• Title/Summary/Keyword: Ceramic glaze

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The hardening effect by ice-quenching after oxidation of a Pd-Ag-Sn-Au metal-ceramic alloy during porcelain firing simulation (금속-세라믹용 Pd-Ag-Sn-Au계 합금의 모의소성 시 산화처리 후 급랭에 의한 경화 효과)

  • Shin, Hye-Jeong;Kim, Min-Jung;Kwon, Yong-Hoon;Kim, Hyung-Il;Seol, Hyo-Joung
    • Korean Journal of Dental Materials
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    • v.44 no.3
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    • pp.197-206
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    • 2017
  • The hardening effect by ice-quenching after oxidation of a Pd-Ag-Sn-Au metal-ceramic alloy during porcelain firing simulation was investigated by means of hardness test, field emission scanning electron microscopic observations, and X-ray diffraction analysis. The hardness decreased by ice-quenching after oxidation, which was induced by the homogenization of the ice-quenched specimen. The decreased hardness by ice-quenching after oxidation was recovered from the wash stage which was the first stage of the remaining firing process for bonding porcelain. After wash stage, the hardness of the ice-quenched specimens decreased during the subsequent porcelain firing process. But the final hardness of the ice-quenched specimens after oxidation was higher than that of the specimens cooled at stage 0 after oxidation. The increase in hardness of the specimens during the first firing process was caused by the lattice strains generated at the interface between the face-centered cubic Pd-Ag-rich matrix and the face-centered tetragonal Pd3(Sn, Ga, In) precipitate. The decrease in hardness of the specimens during the remaining firing process was caused by the microstructural coarsening.

Composition and Microstructure of Punch'ong Sherds from Bokwang-ri, Kangnung (강릉 보광리 분청도편의 성분과 미세구조 연구)

  • Kim, Kyung-nam;Han, Sang-mok;Shin, Dae-yong
    • Journal of Conservation Science
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    • v.8 no.1 s.11
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    • pp.10-15
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    • 1999
  • The chemical compositions and microstructure of the punch'ong excavated from Bokwangri, Kangnung were investigated by the scanning electron microscope (SEM) with an energy dispersive X-ray spectrometer (EDS), X-ray diffractometer (XRD), and dilatometer. The compositions of body were $SiO_2(73-78\%),\;Al_2O_3(13-16\%)$, $RO{\cdot}R_2O(4-5\%,\;R=Ca,\;Mg,\;Na,\;K),\;R_xO_y(3-6\%,\;R=Fe,Ti)$ in weight ratio, which were higher silica and flux $(RO{\cdot}R_2O)$ but lower alumina. Owing to the high content$(21-30\%)$ of calcium oxide the glaze is considered lime type. Firing temperature range for the ceramic was presumed to about $1150^{\circ}C$.

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Porous and Pottery with Dark Brown Glaze (한국전통옹기의 통기성)

  • Kim, Seok-Ho
    • The Journal of the Korea Contents Association
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    • v.7 no.10
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    • pp.157-164
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    • 2007
  • Human made a vessel which was made naturally to store something being hunted and picked, which was a great invention.(n modern times, society changed and development of science gave us convenience in making a vessel and various kinds of store instruments which was made of pure natural material), They have built the house which became to be a part of nature, and studied a method of storing food to eat for four seasons, then displayed a storage house and storage containers everywhere of the house. Now Korean has the custody of kimchi in refrigerator at every house. With hot wind of well-being, Korean food is becoming to be globalized, according to this the world shows concern seriously about the pottery This study have three purposes, the first. checking documents about the development history of pottery which is a kind of ceramic, and then the second, through an scientific experiment, with studying characteristic of pottery being built by the wisdom of ancestors, informing the merit of pottery and necessity to the world, and futhermore, the third, working up the development of close environmental vessels putting to use the characteristic of pottery.

Whiteware from the Official Kiln of Choseon Dynasty Period in Beoncheon-ri, Gwangju (조선시대 관요인 광주 번천리 출토 백자의 기술적인 연구)

  • Gang, Gyung In
    • Journal of Conservation Science
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    • v.12 no.1 s.15
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    • pp.1-14
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    • 2003
  • Chemical characteristics of whitewares excavated from the of official kiln of the Choseon Dynasty period in Gwangju, Gyeonggido have been stuied using x-ray diffraction, inductively coupled plasma atomic absorption spectrometry and energy dispersive spectrometry. This study shows that most of whitewares excavated from the kiln site are similar in chemistry to each other regardless of their excavated positions and that the their bodies were not made of feldspar minerals. However, the whiteware from sedimentation 1 of waste articles shows mineralogical characters different from those of other sites. This result is in accordance with the report that the whitewares from sedimentation 1 of waste articles have characters different from other sites. The whiteware glaze was produced from raw minerals of both lime and alkali-lime system resulting in wide variation in chemical composition.

