• Journal of Food Hygiene and Safety
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• v.36 no.5
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• pp.376-381
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• 2021

Red beet (Beta vulgaris L.) is a root vegetable and a popular functional food ingredient of dark red-purple appearance due largely to betacyanins, principally betanine (75-95%) and its isomer, isobetanine (15-45%). This study developed an analytical method for beet red in terms of betanine and isobetanine in processed food products labeled with beet red as a food additive. High Performance Liquid Chromatography-Diode Array Detector (HPLC-DAD) was used with a C₁₈ column. Linearity, limit of detection (LOD), limit of quantitation (LOQ), accuracy, precision and uncertainty in measurement were calculated for method validation. Matrix-matched calibration was applied to the candy, ice cream, and cocoa product, respectively, and R² was ≥0.9998, showing a high level of linearity. The LOD and LOQ were 0.16 to 0.32 and 0.48 to 0.97 mg/L, respectively. As a result of repeated intra-day and interday experiments to validate the accuracy and precision of the analytical method, the recovery rates were 96.0-103.1% and 100.0-102.2%, respectively and the RSD% was 0.5-3.3% and 0.9-3.8%, respectively. Moreover, the measurement uncertainty was estimated to be 1.71-12.43% depending on the matrix and the measured concentration. In this study, betanine and isobetanine were quantified (8.4-3,823.4 mg/kg) by applying the developed analytical method to processed food products (n= 26; e.g., candy, ice cream, and other processed foods) labeled with beet red as a food additive.

• Journal of Korea Water Resources Association
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• v.57 no.9
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• pp.585-598
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• 2024

To mitigate natural disasters and efficiently manage water resources, it is essential to enhance hydrologic prediction while reducing model structural uncertainties. This study analyzed the impact of lumped and semi-distributed GR4J model structures on simulation performance and evaluated uncertainties with and without data assimilation techniques. The Ensemble Kalman Filter (EnKF) and Particle Filter (PF) methods were applied to the Namgang Dam basin. Simulation results showed that the Kling-Gupta efficiency (KGE) index was 0.749 for the lumped model and 0.831 for the semi-distributed model, indicating improved performance in semi-distributed modeling by 11.0%. Additionally, the impact of uncertainties in meteorological forcings (precipitation and potential evapotranspiration) on data assimilation performance was analyzed. Optimal uncertainty conditions varied by data assimilation method for the lumped model and by sub-basin for the semi-distributed model. Moreover, reducing the calibration period length during data assimilation led to decreased simulation performance. Overall, the semi-distributed model showed improved flood simulation performance when combined with data assimilation compared to the lumped model. Selecting appropriate hyper-parameters and calibration periods according to the model structure was crucial for achieving optimal performance.

• Journal of Korean Society for Atmospheric Environment
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• v.15 no.4
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• pp.403-415
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• 1999

To properly assess air pollution levels, application of quality assurance and quality control(QA/QC) is believed to be an essential step. In order to cope with such scientific principle, a field study was designed with an aim of comparing: 1) the methods of calibration for airborne pollutants and 2) the protocols developed for their measurements. Measurements were made at Han Yang University, Seoul during 29 May through 1 June 1998 under the management of the Division of Measurements and Analysis(DMA) of Korean Society for Atmospheric Environment(KOSAE). In this work, we report our results of intercomparative measurements on several gaseous criteria pollutants that were investigated mainly by the two institutes-Seoul National University(SNU) and the Korean Research Institute for Standards and Science(KRISS). Although measurements of major gaseous pollutants had been made routinely by many scientific institutes and organizations in Korea, most scientists involved in those studieswere obliged to do their experiments on the basis of their own procedural steps spaning from the preparation of gaseous standards to the methodological selections for the calibration. Hence, this campaign offered a unique opportunity to examine many important aspects on the measurements of these important gaseous pollutants. In the course of our study, we investigated the compatibility of data sets obtained by the two institutes in concert with reference data sets collected concurrently from a government-managed monitoring station. On the basis of our study, we conclude that different data sets made by different participants during this campaign agree well within the reasonable range of uncertainties.low, which indicated that during this period the potential acidity of precipitation was high but the neutralizing capacity was low. For Spring, pAi was very low but pH was slightly high. This was likely due to the large amount of $CaCO_3$ in the soil particles transported over a long range from the Chinese continent that were incorporated into the precipitation, and then neutralized the acidifying species with its high concentraton.

• Journal of the Korean Society for Nondestructive Testing
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• v.20 no.3
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• pp.206-212
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• 2000

The guided wave mode conversion phenomena were investigated for the NDE of a plate-like structure with thickness variation. The ratios of reflection and transmission (R/T) were measured via the self-calibrating procedure which allows us to obtain experimental guided wave data in a more reliable way regardless of the coupling uncertainty between transducer & specimen. The results on R/T could be used to determine the thickness reduction of the structure. It was shown that not only the incident modes but also the converted ones need to be considered in the self-calibrating guided wave inspection to extract a reasonable correlation between experimental data & the thickness variation. Through this study, the potential of guided wave inspection as a quantitative NDE technique was explored based on the combined concept of self-calibration & multi-mode conversion in guided wave scattering problems.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.26 no.11
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• pp.1613-1621
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• 2002

