• Journal of the Korean Ceramic Society
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• v.30 no.6
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• pp.492-498
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• 1993

The pretreatment condition for uniform distribution of SiC whisker in A2O3-SiCw composites has been determined and the mechanical properties of the composites with various whisker contents have been measured. Good dispersion of the whisker can be obtained in a solution of pH=10.45 by ball milling and ultrasonic treatment. The relative density of hot pressed composites decreases with the whisker content up to 40vol%, but is found to be satisfactory, over 98% for all samples. The mechanical property of the composites is sensitive to the whisker dispersion. Uniform distributjion of the whisker is critical in order to guarantee good mechanical property.The samples containing 20~30vol% whisker show the best mechanical property within the studied range.

• Journal of the Korean Ceramic Society
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• v.32 no.6
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• pp.643-652
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• 1995

Si-SiC-graphite composites were developed by incorporating solid lubricant graphite into Si-SiC, in the light of improving tribological properties of Si-SiC ceramics. Si-SiC-graphite composites were fabricated by infilterating silicon melt into the mixture of α-SiC, carbon black and graphite powder at 1750℃ under 3 Torr. The particle size of graphite was in the range of 150 to 500㎛, and the loading content of graphite was 0, 20, 25, 30, 35 vol% in the mixture of α-SiC and carbon black. The mechanical and tribological properties of this composites were studied. The density, hardness, flexural strength, compressive strength and Young's modulus were decreased with increasing of graphite content. An additiion of solid-lubricant graphite up to 30 vol% has improved tribological properties of Si-SiC ceramics without considerable degradation of mechanical properties.

• Journal of the Korean Ceramic Society
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• v.30 no.2
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• pp.139-147
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• 1993

Two sheets of high strength cement paste using ordinary Portland cement and water soluble polymer (polyacrylamide) were made by kneading with a twin roll mill. A carbon fiber layer out between two sheet of the cement paste, and then carbon fiber reinforced high strength cement composites were prepared by pressing them. The mechanical properties of the composites were investigated through the observation of the microstructure and the application of fracture mechanics. When the carbon fiber was added with 0.2 and 0.3wt% to the composites the flexural strength and Young's modulus were about 110∼116MPa and 74∼77GPa respectively, and critical stress intensity was about 3.14MPam1/2. It can be considered that the strength improvement of high strength cement fiber composites may be due to the removal of macropores and the increase of various fracture toughness effects; grain bridging, frictional interlocking, polymer fibril bridging and fiber bridging.

• The Korean Journal of Ceramics
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• v.5 no.1
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• pp.55-72
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• 1999

A cheallenge in the aerospace field is to design new composites satisfying specific and sometimes conflicting properties. The key steps are ⅰ)the understanding and the control of the reaction between the reinforcement and the embedding matrix, ⅱ) the achievement of a coherent and robust matrix. The problems encountered to prepare particulate, 1D, 2D and 3D reinforced composites using polymeric are discussed. Emphasis is given to the control of the micro/nanostructure using Raman microspectrometry and depth-sensing microindentation, in order to get information on the micromechanics and fiber structure simultaneously, within ceramic (CMC's) and metal matrix (MMC's) composites.

• Tribology and Lubricants
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• v.10 no.3
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• pp.39-46
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• 1994

In order to investigate the effect of the ceramic reinforcements on the wear properties of aluminum bronze composites, Cu-8wt%Al aluminum bronze alloys reinforced with the Saffil alumina short fiber were produced by the powder metallurgical method and tested by a pin-ondisc wear testing machine. The wear surfaces of the pin specimens and discs, wear debris, and the cross sections of the wear specimens were observed by SEM. The wear mechanism according to various wear conditions and the change of microstructure in the composites were also discussed. In the results, the reinforcement of the composites with alumina short fiber was very effective at the higher applied load over 10N. The material transportation to the counter disc was observed in the alloy specimens without reinforcements. However, the composites reinforced with ceramic particles and fibers showed the resistance against the material transportation.

