• Carbon letters
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• v.12 no.4
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• pp.249-251
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• 2011

Carbon/epoxy woven composites are prominent wear-resistant materials due to the strength, stiffness, and thermal conductivity of carbon fabric. In this study, the effect of oilabsorption on the wear behaviors of carbon/epoxy woven composites was investigated. Wear tests were performed on dry and fully oil-absorbed carbon/epoxy woven composites. The worn surfaces of the test specimens were examined via scanning electron microscopy to investigate the wear mechanisms of oil-absorbed carbon/epoxy woven composites. It was found that the oil absorption rate was 0.14% when the carbon/epoxy woven composites were fully saturated. In addition, the wear properties of the carbon/epoxy woven composites were found to be affected by oilabsorption. Specifically, the friction coefficients of dry and oil-absorbed carbon/epoxy woven composites were 0.25-0.30 and 0.55-0.6, respectively. The wear loss of the oilabsorbed carbon/epoxy woven composites was $3.52{\times}10^{-2}\;cm^3$, while that of the dry carbon/epoxy woven composites was $3.52{\times}10^{-2}\;cm^3$. SEM results revealed that the higher friction coefficient and wear loss of the oil-absorbed carbon/epoxy woven composites can be attributed to the existence of broken and randomly dispersed fibers due to the weak adhesion forces between the carbon fibers and the epoxy matrix.

• Carbon letters
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• v.12 no.3
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• pp.177-179
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• 2011

The use of carbon nanotubes (CNTs) as a reinforcing material in a polymer matrix has increased in various industries. In this study, the flexural behavior of CNT-modified epoxy/basalt (CNT/epoxy/basalt) composites is investigated. The effects of CNT modification with silane on the flexural properties of CNT/epoxy/basalt composites were also examined. Flexural tests were performed using epoxy/basalt, oxidized CNT/epoxy/basalt, and silanized CNT/epoxy/basalt multi-scale composites. After the flexural tests, the fracture surfaces of the specimens were examined via scanning electron microscopy (SEM) to investigate the fracture mechanisms of the CNT/epoxy/basalt multi-scale composites with respect to the CNT modification process. The flexural properties of the epoxy/basalt composites were improved by the addition of CNTs. The flexural modulus and strength of the silane-treated CNT/epoxy/basalt multi-scale composites increased by approximately 54% and 34%, respectively, compared to those of epoxy/basalt composites. A SEM examination of the fracture surfaces revealed that the improvement in the flexural properties of the silane-treated CNT/epoxy/basalt multi-scale composites could be attributed to the improved dispersion of the CNTs in the epoxy.

• Journal of Ocean Engineering and Technology
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• v.11 no.2
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• pp.48-56
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• 1997

This work has been investigated in order to study the influence of the moisture absorption on the mechanical pf the glass fiber/epoxy resein composites and the carbon fiber/epoxy resein composites. The types of glass fiber used in the glass fiber/epoxy resein composites were randomly oriented fiber and plain fabric fiber. And carbon fiber.epoxy resein composites was laminated with fabric prepreg which was formed with carbon fiber and epoxy resein. Both composites were immersed up to 100 days in distilled water at $80^{\circ}C$, and then dried up to 3 days in an oven at 80$80^{\circ}C$. Both composites were measured for the weight gain of water(wt.%) and tensile strength through immersion and dry time. Consequently, it was found that the tensile strength of thw glass fiber/epoxy resein composites and the carbon fiber/epoxy resein composites were reduced proportionally to the moisture absortion rate. Also, the tensile strength of glass fiber composites was decreased more than that of the carbon fiber composites. Additionally, it was found that the tensile strength of all composites which decreased by moisture absorption were partly recovered by drying in an oven at 80$80^{\circ}C$.

• Carbon letters
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• v.14 no.3
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• pp.190-192
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• 2013

It has been demonstrated in a previous study that carbon nanotube (CNT)/epoxy/basalt composites produce better flexural properties than epoxy/basalt composites. In this study, mode I fracture tests were conducted using CNT/epoxy/basalt composites with and without seawater absorption in order to investigate the effect of the seawater absorption on the mode I fracture toughness ($G_{Ic}$) of the CNT/epoxy/basalt composites. The results demonstrated that the compliance of the seawater-absorbed specimen was larger than that of the dry specimen at the same crack length, while the opposite result was obtained for the fracture load. The $G_{Ic}$ value of the seawater-absorbed CNT/epoxy/basalt composites was approximately 20% lower than that of the dry CNT/epoxy/basalt composites.

