• YAKHAK HOEJI
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• v.48 no.1
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• pp.60-64
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• 2004

Near-infrared (NIR) spectroscopy was used to determine rapidly and nondestructively the content of ambroxol in intact ambroxol tablets containing 30 mg (12.5％ m/m nominal concentration) by collecting NIR spectra in range 1100-1750 nm. The laboratory-made samples had 10.3∼15.9％ m/m nominal ambroxol concentration. The measurements were made by reflection using a fiber-optic probe and calibration was carried out by partial least square regression (PLSR) with autoscaling. Model validation was performed by randomly splitting the data set into calibration and validation data set (7 samples as a calibration data set and 5 samples as a validation data set). The developed NIR method gave results comparable to the known values of tablets in a laboratorial manufacturing Process, standard error of calibration (SEC) and standard error of prediction (SEP) being 0.49％ and 0.49％ m/m respectively. The method showed good accuracy and repeatability NIR spectroscopic determination in intact tablets allowed the potential use of real time monitoring for a running production process.

• ETRI Journal
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• v.35 no.4
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• pp.718-721
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• 2013

This letter proposes a novel calibration method for a multiport amplifier (MPA) to achieve optimum port-to-port isolation by correcting both the amplitude and phase of the calibration signals. The proposed architecture allows for the detection of the phase error and amplitude error in each RF signal path simultaneously and can enhance the calibrated resolution by controlling the analog phase shifters and attenuators. The designed $2{\times}2$ and $4{\times}4$ MPAs show isolation characteristics of 30 dB and 27 dB over a frequency range of 19.5 GHz to 22.5 GHz, respectively.

• Korean Journal of Remote Sensing
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• v.23 no.1
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• pp.55-58
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• 2007

The prototype radiometric calibration algorithm of the imagers for IR channels has been developed according to the Weinreb's method. Applying the algorithm to the GOES-12 count data, we have shown that the calibration coefficients (slope and intercept) evaluated by the algorithm gives good agreement with the NESDIS's ones, and that the scanning error due to the scan mirror emissivity and stripe error are almost eliminated by the East/West angle dependent scan-mirror correction and the respective calculation of intercept for each North/South scan line, respectively.

• 한국신재생에너지학회:학술대회논문집
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• 2010.06a
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• pp.199.2-199.2
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• 2010

The main purpose of the calibration procedure is to perform a one to one comparison of the reference pyranometer and the test pyranometer. In order to achieve this, both pyranometers need to be exposed to exactly the same irradiance, under the same circumstances. There are a number of error sources that could result in a wrong measurement. Most importantly Lamp instability, pyranometer offsets, thermal offsets of junctions, voltmeter offset, voltmeter instability, reference pyranometer instability, tilting of the pyranometers and differences in sensor height. Another sun-disc calibration procedure compares the computed vertical component of the direct irradiance as measured by a pyranometer with that measured by the pyranometer to be calibrated. Readings are taken with the levelled pyranometer on a clear day. Firstly the global irradiance and then the diffuse component are measured. Simultaneously measurement of direct irradiance is made with the pyrheliometer. The ways of performing the calibration and the subsequent calculation have been chosen such that the effect all these error sources has been eliminated as much as possible.

• Journal of Sensor Science and Technology
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• v.20 no.5
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• pp.329-335
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• 2011

We demonstrated that high-stability thermistors can be calibrated with an uncertainty less than 1 mK, if the error due to the heat conduction is minimized. We first investigated the effect of the self-heating of typical thermistor probes to see how accurate we need to determine the effect of self-heating. We, then, calibrated thermistors and fitted the results using various modeling equations. We found out that the heat conduction is an important factor in achieving the calibration uncertainty under 1 mK for thermistors when the diameter of the probe is as thick as 10 mm. Therefore, we controlled the room temperature within $0.5^{\circ}C$ to minimize the heat conduction error during the calibration. The calibration with an uncertainty below 1 mK was possible when the stabilization time for each calibration was long enough to obtain a good thermal equilibrium.

• Geomechanics and Engineering
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• v.22 no.1
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• pp.97-108
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• 2020

The time-consuming and less objectivity are the main problems of conventional micromechanical parameters calibration method of Particle Flow Code simulations. Thus this study aims to address these two limitation of the conventional "trial-and-error" method. A new calibration method for the linear parallel bond model (CM-LPBM) is proposed. First, numerical simulations are conducted based on the results of the uniaxial compression tests on limestone. The macroscopic response of the numerical model agrees well with the results of the uniaxial compression tests. To reduce the number of the independent micromechanical parameters, numerical simulations are then carried out. Based on the results of the orthogonal experiments and the multi-factor variance analysis, main micromechanical parameters affecting the macro parameters of rocks are proposed. The macro-micro parameter functions are ultimately established using multiple linear regression, and the iteration correction formulas of the micromechanical parameters are obtained. To further verify the validity of the proposed method, a case study is carried out. The error between the macro mechanical response and the numerical results is less than 5%. Hence the calibration method, i.e., the CM-LPBM, is reliable for obtaining the micromechanical parameters quickly and accurately, providing reference for the calibration of micromechanical parameters.