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A Comparative Study on the Decoration of Korean Celadon and Chinese Celadon in the 12th and 13th Centuries (12~13세기 고려청자와 중국청자의 장식디자인 비교 연구)

  • Yue, kun;Ren, chuan;Kim, Hea-jin
    • Journal of Digital Convergence
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    • v.17 no.3
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    • pp.427-432
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    • 2019
  • In the 12th century to the 13th century, was the heyday of celadon, Koryo celadon after experienced celadon firing technology of imitation to the peak period of the development of Chinese celadon, especially on decoration technology pioneered the self unique style, the way of engraving, $xi{\grave{a}}ngqi{\grave{a}}n$. During this period, the southern Song dynasty celadon in China also innovated in the mature celadon firing technology and became more distinctive. The decorative style also promoted the aesthetic interest of the Song dynasty. Celadon decoration is not only a decorative art of ceramic art, but also a representation of national cultural phenomenon with the traditional culture in the development of contemporary art, play a more important role and value.

The Properties of Permeability and Freeze-Thaw Resistance of Water-Permeable Paving Brick Using Wastes (폐기물을 이용한 투수블록의 투수성 및 동결융해저항 특성)

  • 신대용;한상목;김경남;이현종
    • Journal of the Korean Ceramic Society
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    • v.41 no.3
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    • pp.210-215
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    • 2004
  • Porous ceramics for water-permeable paving brick was prepared by the sintering of mixed materials comprising of sewage sludge ash, waste porcelain fragment, waste glaze and low-grade clay at 1,000$^{\circ}C$ for 2 h, and the physical $.$mechanical properties, the permeability and the freeze-thaw resistance of specimens with preparation parameters were investigated. The physical mechanical properties were increased in specimens while porosity and permeability were decreased with increasing sewage sludge ash content and sintering temperature on the properties of specimens showed the opposite results. The bulk density, porosity, compressive strength and permeability (passed charge) of 30A60F specimens with 30 wt% of sewage sludge ash content, waste porcelain fragment size with 1∼2 mm and sintered at 1,000$^{\circ}C$ for 2 h were 2.17, 46.2%, 221 kgf/$\textrm{cm}^2$ and 3,150 coulombs, respectively. The permeability was increased with increasing waste porcelain fragment size, however compressive strength was decreased. The freeze-thaw resistance of 30A60F specimen with 1∼2 mm of fragment size was superior to that of the other specimens. The 30A60F specimens can be used for the water-permeable paving brick with the high permeability and adequate strength. The heavy metals included in the all specimens showed lower than the standard level.

Translucency of ceramic veneers on glazing effect (세라믹 비니어의 글레이징에 따른 반투명도 변화)

  • Kim, Sung-Joon;Kahm, Se Hoon
    • The Journal of Korean Academy of Prosthodontics
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    • v.53 no.2
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    • pp.138-143
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    • 2015
  • Purpose: The aim of this study was to compare the translucency of two different laminate ceramic veneers with and without glazing. Materials and methods: Ten millimeter side square-shaped specimens in 0.3 mm and 0.6 mm thick were fabricated for the following materials with and without glazing (n=80): A1 shade IPS e.maxPress (IEM) and Styleveneers (STV). The color coordinates (CIE $L^*a^*b^*$) of the specimens were measured with a colorimeter. The Translucency parameter (TP) was calculated from the color difference of the material on a black versus a white background. For comparisons between materials and between the 'not glazed' and 'glazed' groups, unpaired t-test was used to analyze the data (P=.05). Results: The TP ($Mean{\pm}SD$) of 'not-glazed' and 'glazed' group of IEM specimens at 0.3 mm thickness were $45.99{\pm}3.00$ and $49.53{\pm}2.28$ and the TP at 0.6 mm thickness were $32.82{\pm}2.59$ and $43.02{\pm}0.98$, respectively. Likewise, the TP of 'not-glazed' and 'glazed' group of STV specimens at 0.3 mm thickness were $47.03{\pm}3.65$ and $50.95{\pm}3.05$ and the TP at 0.6 mm thickness group were $34.48{\pm}1.28$ and $43.39{\pm}1.20$, respectively. As the glazing of ceramic veneer differed, the TP of each ceramic veneer showed statistically significant difference. But, the result between the products was not statistically different. Conclusion: Within the limitations of this study, we are concluded that the glazing process changed translucency of laminate ceramic veneers and the TP would not be affected by products.

