building is necessary. This thesis conducted an ambient vibration measuring on the high-rise building through the mobile-phone application to calculate the natural frequency and suggested a natural frequency approximate expression following the building's height, and compared with the domestic/foreign standard and the result of the eigen-value analysis.

Characterization and Transformation of 0.52%C steels for Wheel Bearing Units Produced by High Frequency Induction Hardening after Hot Forging (열간단조 후 고주파 유도경화에 의해 제조된 휠 베어링 유니트용 0.52%C강의 특성과 변태거동)

  • Choi, Byung-Young
    • Korean Journal of Metals and Materials
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    • v.48 no.12
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    • pp.1103-1108
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    • 2010
  • We fabricated flanged outer races for wheel bearing units using 0.52%C clean steels, and then characterized and studied the transformation behavior. The outer races produced by hot forging and high frequency induction hardening in this study were analyzed through microstructural characterization using OM, SEM, TEM, and X-ray diffractometer and their microhardness depth profiles of the raceway contacted by balls were measured using MVH tester. The surface hardened layers with a uniform hardness profile in the raceway consisting of very fine martensite with sub-micron sized retained austenite could be formed for very short time during high frequency induction hardening after hot forging. The very fine martensite may be transformed on rapid cooling, from the inhomogeneous austenite nucleated on rapid heating in small particles of pearlitic cementite fragmentated by hot forging. On the other hand the sub-micron sized retained austenite may be chemically stabilized due to their extremely small size, from the small austenite nucleated at the grain boundaries.

Syntheses and characterization of nanonetworked carbon materials

  • Kawasaki, S.;Matsuoka, Y.;Okino, F.;Touhara, H.;Suito, K.
    • Proceedings of the Korean Fiber Society Conference
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    • 2003.10a
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    • pp.29-30
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    • 2003
  • Several forms of nanonetworked carbon materials were synthesized by high pressure and high temperature treatments of fullerene C$\_$60/ and single-walled carbon nanotube bundles. Structural properties (e.g. thermal expansion coefficients and compressibilities) of the synthesized materials were investigated by XRD measurements using synchrotron X-ray. Their formation mechanisms are also discussed.

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Ultrasonic Characterization of a Resonating High-Speed Microcantilever (초음파 기법을 이용한 고속 마이크로 캔틸레버의 공진 특성평가)

  • Kim, Yun Young;Lee, Seonwook;Park, Jiwon;Cho, Younho
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.41 no.6
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    • pp.483-489
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    • 2017
  • An ultrasonic technique was developed to characterize the resonance behavior of a microcantilever operating in a megahertz regime. A high-power ultrasonic pulser and a contact transducer were employed to excite the silicon microcantilever, and a Michelson interferometer was used to obtain the time domain waveform. The natural frequency of the microcantilever was evaluated through the fast Fourier transform of the signal, and a numerical analysis using the finite element method confirmed the measurement data. The present study proposes a novel and facile method to evaluate nanoscale materials and structures with high sensitivity compared to conventional approaches.

Molecular Characterization of Porcine DNA Methyltransferase I

  • Lee, Yu-Youn;Kang, Hye-Young;Min, Kwan-Sik
    • Reproductive and Developmental Biology
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    • v.34 no.4
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    • pp.283-288
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    • 2010
  • During normal early embryonic development in mammals, the global pattern of genomic DNA methylation undergoes marked. changes. The level of methylation is high in male and female gametes. Thus, we cloned the cDNA of the porcine DNA methyltransferase 1 (Dnmt1) gene to promote the efficiency of the generation of porcine clones. In this study, porcine Dnmt1 cDNA was sequenced, and Dnmt1 mRNA expression was detected by reverse transcription-polymerase reaction (RT-PCR) in porcine tissues during embryonic development. The porcine Dnmt1 cDNA sequence showed more homology with that of bovine than human, mouse, and rat. The complete sequence of porcine Dnmt1 cDNA was 4,774-bp long and consisted of an open reading frame encoding a protein of 1611 amino acids. The amino acid sequence of porcine DNMT1 showed significant homology with those of bovine (91%), human (88%), rat (76%), and mouse (75%) Dnmt1. The expression of porcine Dnmt1 mRNA was detected during porcine embryogenesis. The mRNA was detected at stages of porcine preimplantation development (1-cell, 2-cell, 4-cell, 8-cell, morula, and blastocyst stages). It was also abundantly expressed in tissues (lung, ovary, kidney and somatic cells). Further investigations are necessary to understand the complex links between methyltransferase 1 and the transcriptional activity in cloned porcine tissues.

Activated Carbon-Embedded Reduced Graphene Oxide Electrodes for Capacitive Desalination

  • Tarif Ahmed;Jin Sun Cha;Chan-gyu Park;Ho Kyong Shon;Dong Suk Han;Hyunwoong Park
    • Journal of Electrochemical Science and Technology
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    • v.14 no.3
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    • pp.222-230
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    • 2023
  • Capacitive deionization of saline water is one of the most promising water purification technologies due to its high energy efficiency and cost-effectiveness. This study synthesizes porous carbon composites composed of reduced graphene oxide (rGO) and activated carbon (AC) with various rGO/AC ratios using a facile chemical method. Surface characterization of the rGO/AC composites shows a successful chemical reduction of GO to rGO and incorporation of AC into rGO. The optimized rGO/AC composite electrode exhibits a specific capacitance of ~243 F g-1 in a 1 M NaCl solution. The galvanostatic charging-discharging test shows excellent reversible cycles, with a slight shortening in the cycle time from the ~260th to the 530th cycle. Various monovalent sodium salts (NaF, NaCl, NaBr, and NaI) and chloride salts (LiCl, NaCl, KCl, and CsCl) are deionized with the rGO/AC electrode pairs at a cell voltage of 1.3 V. Among them, NaI shows the highest specific adsorption capacity of ~22.2 mg g-1. Detailed surface characterization and electrochemical analyses are conducted.

Study on the ultra thin film of silicon oxyinitride deposited by plasma - assisted $N_2O$ oxidation in ICP-CVD reactor (ICP-CVD 반응기 내에서 $N_2O$ 플라즈마 산화법을 이용하여 증착된 ultra thin silicon oxynitride films 에 관한 연구)

  • Hwang, Sung-Hyun;Jung, Sung-Wook;Yi, J.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.161-162
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    • 2006
  • Scaling rules for TFT application devices have led to the necessity of ultra thin dielectric films and high-k dielectric layers. In this paper, The advantages of high concentration of nitrogen in silicon oxide layer deposited by using $N_2O$ in Inductively Coupled Plasma Chemical Vapor Deposition (ICP-CVD) reported about Ellipsometric measurement, Capacitance-Voltage characterization and processing conditions.

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Characterization of CO2 Adsorption Process for a Water Removal from Coal (석탄 내 수분 제거를 위한 CO2 흡착 효과에 대한 연구)

  • SEUNGTAEK LEE;HAKDEOK KIM;JUHUN SONG
    • Transactions of the Korean hydrogen and new energy society
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    • v.35 no.2
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    • pp.115-120
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    • 2024
  • In this study, the extent of water removal in the high-moisture coal was measured. The simplified adsorption model was developed to predict the extent of water removal. The water removal was observed to increase up to 25% at saturation condition of 25℃. The modeling work shows that adsorption contributes the water removal only by 3%, whereas other factors such as CO2 solubility and wettability would be responsible for the water removal.