• Journal of the Korean Ceramic Society
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• v.55 no.4
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• pp.392-399
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• 2018

$C_f/SiC$ composites were prepared via a process combining chemical vapor infiltration (CVI) and precursor infiltration pyrolysis (PIP), wherein silicon carbide matrices were infiltrated into 2.5D carbon preforms. The obtained composites exhibited porosities of 20 vol % and achieved strengths of 244 MPa in air at room temperature and 423 MPa at $1300^{\circ}C$ under an Ar atmosphere. Carbon fiber pull-out was rarely observed in the fractured surfaces, although intermediate layers of pyrolytic carbon of 150 nm thickness were deposited between the fiber and matrix. Fatigue fracture was observed after 1380 cycles under 45 MPa stress at $1000^{\circ}C$. The fractured samples were analyzed by transmission electron microscopy to observe the distributed phases.

• Journal of the Korean Ceramic Society
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• v.46 no.3
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• pp.301-305
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• 2009

The novel carbon coating process for interlayer of fiber reinforced ceramic composites between fiber and matrix was performed by carbonizing phenolic resin solution that coated on fiber surface in $N_2$ atmosphere at $600^{\circ}C$ to improve the strength and fracture toughness of CMC(ceramic matrix composite). 160 nm carbon layer was coated on fiber surface with 5 vol% of phenolic resin solution. Since the process temperature ($600^{\circ}C$) is lower than chemical vapor deposition($900{\sim}1000^{\circ}C$), the strength and toughness could be preserved. Furthermore the coating thickness uniformity was improved to 8% of deviation along the stacking sequence. Therefore, prevention from fiber degradation during coating process and controlling coating thickness uniformity along the preform depth were achieved by coating with phenolic resin carbonizing method.

• Journal of the Korean Ceramic Society
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• v.40 no.7
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• pp.625-631
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• 2003

Recent work at USC has focused on strategies to enhance the toughness and overall mechanical performance of polymer foams for use in lightweight sandwich structures. Both mechanical and chemical approaches have been employed with reasonable success. Fiber reinforcement, though difficult from a processing perspective, can lead to substantial enhancements in toughness and strength, while reducing friability. Chemical modifications are also challenging from a processing perspective, but can produce similar enhancements in performance. Efforts to enhance performance of phenolic foam and PVC foam through fiber reinforcement and chemical modification are described, along with the resulting enhancements in performance.

• Journal of the Korean Society for Precision Engineering
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• v.23 no.5 s.182
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• pp.170-176
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• 2006

Multi-layered laminate made of ceramic/composite have been developed to prevent penetration by high velocity impact. In this study, three-layered plates consisted of 1) cover layer (glass fiber reinforced polymer), 2) $Al_{2}O_{3}$, ceramic plate, and 3) backing plate (glass fiber reinforced polymer) were fabricated with various conditions and tested for their ballistic protection characteristic. The ceramic composite laminates, with thin backing plate, were completely penetrated by armor piercing projectile. The plate with inserted rubber between ceramic and backing plate showed excellent ballistic protection, though completely penetrated by the second shoot.

• Macromolecular Research
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• v.13 no.1
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• pp.19-29
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• 2005

Polymer composites based on a thermotropic liquid-crystalline polymer (TLCP) and poly(butylene terephthalate) (PBT) were prepared using a melt blending process. Polymer composites consisting of bulk cheap polyester with a small quantity of expensive TLCP are of interest from a commercial perspective. The interactions between the PBT chains and the flexible poly(ethylene terephthalate) (PET) units in the TLCP phase resulted in an improvement in the compatibility of PBT/TLCP composites. TLCP droplets deformed and fragmented into smaller droplets in the PBT/TLCP composites, which resulted in TLCP fibrillation through the effective deformation of the TLCP droplets. The nucleation activities of the PBT/TLCP composites increased by adding even a small amount of the TLCP component.

