• Title/Summary/Keyword: Calibration of PIXE

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PIXE Analysis of Aerosol Particles - Preparation of Standard Samples and Calibration Test - (PIXE 분석에 의한 대기에어로졸의 원소분석 -표준시료의 작성 및 정량화-)

  • 崔琴簒
    • Journal of Korean Society for Atmospheric Environment
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    • v.7 no.2
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    • pp.114-118
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    • 1991
  • Particle Induce X-Ray Emission (PIXE) analysis is one of the most useful methods which can determine the elemental concentration of aerosol particles in nano-gram range. The main purpose of this paper is to establish the measurement system and the procedure of PIXE analysis. The standard samples were prepared to calibrate the PIXE analysis by three different techniques. The linear relationships between the peak counts from PIXE spectra and the mass density from RBS spectra were obtained for each standardized element under the applied measurment geometry and conditions. The sensitivity curves for PIXE analysis were determined from these relationships.

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Evaluation of Quantitative Results of PIXE Analysis (다원소 동시분석법 PIXE법의 정량성 평가)

  • Park, Jeong-Ho;Choi, Kum-Chan
    • Analytical Science and Technology
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    • v.10 no.5
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    • pp.386-394
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    • 1997
  • The standard samples for the calibration of PIXE analysis were prepared using the single element standard samples and sulfur and chlorine compounds. The diluted standard solutions were dropped on the non-hole nuclepore film and dried. Standard sample of six elements of Ca, Cr, Co, Cu, Se and Sr had close agreement between the measurement and theoretical values. According to the theoretical study about the effects of thick samples on the accuracy of the PIXE analysis, the reduction of X-ray yields in the thick sample can not be neglected for the sample thicker than $100{\mu}g/cm^2$.

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Setup and Atomic Calibration of Particle Induced X-ray Emission System

  • Song, Jin-Ho;Song, Jae-Bong;;Kim, Jun-Gon
    • Proceedings of the Korean Vacuum Society Conference
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    • 2014.02a
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    • pp.206.2-206.2
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    • 2014
  • Recently, particle induced X-ray emission (PIXE) analysis system was installed at the 2MV ion acceleration system in Korea institute science and technology (KIST). This installation is for complement to low atomic resolution of heavy atoms at Rutherford backscattering spectrometry (RBS) system. For quantitative analysis, a mass calibration of the PIXE set-up has been done with thin film standards and. The GUPIX software package has been used to process the PIXE spectra and the results are compared with the values from RBS system. Therefore, the instrumental constant H (solid angle and correction factor) is determined relying completely on the GUPIX data base (cross-sections, fluorescence and Coster-Kronig probabilities, stopping powers and attenuation coefficients) for a large set of elements. These H values can be used in future analysis.

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Preliminary Study on the Elemental Quantification of in Ambient Liquid Samples of Microliter Volume Using the In-air Micro-PIXE Technique

  • Ma, Chang-Jin;Lim, Cheol-Soo;Sakai, Takuro
    • Asian Journal of Atmospheric Environment
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    • v.11 no.1
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    • pp.54-60
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    • 2017
  • Quantifying the trace elements in infinitesimal ambient liquid samples (e.g., single raindrop, cloud/fog water, and the soluble fraction extracted from the particles collected for a short time) is an important task for understanding formation processes, heating/cooling rates, and their health hazards. The purpose of this study is to employ an in-air micro PIXE system for quantitative analysis of the trace elements in a thimbleful of reference liquid sample. The bag type liquid sample holder originally designed with $10{\mu}m$ thick $Mylar^{(R)}$ film retained the original shape without any film perforation and apparent peaks of film blank by the end of the analysis. As one of tasks to be solved, the homogeneity of the elemental distribution in liquid reference species was verified by the X-ray line profiles for several references. It was possible to resolve the significant peaks for whole target elements corresponding to the channel number of micro-PIXE spectrum. The calibration curves for the six target elements (Si, S, Cl, Fe, Ni, and Zn) in standard solutions were successfully plotted by concentration (ppm) and ROI of interest net counts/dose (nC).

A Study on the Mark Reader Using the Image Processing (영상처리를 이용한 Mark 판독 기법에 관한 연구)

  • 김승호;김범진;이용구;노도환
    • 제어로봇시스템학회:학술대회논문집
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    • 2000.10a
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    • pp.83-83
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    • 2000
  • Recently, Vision system has being used all around industry. Sensor systems are used for Mark Reader, for example, optical scanning is proximity sensor system, have many disadvantages, such as, lacking user interface and difficulty to store original specimens. In contrast with this, Vision systems for Mark Reader has many advantages, including function conversion to achieve other work, high accuracy, high speed, etc. In this thesis, we have researched the development of Mark Reader by using a Vision system. The processing course of this s)'stem is consist to Image Pre-Processing such as noise reduction, edge detection, threshold processing. And then, we have carried out camera calibration to calibrate images which are acquired from camera. After searching for reference point within scanning area(60pixe1${\times}$30pixe1), we have calculated points crossing by using line equations. And then, we decide to each ROI(region of interest) which are expressed by four points. Next we have converted absolute coordinate into relative coordinate for analysis a translation component. Finally we carry out Mark Reading with images classified by six patterns. As a result of experiment which follows the algorithm has proposed, we have get error within 0.5% from total image.

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