• 제목/요약/키워드: Centrifugal Melting Process

검색결과 28건 처리시간 0.022초

Fractional Melting에 의한 Si 정련에 관한 연구 (Refining of Silicon by Fractional Melting Process)

  • 김귀욱;윤우영
    • 한국주조공학회지
    • /
    • 제17권6호
    • /
    • pp.598-607
    • /
    • 1997
  • Fractional melting process involves heating an alloy within its liquid-solid region simultaneously ejecting liquid from the solid-liquid mixture. The extent of the purification obtained is comparable to that obtained in multi-pass zone refining. The new fractional melting process in which centrifugal force was used for separating the liquid from the mixture has been developed and applied to the purification of the metallic grade. Refining ratio depends on partition ratio, cake wetness and diffusion in the solid, and it was controlled by various processing parameters such as rotating speed and heating rate. The new parameter called "refining partition coefficient" has been suggested to estimate the effects of processing variables on the refining ratio. Because major impurities in MG-silicon such as Fe, Al, Ni have a low segregation coefficient, good purification effect is expected. The results of refining MG-silicon(98%) showed that 3N-Si was obtained in refined solid of 50% of the original sample.

  • PDF

원심성형법으로 제조한 고온초전도 튜브의 특성 분석 (Characteristics of HTS tube fabricated by centrifugal forming process)

  • 장건익;박용민
    • 한국초전도학회:학술대회논문집
    • /
    • 한국초전도학회 2000년도 High Temperature Superconductivity Vol.X
    • /
    • pp.211-215
    • /
    • 2000
  • Bi-2212 HTS tube was fabricated by CFP(Centrifugal Forming Process). Slury was prepared in the mixing ratio of 8:2 between powder and binder and ball-milled for 24 hrs. Slurry was initially charged into the rotating mold with 300${\sim}$450 rpm and heated at the temperature ranges of 840${\sim}$860$^{\circ}$C for partial melting to finally obtain a uniformly textured tube shape. It was observed the plate-like grains with more than 20 ${\mu}$m were well oriented along the rotating axis and the measured T$_c$ was around 67K. In this paper we will discuss and analyze the tube characteristics depending on many different processing parameters such as, powder composition, binder mixing ratio between powder and binder, motor speed, heating temperature and etc.

  • PDF

원심성형법을 이용한 BSCCO계 고온초전도체 제조 및 특성 분석 (Fabrication and Characterization of BSCCO System High-Temperature Superconductor Using Centrifugal Forming Process)

  • 박용민;장건익
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2000년도 하계학술대회 논문집
    • /
    • pp.189-192
    • /
    • 2000
  • High-temperature superconductor of Bi-2212 system was fabricated by CFP(centrifugal forming process). To make a uniform specimen slurry was prepared in the ratio of 7:3(powder:binder) and ball milled for 24 hours. Milled slurry was charged into a rotating mold with 450 rpm and dried at room temperature. Then the specimen was performed binder burn-out at 35$0^{\circ}C$ and heated for partial melting to 86$0^{\circ}C$. XRD analysis of most specimens were shown 2212 phase and observed a local plate shaped microstructure with a well aligned c-axis direction from SEM images. T$_{c}$(Critical temperature) of Bi-2212 was 64K.K.

  • PDF

원심성형법을 이용한 BSCCO계 고온초전도튜브 제조 및 특성 분석 (Fabrication and Characterization of BSCCO System High-Temperature Superconductor Tube Using Centrifigal Forming Process)

  • 박용민;장건익
    • 한국전기전자재료학회논문지
    • /
    • 제13권9호
    • /
    • pp.801-804
    • /
    • 2000
  • High-temperature superconductor of Bi-2212 system was fabricated by CFP(Centrifugal Forming Process). To make a uniform specimen slurry was prepared in the ratio of 7:3(powder : binder) and ball milled for 24 hours. Milled slurry was charged into a rotating mold with 450 rpm and dried at room temperature. Then the specimen was performed binder burn-out at 35$0^{\circ}C$ and heated for partial melting to 86$0^{\circ}C$. XRD analysis of most specimens were shown 2212 phase and observed a local plate shped microstructure with a well aligned c-axis direction from SEM images. Measured T$_{c}$(Critical temperature) was about 64 K.K.