Study of Material Characteristics by a Componential Analysis on the Whiteware from the Kiln of Chiljeon-ri, Bangsan-myeon, Yanggu-gun (양구 방산 칠전리 출토 백자의 성분분석을 통한 원료특성 연구)

  • Ahn, Songyee;Hwang, Hyunsung
    • Journal of Conservation Science
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    • v.29 no.3
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    • pp.261-277
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    • 2013
  • This study aims to research the relationship between whitewares and their rare materials from the site of Yanggu and Bunwon through the componential characteristic of the excavated whitewares from the 1st and the 2nd kilns of Chiljeon-ri in Bangsan-myeon, Yanggu-gun. As a result, the sherds were devided according to the chemical compositions of the body and the glaze via their respective production era. However, it considered that the whitewares from Chiljeon-ri had been manufactured with geochemically similar materials and the production process, such as refining and combining materials, had been different. It assumed that the firing temperatures of the whitewares from Chiljeon-ri were around $1,100-1,200^{\circ}C$ and substantially lower than for general whitewares. In the componential analysis, there were disparate properties in the cobalt pigment, which contained trace elements and rare earth elements. A review of the literature revealed a correlation between the whitewares from the late Chosun kiln site in Bunwon-ri and the raw materials from Yanggu-gun, but this was there were various techniques for refining and combining materials in Bunwon-ri.

Characteristics and Production Period of Goryo(高麗) Iron 'Sung(成)' Inscribed Celadon (고려(高麗) 철화(鐵畵) '성(成)' 명청자(銘靑瓷)의 특징(特徵)과 제작시기(製作時期))

  • Han, Sung Uk
    • Korean Journal of Heritage: History & Science
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    • v.41 no.2
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    • pp.61-78
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    • 2008
  • Celadons painted in underglaze iron brown 'Sung(成)' inscription are characteristic celadons excavated only at the No. 7 kiln site located at Sadang-ri(沙堂里), Daegu-myeon(大口面), Gangjin-gun(康津郡), Jeollanamdo(全羅南道), Korea and has inscription in the inner center of the foot by brush. The inscription was marked where it is not easily seen. it can be assumed that since it showed a variety of hand writings, many people were involved in manufacturing these celadons and the 'Sung' inscription was marked after workshop rather than manufacturer. It was also found that quality of glaze, paste, shape, pattern and firing method were same and these were manufactured with the same techniques in the same period. Kinds of these celadons were mainly sets of tablewares including bowl with handle, bowl, plate, cup, bowl with cover and bottle. Raised relief designs using extrusion technic were especially preferred rather than incised designs and inlaid designs. Cases of using inlaid designs were not frequently found compared to incised designs, thus it can be assumed that in this period, inlaid designs were not generally used. Special designs having the meaning of authority or dignity such as chrysanthemum, peony, parrot and lotus plate designs were not found. Foot was molded with 'U' type except some bowls with cover and plates and firing was done after glazing the whole surface of the ceramic with the support of quartzite at 3 to 4 places of inner bottom of foot. Production period of these celadons with 'Sung' inscription can not be confirmed from other excavation sites outside of No. 7 kiln site at Sadang-ri since there are no other excavation sites whose relics bear 'Sung' inscription. Through comparison research with other relics bear the characteristics of these celadons from tombs, temple sites, shipwrecks, production period of these celadons with 'Sung' inscription can be assumed as second quarter of 13th century. And since the quality of these celadons are generally inferior to the top-quality celadons which were supplied to royal familes and high-ranking aristocrats, it can be deducted that these celadons with 'Sung' inscription were supplied to classes lower than royal familes and high-ranking aristocrats. So it is considered that Celadons with 'Sung' inscription have a great significance as a chronological material to complement the blank of the first half of the 13th century because most of celadons with raised relief designs and engraved relief designs were attributed to 12th century, the period of prosperity.