An electromagnetic flowmeter(EMF) essentially averages the velocity distribution over the pipe cross- sectional area, and the measured value is dependent on the velocity profiles. In this study, installation effects of 90$^{\circ}$long elbow(KS B 1522, ISO 3419) on the EMF characteristics was investigated. A commercial EMF was adopted and the distribution of magnetic field in the electrodes cross section was measured. In the experiment, the national flow standard system, of which measurement uncertainty was evaluated in accordance with ISO 17025 recommendation, was used fur characterization of EMF. The leading line has 150D long straight pipe to established a fully developed flow before entering into the elbow and the elbow was installed downstream of it. then the flowmeter was tested within 50 D from the elbow. The installation effects of the flowmeter were investigated by varying the mean velocity(Reynolds No.)in pipe section, the locations and the direction of electrodes plane.($\phi$) From the experimental results, we find the optimal conditions to get most accurate measurements. Generally, the deviations from the calibration value were less than 0.5 % in farther than 10D distance from the elbow and the direction of electrode plane. $\phi$ = 90$^{\circ}$yielded the smallest measurement deviation. These characteristics were shown consistently in turbulent region regardless of the mean Reynolds number.

• Proceedings of the Korean Society of Medical Physics Conference
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• 2002.09a
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• pp.294-297
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• 2002

For the quality control procedure of diagnostic x ray units, a method for simultaneous measurement of air kerma, half value layer and tube potential was developed utilizing a computed radiography system for intraoral radiography and film badge case. The response of average pixel values under the windows were calibrated by x rays generated at tube potentials from 40 to 140 kV with filtration from 1.5 to 3.7 mmAl. The calibration curves for half value layer and tube potential were derived as functions of attenuation factors by the 1.4 mmAl filter and the 0.2 mmCu filter. The energy dependency of the open window response was corrected by the calibration factor as a function of the attenuation factor by the 1.4 mmAl filter. The uncertainty of the estimated half value layer, tube potential and air kerma were 0.2 mmAl, 3.6 % and 5 %, respectively. It was thus suggested that this system could be applied to quality control program to detect the variation of working condition of x ray units in clinical use.

• Progress in Medical Physics
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• v.24 no.3
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• pp.140-144
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• 2013

In this research, the glass dosimeter was calibrated to measure the standard absorbed dose of the Cs-137 irradiator and absorbed dose in a biological sample. Absorbed dose in water for Cs-137 gamma ray was determined by the IAEA TRS-277 protocol. The PTW-TM30013 ion chamber and the PTW-TM41023 water phantom were utilized for measuring absorbed dose and the value was compared with the reading from DoseAce GD-302M glass dosimeter from Asahi Techno Glass Corporation for its calibration. The uncertainty of measurement ($1{\sigma}$) of the calibrated glass dosimeter was 2.7% and this result would be applied to improve the accuracy in measurement of absorbed dose in a biological sample.

• The Journal of the Acoustical Society of Korea
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• v.24 no.4
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• pp.194-201
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• 2005

Since the necessity for the accurate measurement in the field of acoustics, vibration, and ultrasound was internationally increased, CCAUV (Consultative Committee for Acoustics , Ultrasound and Vibration) was created by the CIPM (International Committee for Weights and Measures) in 1998. One of the first activities of CCAUV is the key comparison on 1' standard microphones. The key comparison was done from April. 1999 to April. 2001 and 12 NMIs(National Metrology Institutes) including KRISS (Korea Research Institute of Standards and Science) were participated. The pilot laboratory was the National Physical Laboratory(NPL). The traveling standards were two LSIP(Laboratory Standard 1' Pressure Type) microphones specified in IEC 61094-1 and the calibration frequency ranges covers from 63Hz to 8kHz. In this paper, the analyzed results in the final report were summarized.

• The Journal of Korean Institute of Electromagnetic Engineering and Science
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• v.24 no.1
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• pp.47-54
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• 2013

This paper introduces a W-band millimeter-wave power standard transfer system using the direct comparison method. The transfer system was developed to evaluate the effective efficiency and calibration factor of a W-band waveguide power sensor. The evaluation method and the measured results of the directional coupler that characterizes the calibration system are studied. The uncertainties of the standard transfer system are investigated, and the major uncertainty contributors are discussed as well. The performance of the realized W-band power standard transfer system was verified by comparing results with reference values.

• Journal of the Computational Structural Engineering Institute of Korea
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• v.24 no.4
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• pp.383-389
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• 2011

In this paper, a statistical calibration method is proposed in order to identify the variability of complex modulus for a rubber material due to operational temperature and experimental/model errors. To describe temperature- and frequency-dependent material properties, a fractional derivative model and a shift factor relationship are used. A likelihood function is defined as a product of the probability density functions where experimental values lie on the model. The variation of the fractional derivative model parameters is obtained by maximizing the likelihood function. Using the proposed method, the variability of a synthetic rubber material is estimated and applied to a rubber mount problem. The dynamic characteristics of the rubber mount are calculated using a finite element model of which material properties are sampled from Monte Carlo simulation. The calculated dynamic stiffnesses show very large variation.