• Journal of the Korean Ceramic Society
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• v.32 no.11
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• pp.1219-1226
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• 1995

Creep behaviors of Cr3C2 composites containing 90 wt% Cr3C2 and 10 wt% Ni were studied at high temperature. Compression tests at 100$0^{\circ}C$ and bending tests at 100$0^{\circ}C$ and 105$0^{\circ}C$ were done in argon environment. In all test conditions primary and steady-state creep behaviors were observed. Stress exponent and activatiion energy were determined from the experimental data. By microstructural analysis of Cr3C2 composites after creep test, the separate agglomerations of Ni phase were observed. Numerical analysis was also studied to analyze bending creep behaviors of Cr3C2 by assumming different tensile and compressive creep behavior in a bending sample. From the analysis, it was found that the stress state at the compressive region as applied stress increased. The observed creep rates were compared with the predicted creep rates by estimating power-law creep parameters from bending test data.

• Journal of the Korean Ceramic Society
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• v.43 no.8 s.291
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• pp.509-514
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• 2006

In this study, chopped Hi-Nicalon SiC fiber Reinforced Porous Reaction Bonded SiC (RBSC) composites and it fabrication process were developed by using Si melt infiltration process. The porosity and average pore size in fabricated chopped SiC fiber reinforced porous RBSC composites were in the range of $30{\sim}40%$ and $40-90{\mu}m$, which mainly determined by the SiC powder size used as starting material and amount of residual Si in porous composites. The maximum flexural strength of chopped SiC fiber reinforced porous RBSC composite was as high as 80 MPa. The delayed fracture behavior was observed in chopped SiC fiber reinforced porous RBSC composites upon 3-point bending strength test.

• Journal of the Korean Ceramic Society
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• v.28 no.12
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• pp.1012-1018
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• 1991

SiC whisker-reinforced LAS matrix composites were developed by a mixed colloidal processing route. An optimization of processing conditions was made using the zeta potential data of silica, boehmite, and SiC whisker dispersions. Similarly, the SiC whisker-reinforced composites were also fabricated by the conventional sol-gel process using the hydrolysis-condensation reaction of relevant metal alkoxides. The composites fabricated by the mixed colloidal processing route were characterized by a uniform spatial distribution of SiC whisker throughout the matrix. The fracture toughness increased from 1.3 MPa.m1/2 for the LAS specimen to 5.0 Mpa.m1/2 for the hot-pressed composite (95$0^{\circ}C$ and 20 MPa for 20 min) containing 20 wt% SiC whisker. The increase in fracture toughness appears to result mainly from the crack deflection and the crack bridging by whiskers with some additional toughenings from the whisker pullout and the matrix prestressing mechanisms.

• Journal of the Korean Ceramic Society
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• v.36 no.8
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• pp.799-804
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• 1999

Composites of SiC-Si3N4 consisted of uniformly distributed elongated $\beta$-Si3N4 grains and equiaxed $\beta$-SiC grains were fabricated with $\beta$-SiC,. $\alpha$-Si3N4 Al2O3 and Y2O3 powders. By hot-pressing and subsequent annelaing elongated $\beta$-Si3N4 grains were grown via$\alpha$longrightarrow$\beta$ phase transformation and equiaxed $\beta$-Si3N4 composites increased with increasing the Si3N4 content owing to the reduced defect size and enhanced crack deflection by elongated $\beta$-Si3N4 grains and the grain boundary strengthening by nitrogen incorporation. Typical flexural strength and fracture toughness of SiC-40 wt% Si3N4 composites were 783 MPa and 4.2 MPa.m1/2 respectively.

• Journal of the Korean Ceramic Society
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• v.37 no.8
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• pp.792-798
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• 2000

Alumina composites reinforced with SiC whiskers only or combinded with TiC particles were prepared by hot-pressing at 1850$^{\circ}C$ for 1h. The mechanical properties and microstructures of composites were investigated in this study. By of addition either 20 vol% SiC whiskers or 20 vol% TiC particles, the flexural strength fo alumina was increased from 360 MPa to 650 MPa or 730 MPa, respectively, and the KIC was also increased from 3.5 MPa$.$m1/2 to 5.5MPa$.$m1/2 or 4.4MPa$.$m1/2, respectively. In the case of composites with 20 vol% SiC whiskers and 2 vol% TiC particles. The flexural strength and KIC showed relatively high value of 800 MPa and 5.3MPa$.$m1/2, respectively. The improvement of mechanical properties was considered to be due to both the smaller average grain size and the crack deflection.