• Journal of Korea Foundry Society
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• v.25 no.2
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• pp.88-94
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• 2005

The microstructure and mechanical property of the ceramic reinforced AC4C matrix composites processed by squeeze casting were investigated. In this study Kaowool and Saffil fiber which are ceramic reinforcements are used as preform materials. As a matrix material, Al-7wt.%Si-0.3wt.%Mg(AC4C) has been used. In case of Kaowool and Saffil/AC4C composites, 7.5 MPa squeezing pressure and minimum 7.0% binder amount are needed to produce sound composite materials. The tensile strength of Kaowool/ AC4C composite is lower than the matrix metal and this can be explained by the melt unfilling due to formed cluster of Kaowool reinforcements. But the mechanical properties of hardness, wear resistance and thermal expansion are better than the matrix materials due to the strengthening effect of ceramic reinforcements.

• Journal of the Korean Ceramic Society
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• v.32 no.7
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• pp.846-852
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• 1995

The multiply reinforced mullite-zirconia composites were prepared with addition of Al2O3 particles, platelets, and fibers. The sinter-HIP specimens (presintered at 1$700^{\circ}C$ and hipped at 1$600^{\circ}C$) showed that the fracture toughness of Al2O3 fiber reinforcement (4.4 MPa.{{{{ SQRT {m} }}) was higher than those of platelet (4.0 MPa.{{{{ SQRT {m} }}) and of particle (3.9MPa.{{{{ SQRT {m} }}) reinforcement, whereas the fracture strength of Al2O3 particle reinforcement (304 MPa) was higher than those of platelet (293MPa) and of fiber (248MPa) reinforcement.

• The Korean Journal of Ceramics
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• v.4 no.3
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• pp.245-248
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• 1998

Porous carbon fiber composites (CFCs) having variable specific surface area ranging 35~1150 $\m^2$/g were reacted to produce silicon carbide fiber composites with SiO vapor generated from a mixture of Si and $SiO_2$ at 1673 K for 2 h under vacuum. Part of SiO vapor generated during conversion process condensed on to the converted fiber surface as amorphous silica. Chemical analysis of the converted CFCs resulting from reaction showed that the products contained 27~90% silicon carbide, 7~18% amorphous silica and 3~63% unreacted carbon, and the composition depended on the specific carbide, 7~18% amorphous silica and 3~63% unreacted carbon, and the composition depended on the specific surface area of CFCs. CFC of higher specific surface area yielded higher degree of conversion of carbon to silicon and conversion products of lower mechanical strength due to occurrence of cracks in the converted caron fiber. As the conversion of carbon to silicon carbide proceeded, pore size of converted CFCs increased as a result of growth of silicon carbide crystallites, which is also linked to the crack formation in the converted fiber.

• Journal of the Korean Society for Precision Engineering
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• v.24 no.5
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• pp.82-88
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• 2007

This work is to fabricate a precise optical fiber array using polymer composite for optical interconnection. Optical fiber array has to satisfy low optical loss requirement less than 0.4 dB according to temperature change. For this purpose, design criteria for an optical fiber array was derived. The coefficient of thermal expansion of silica particulate epoxy composites was affected by volume fraction of silica particles. And also, elastic modulus of silica particulate epoxy composites was affected by volume fraction of silica particles. To obtain the coefficients of thermal expansion below $10{\times}10E-6/^{\circ}C$ and elastic modulus more than 20 GPa , we chose the volume fraction more than 76%. Using silica particulate epoxy composites with the volume fraction 76%, 8-channel optical fiber array with dimensional tolerances below $1\;{\mu}m$ was manufactured by transfer molding technique using dies with the uniquely-designed core pin and precisely-machined zirconia ceramic V block. These optical fiber arrays showed optical loss variations within 0.4 dB under thermal cycling test and high temperature test.

• The Korean Journal of Ceramics
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• v.4 no.3
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• pp.254-259
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• 1998

A kinetic model predicting the oxidation of carbon fiber reinforced glass matrix composites has been described. The weight loss of composites during oxidation implied that a gasification of carbon fiber takes place and the transport of reactants $(O_2)$ or product (CO or $CO_3$) in the glass matrix was partially the rate controlling step. The kinetic model in this study was based on the work of Sohn and Szekely which may be regarded as a generalization of numerous models in the gas-solid reaction system. A comparison of this model with experimental data is also presented.