  • PDF

원심주조법에 의한 주철-Babbitt Metal 복합관 제조에 관한 연구 (A Study on the Fabrication of Cast Iron-Babbitt Metal Composite Pipes by Centrifugal Casting Process)

  • 이충도;강춘식
    • 한국주조공학회지
    • /
    • 제13권1호
    • /
    • pp.42-49
    • /
    • 1993
  • Conventional manufacturing process for cast iron-babbitt metal composite is complicate and bimetallic bonding by centrifugal casting is also difficult because their melting point is largely different and nonmetallic inclusion exists on outer shell. This study is aiming to simplify multistage process by adding Cu-powder as insert metals during cast iron solidification. The variables on fabrication of composite pipe are mold rotating speed and inner surface temperature of outer metal. The optimum temperature range for fusion bonding between cast iron and Cu-layer was $1100^{\circ}C-1140^{\circ}C$ in case of mold rotating speed was 700rpm. When the inner surface of Cu-layer was at $900^{\circ}C$, the value of interfacial hardness between Cu-layer and babbitt metal were higher than Cu-matrix by forming diffusion layer, interfacial products between Cu-layer and babbitt metal are proved to be $Cu_6Sn_5({\eta})$by XRD.

  • PDF

The Effect of Processing Parameters on HTS Tube Characteristics

  • Jung, Sengho;Jang, Guneik;Ha, Dongwoo;Sung, Taehyun
    • Transactions on Electrical and Electronic Materials
    • /
    • 제5권2호
    • /
    • pp.55-60
    • /
    • 2004
  • High-temperature Superconductor(HTS) tubes were fabricated in terms of different chemical compositions and various SrSO$_4$additions by centrifugal forming method. For powder melting by induction the optimum range of melting temperatures and preheating temperature were 1050$^{\circ}C$, 1100$^{\circ}C$ and 550$^{\circ}C$ for 30 min, respectively. The mould rotating speed was 1000 rpm. A tube was annealed at 840$^{\circ}C$ for 72 hours in oxygen atmosphere. The plates like grains more than 20 $\mu\textrm{m}$ were well developed along the rotating direction of mould regardless of initial chemical compositions and the amounts of SrSO$_4$in Bi2212. The specimen with Bi2212 composition exhibited T$\_$c/ of 83 K, while the specimens fabricated with other compositions are lower than 60 K. The measured I$\_$c/ and J$\_$c/ at 77 K(B = 0 T) in Bi2212 with 7 % SrSO$_4$ composition were about 680 A and 380 A/$\textrm{cm}^2$.

초고속 용융 원심방사를 이용한 폴리에틸렌 마이크론 섬유의 제조 (Preparation of Polyethylene Micro-fibers by High Speed Centrifugal Melt Spinning)

  • 양성백;이정언;지병철;주남식;염정현
    • 한국염색가공학회지
    • /
    • 제32권4호
    • /
    • pp.239-244
    • /
    • 2020
  • Polyethylene (PE) micro-fiber have been prepared at different hot air temperature (60, 80 and 100 ℃) and different pressure (20, 40, 60 and 80 kPa) by melt centrifugal spinning technique. The parameters of melting centrifugal spinning including polymer contents, rotational velocity, temperature of hot air and pressure were optimized for the fabrication process. The study showed that 8000 rpm rotational velocity, 80 ℃ heated hot air and 40 kPa air pressure are the best condition to obtain uniform and strong PE fiber. The prepared PE fibers were analyzed by field emission scanning electron microscope and universal testing machine and found that fibers with reduced diameter and improved tensile strength are obtained at hot air condition.