Browse > Article
http://dx.doi.org/10.4191/KCERS.2009.46.3.301

Novel Phenol Resin Carbonizing Method for Carbon Interlayer Coating between Reinforcing Fiber and Matrix in Fiber Reinforced Ceramic Composite  

Kim, Se-Young (Reaction and Separation Material Research Center, Korea Institute of Energy Research)
Woo, Sang-Kuk (Reaction and Separation Material Research Center, Korea Institute of Energy Research)
Han, In-Sub (Reaction and Separation Material Research Center, Korea Institute of Energy Research)
Publication Information
Abstract
The novel carbon coating process for interlayer of fiber reinforced ceramic composites between fiber and matrix was performed by carbonizing phenolic resin solution that coated on fiber surface in $N_2$ atmosphere at $600^{\circ}C$ to improve the strength and fracture toughness of CMC(ceramic matrix composite). 160 nm carbon layer was coated on fiber surface with 5 vol% of phenolic resin solution. Since the process temperature ($600^{\circ}C$) is lower than chemical vapor deposition($900{\sim}1000^{\circ}C$), the strength and toughness could be preserved. Furthermore the coating thickness uniformity was improved to 8% of deviation along the stacking sequence. Therefore, prevention from fiber degradation during coating process and controlling coating thickness uniformity along the preform depth were achieved by coating with phenolic resin carbonizing method.
Keywords
Fiber; Coating; Composite; Interlayer; PyC;
Citations & Related Records

Times Cited By SCOPUS : 2
연도 인용수 순위
1 J. P. Singh, D. Singh, and M. Sutaria, 'Ceramic Composites: Roles of Fiber and Interface,' Comp.:Part A, 30 445-50 (1999)   DOI   ScienceOn
2 S. Kumar, and R. N. Singh, 'Effects of Coating Properties on Crack Propagation in Nicalon-fiber/sic-matrix Composites,' Comp. Sci. & Tech., 56 1271-81 (1996)   DOI   ScienceOn
3 Hua-Tay Lin, and Paul F. Becher, 'Effect of Fiber Coating on Lifetime of Nicalon Fiber-silicon Carbide Composites in Air,' Mat. Sci. & Eng. A, A231 143-50 (1997)   DOI   ScienceOn
4 D.B. Fischbach and P.M. Lemoine, 'Influence of a CVD Carbon Coating on the Mechanical Property Stability of Nicalon SIC Fiber,' Comp. Sci. & Tech., 37 55-61 (1990)   DOI   ScienceOn
5 T. Horikawa, K. Ogawa, K. Mizuno, J. Hayashi, and K. Muroyama, 'Preparation and Characterization of the Carbonized Material of Phenol-formaldehyde Resin with Addition of Various Organic Substances,' Carbon, 41 465-72 (2003)   DOI   ScienceOn
6 A. Kelly, and C. Zweben, 'Comprehensive Composite Materials:' Vol. 4, pp. 611-44, Elsevier science Ltd., Oxford, 2000
7 N. Kuentzer, P. Simacek, S. G. Advani, and S. Walsh, 'Correlation of Void Distribution to VARTM Manufacturing Techniques,' Comp. :Part A, 38 802-13 (2007)   DOI   ScienceOn
8 S. Wu, L. Cheng, L. Zhang, Y. Xu, J. Zhang, and H. Mei, 'Wet Oxidation Behaviors of Hi-Nicalon Fibers,' App. Surface Sci., 253 1447-50 (2006)   DOI   ScienceOn
9 J.H. Miller, P.K. Liaw, and J.D. Landes, 'Influence of Fiber Coating Thickness on Fracture Behavior of Continuous Woven Nicalon Fabric-reinforced Silicon-carbide Matrix Ceramic Composites,' Mat. Sci. & Eng. A, A317 49-58 (2001)   DOI   ScienceOn
10 G. Hackl, H. Gerhard, and N. Popovska, 'Coating of Carbon Short Fibers with Thin Ceramic Layers by Chemical Vapor Deposition,' Thin Solid Films, 513 217-22 (2006)   DOI   ScienceOn
11 W.D. Brouwer, E.C.F.C. van Herpt, and M. Labordus, 'Vacuum Injection Moulding for Large Structural Applications,' Comp. :Part A, 34 551-58 (2003)   DOI   ScienceOn
12 Michael D. Sacks, 'Effect of Composition and Heat Treatment Conditions on the Tensile Strength and Creep Resistance of SiC-based Fibers,' J. Euro. Ceram. Soc., 19 2305-15 (1999)   DOI   ScienceOn