• Journal of Institute of Control, Robotics and Systems
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• v.17 no.12
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• pp.1256-1265
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• 2011

Automated parking assist systems are being commercialized and rapidly spread in the market. In order to improve odometry accuracy, we proposed a practical odometry calibration scheme of Car-Like Mobile Robot (CLMR). However, there were some open problems in our prior work. For example, it was not clear whether the kinematic parameters always converged or not using the proposed calibration scheme. In addition, test driving had to be carried out "twice" without detailed explanation. This research aims to provide answers for the addressed questions though the convergence property analysis of the calibration scheme. In this paper, we evaluate on the effect of the kinematic parameter error on the odometry error at the final pose by numerical computation. The evaluation will show that the wheel diameter and tread of the CLMR can be calibrated by iterative test drives. In addition, the region of convergence in the parametric space will be discussed. Presented experimental results clearly showed that the proposed calibration scheme would be useful in practical applications.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2002.10a
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• pp.355-360
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• 2002

To calibrate a non-redundantly actuated parallel mechanism, one can find actual kinematic parameters by means of geometrical constraint of the mechanism's kinematic structure and measurement values. However, the calibration algorithm for a non-redundant case does not apply fur a redundantly actuated parallel mechanism, because the angle error of the actuating joint varies with position and the geometrical constraint fails to be consistent. Such change of joint angle error comes from constraint torque variation with each kinematic pose (meaning position and orientation). To calibrate a redundant parallel mechanism, one therefore has to consider constraint torque equilibrium and the relationship of constraint torque to torsional deflection, in addition to geometric constraint. In this paper, we develop the calibration algorithm fir a redundantly actuated parallel mechanism using these three relationships, and formulate cost functions for an optimization algorithm. As a case study, we executed the calibration of a 2-DOF parallel mechanism using the developed algorithm. Coordinate values of tool plate were measured using a laser ball bar and the actual kinematic parameters were identified with a new cost function of the optimization algorithm. Experimental results showed that the accuracy of the tool plate improved by 82% after kinematic calibration in a redundant actuation case.

• Journal of The Korean Society of Agricultural Engineers
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• v.47 no.4
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• pp.65-74
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• 2005

AnnAGNPS model was applied to a catchment mainly occupied with bushland for modeling non-point source pollution. Since the single event model cannot handle events longer than 24 hours duration, the event-based calibration was carried out using the continuous mode. As event flows affect sediment and nutrient generation and transport, the calibration of the model was performed in three steps: Hydrologic, Sediment and Nutrient calibrations. The results from hydrologic calibration for the catchment indicate a good prediction of the model with average ARE(Absolute Relative Error) of $24.6\%$ fur the runoff volume and $12\%$ for the peak flow. For the sediment calibration, the average ARE was $198.8\%$ indicating acceptable model performance for the sediment prediction. The predicted TN(Total Nitrogen) and TP(Total Phosphorus) were also found to be acceptable as the average ARE for TN and TP were $175.5\%\;and\;126.5\%$, respectively. The AnnAGNPS model was therefore approved to be appropriate to model non-point source pollution in bushland catchments. In general, the model was likely to result in underestimation for the larger events and overestimation fur the smaller events for the water quality predictions. It was also observed that the large errors in the hydrologic prediction also produced high errors in sediment and nutrient prediction. This was probably due to error propagation in which the error in the hydrologic prediction influenced the generation of error in the water quality prediction. Accurate hydrologic calibration should be hence obtained for a reliable water quality prediction.

• Journal of the Korean Society of Tobacco Science
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• v.17 no.2
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• pp.177-183
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• 1995

This study was conducted to develop the most precise NIR(near infrared spectrometric) calibration for rapid determination of chemical composition in ground samples of toasted burley tobacco using stepwise, stepup, principal component regression(PCR), partial least square(PLS) and modified partial least square(MPLS) calibration method. The number of wavelength(W) selected by stepup multiple linear regression using: second derivative spectra was as follows: total sugar(TS)-4 W, nicotine-9 W, total nitrogen(TN)-2 W, ash-8 W, total volatile base(TVB)-5 W, chlorine4 W, L of color-6 W, a of color-6 W and b of color-7 W. Comparing the calibration equations followed by each chemical components, the most precise calibration equation was MPLS for 75, a and b of color, PLS for nicotine, ash, TVB, chlorine and L of color and stepup for TN. The standard error of calibration(SEC) and standard error of performance(SEP) between result of near infrared analysis and standard laboratory analysis were 0.18, 0.40% for 75, 0.06, 0.08% for nicotine, 0.18, 0.16% for TN, 0.33, 0.46% for ash, 0.04, 0.03% for TVB, 0.08, 0.06% for chlorine, 0.54, 0.58 for L of color, 0.22, 0.22 for a of color and 0.27, 0.27 for b of color, respectively. The SEC and SEP of ash and TVB were within allowable error of standard laboratory analysis, nicotine, TN and chlorine were 1.2-2.0 times and 75 were 2.1-4.0 times larger than allowable error of standard laboratory analysis. The ratio of SEC and SEP to mean were 1.5, 1.6% for L of color, 3.7, 3.8% for a of color and 1.8, 1.8% for b of color, respectively. Key words : burley tobacco chemistry, near infrared spectroscopy.