• Journal of the Korean Society for Precision Engineering
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• v.27 no.12
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• pp.113-118
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• 2010

For a present study, woven type carbon fibers were surface-modified by oxygen plasma to improve adhesive strength between carbon fibers and epoxy. The change of hydrophilic properties by the plasma modification was investigated through the contact angle measurement and the calculation of surface energy of carbon fiber due to the oxygen plasma modification. FESEM and XPS analyses were performed to study the chemical and physical changes on the surface of carbon fibers due to the oxygen plasma modification. Pin-on-disk wear tests were conducted under dry condition using unmodified and plasma-modified carbon/epoxy composites to investigate the effect of plasma modification on the wear behavior of woven type carbon/epoxy composites. The results showed that the friction coefficient and the wear rate of plasma-modified carbon/epoxy composites were lower than those of unmodified carbon/epoxy composites, respectively. XPS analysis showed that new functional group of a carbonyl type was created on the carbon fibers by the $O_2$ plasma treatment, which enhanced adhesive strength between carbon fibers and epoxy, leading to improve wear properties

• Composites Research
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• v.34 no.2
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• pp.82-87
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• 2021

The mechanical properties of carbon fiber-reinforced epoxy composites (CFRPs) are greatly dependent on the interfacial adhesion between the carbon fibers and the epoxy matrix. Introducing nanomaterial reinforcements into the interface is an effective approach to enhance the interfacial adhesion of CFRPs. The main purpose of this work was to introduce graphitic nanofiber (GNFs) between an epoxy matrix and carbon fibers to enhance interfacial properties. The composites were reinforced with various concentrations of GNFs. For all of the fabricated composites, the optimum GNF content was found to be 0.6 wt%, which enhanced the interlaminar shear strength (ILSS) and fracture toughness (KIC) by 101.9% and 33.2%, respectively, compared with those of neat composites. In particular, we observed a direct linear relationship between ILSS and KIC through surface free energy. The related reinforcing mechanisms were also analyzed and the enhancements in mechanical properties are mainly attributed to the interfacial interlocking effect. Such an effort could accelerate the conversion of composites into high performance materials and provide fundamental understanding toward realizing the theoretical limits of interfacial adhesion and mechanical properties.

• Carbon letters
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• v.22
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• pp.36-41
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• 2017

Biodegradable epoxy (B-epoxy) was prepared from diglycidyl ether of bisphenol A and epoxidized linseed oil. The mechanical properties of B-epoxy composites reinforced with multi-walled carbon nanotubes (MWCNTs/B-epoxy) were examined by employing dynamic mechanical analysis, critical stress intensity factor ($K_{IC}$) tests, and impact strength tests. The electromagnetic interference shielding effectiveness (EMI-SE) of the composites was evaluated using reflection and absorption methods. Mechanical properties of MWCNTs/B-epoxy were enhanced with an increase in the MWCNT content, whereas they deteriorated when the MWCNT content was >5 parts per hundred resin (phr). This can likely be attributed to the entanglement of MWCNTs with each other in the B-epoxy due to the presence of an excess amount of MWCNTs. The highest EMI-SE obtained was ~16 dB for the MWCNTs/B-epoxy composites with a MWCNT content of 13 phr at 1.4 GHz. The composites (13 phr) exhibited the minimum EMI-SE (90%) when used as shielding materials at 1.4 GHz. The EMI-SE of the MWCNTs/B-epoxy also increased with an increase in the MWCNT content, which is a key factor affecting the EMI-SE.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2002.10a
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• pp.15-19
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• 2002

In this work, the surface modification of carbon/epoxy composites was investigated using UV (ultraviolet ray) surface treatment to increase adhesion strength between the carbon/epoxy composites and adhesives. After UV surface treatment, XPS (X-ray photoelectron spectroscopy) tests were performed to analyze the surface characteristics of the carbon/epoxy composites. Comparing adhesion strengths with the surface characteristics, the effects of the surface modification of carbon/epoxy composites by UV surface treatments on the adhesion strengths were investigated.

• Carbon letters
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• v.12 no.1
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• pp.53-56
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• 2011

This study aimed to investigate the influence of mesoporous carbons on the thermal insulation properties of epoxy/mesoporous carbon composites. The mesoporous carbon (CMK-3) was prepared by conventional templating method using SBA-15. The epoxy/mesoporous carbon composites were prepared by mixing the synthesized CMK-3 with diglycidylether of bisphenol A (DGEBA). As experimental results, the curing reactivities of the DGEBA/CMK-3 composites were found to decrease with the addition of the CMK-3. Also, the thermal conductivities of DGEBA/CMK-3 composites were found to decrease with increasing CMK-3 content. This could be interpreted in terms of the slow thermal diffusion rate resulting in pore volume existing in the gaps in the interfaces between the mesoporous carbon and the DGEBA matrix.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.06a
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• pp.663-667
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• 2005

Surface modified carbon nanotubes were applied into the epoxy composites to investigate its tribological property. Carbon nanotubes reinforced epoxy composites were fabricated by casting. Effects to the tribological property of loading concentrations and types of surface modification of carbon nanotubes were investigated under sliding condition using linear reciprocal sliding wear tester. The results show that the small amount of carbon nanotubes into the epoxy exhibited lower weight loss than the pure epoxy. It is concluded that the effect of an enormous aspect ratio of carbon nanotubes surface area which wider than conventional fillers that react as interface for stress transfer. As increased the contents of carbon nanotubes, the weight loss from the wear test was reduced. And the surface modified carbon nanotubes show better tribological property than as produced carbon nanotubes. It is due that a surface modification of carbon nanotubes increases the interfacial bonding between carbon nanotubes and epoxy matrix through chemical bonding. Changes in worn surface morphology are also observed by optical microscope and SEM for investigating wear behaviors. Carbon nanotubes in the epoxy matrix near the surface are exposed, because it becomes the lubricating working film on the worn surface. It reduces the friction and results in the lower surface roughness morphology in the epoxy matrix as increasing the contents of the carbon nanotubes.