• 소성∙가공
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• 제18권8호
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• pp.640-645
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• 2009

Recently, boss and rib test based on backward extrusion process was proposed to quantitatively evaluate the interfacial friction condition in bulk forming process. In this test, the tube-shaped punch with hole pressurizes the workpiece so that the boss and rib are formed along the hole and outer surface of the punch. It was experimentally and numerically revealed that the height of boss is higher than that of the rib under the severe friction condition. This work is focused on the effect of the punch design and flow stress on deformation pattern in boss and rib test. From the boss and rib test simulations, it was found that there is slight variation in both the heights of boss and rib according to the length of punch land, nose radius, and face angle. However the hole diameter of the punch and the clearance between the punch and die have a significant influence on the calibration curves showing the heights of the boss and rib. In addition, the effect of flow stress on the calibration curves was investigated through FE simulations. It was found that there is no effect of strength coefficient of the workpiece on the calibration curves for estimation of friction condition. On the other hand, the strain-hardening exponent of the workpiece has a significant influence on the calibration curve.

• 한국재료학회지
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• 제33권3호
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• pp.106-114
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• 2023

The carbon concentration in the carburized steels was measured by electron probe microanalysis (EPMA) for a range of soluted carbon content in austenite from 0.1 to 1.2 wt%. This study demonstrates the problems in carbon quantitative analysis using the existing calibration curve derived from pure iron (0.008 wt%C) and graphite (99.98 wt%C) as standard specimens. In order to derive an improved calibration curve, carbon homogenization treatment was performed to produce a uniform Kα intensity in selected standard samples (AISI 8620, AISI 4140, AISI 1065, AISI 52100 steel). The trend of detection intensity was identified according to the analysis condition, such as accelerating voltage (10, 15, 30 keV), and beam current (20, 50 nA). The appropriate analysis conditions (15 keV, 20 nA) were derived. When the carbon concentration depth profile of the carburized specimen was measured for a short carburizing time using the improved calibration curve, it proved to be a more reliable and accurate analysis method compared to the conventional analysis method.

• 디지털산업정보학회논문지
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• 제8권4호
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• pp.1-11
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• 2012

This paper is the study on the development of a torque precision measuring system using the curve fitting algorithm. This system can be divided into the hardware part and the software part. The hardware part consists of the main base board, the DAQ(Data Aquisition) board and Calibration parts. The software part consists of the software filter module and the curve fitting algorithm module. We have tested the torque transducer including the strain gauge for 200 Nm range and have analyzed the data acquired with the curve fitting algorithm by using this system. The DAQ board converts the electric signal induced by the transducer to the digital value precisely by using the shunt calibration procedure. The main board including the curve fitting algorithm calculates the exact digital torque value by using the digital value from the DAQ board. In this study, we confirmed that the result of the appropriate high-order power-series polynomial function is more accurate than the result of the low-order power-series polynomial through the system.

• 한국자동차공학회논문집
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• 제24권3호
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• pp.365-371
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• 2016

The electromechanical brake (EMB) is one of future brake systems due to its many advantages. For implementation of the EMB, the correct feed back about clamping force is necessary. Keeping commercialization of the EMB in mind, it is strongly demanded that an expensive load cell measuring the clamping force is replaced with an estimation algorithm. In addition, an estimation of the kissing point where the brake pads start to come into contact with a disk wheel is proposed in this paper. With these estimation algorithms, the clamping force can be expressed as a polynomial characteristic curve versus the motor angle. Also, a method for calibration of measured values by the load cell is proposed and used for an actual characteristic curve. Lastly, the performance of the proposed algorithms is evaluated in comparison with the actual curve on a developed EMB test bench.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2000년도 추계학술대회논문집B
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• pp.99-104
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• 2000

Calibration equation for Variable Temperature Anemometer(VTA) has been tested for measured velocity-output data and the calibration process has been compared with that of Constant Temperature Anemometer(CTA). VTA has greater sensitivity than that of any other conventional anemometers, but to be more popular technique in flow field measurement, simple, accurate and well established calibration process should be suggested. To meet this purpose, similar calibration method used for CTA has been adopted for VTA and finally calibration equation for VTA including the effect of temperature drift has been proposed.

• 한국수자원학회:학술대회논문집
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• 한국수자원학회 1995년도 학술발표회 논문집
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• pp.254-259
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• 1995

• Mass Spectrometry Letters
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• 제9권3호
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• pp.77-80
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• 2018

The focus of this paper is to present techniques to overcome certain difficulties in quantitative analysis with a time-of-flight mass spectrometer (TOF-MS). The method is based on conventional solid-phase extraction, followed by reversed-phase ultra high performance liquid chromatography of the extract, and mass spectrometric analysis. The target compounds included atenolol, atrazine, caffeine, carbamazepine, diclofenac, estrone, ibuprofen, naproxen, simazine, sucralose, sulfamethoxazole, and triclosan. The matrix effects caused by high concentrations of organic compounds in wastewater are especially significant in electrospray ionization mass spectroscopy. Internal-standard calibration with isotopically labeled standards corrects the results for many matrix effects, but some peculiarities were observed. The problems encountered in quantitation of carbamazepine and triclosan, due to nonlinear calibration were solved by changing the internal standard and using a narrower mass window. With simazine, the use of a quadratic calibration curve was the best solution.

• 한국군사과학기술학회지
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• 제17권2호
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• pp.204-212
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• 2014

The purpose of this paper is to investigate the effects of calibration rounds on the statistical distribution of the muzzle velocity in acceptance test of propelling charge. It is shown that the normal distribution fits best among statistical distributions from goodness-of fit test. The 3p-Weibull distribution is also acceptable because the shape of the probability density function curve is similar to that of normal distribution and it also has near zero skewness value. Muzzle velocities of test rounds uncompensated by calibration rounds showed high variation and had comparatively higher skewness. Because the skewness of normal distribution is defined to be zero, calibration rounds make the normality of data higher.

• 한국물환경학회지
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• 제37권6호
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• pp.510-519
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• 2021

Volatile Organic Compounds (VOCs) in sediments, which can cause human health problems, have been monitored in Korea since 2014. Measured VOC concentrations can be affected by matrix type and the volatility of target substances. In this study, (1) VOCs volatility and the influence of matrix interference were confirmed, and (2) internal standards (IS) method was applied to improve analytical method. For these purposes, method detection limit (MDL), calibration linearity, precision and accuracy of VOCs were compared in various matrices using the IS. Some of VOCs in sediments showed different peak areas and reduced rates compared to water matrix. It was suggested that adsorption properties of sediments hindered the migration to vapor during heat pretreatment in headspace method. A calibration curve was created in clean sand. Recovery rates for the calibration curve method and IS applying method were 64.1~83.1% and 99.1~119.3%, respectively. Relative standard deviations ranged from 11.1% to 21.6% for the calibration curve method and those for IS ranged 4.7% to 13.7%. In case of real sediment, calibration curve and 1,2-Dichlorobenzene-d4 (ODCB) among IS were not suitable. The average recovery rate of Fluorobenzene (FBZ) increased by 56.4% and Relative Standard Deviation (RSD) by 4.7%. However, the recovery rate was increased in the samples with large values of igniting intensity. This study confirmed that influence of the matrix of VOCs in sediment, and addition of IS materials improved precision and accuracy. Although IS corrects volatilization and adsorption, it is recommended that more than two types of IS should be added rather than single.

• Journal of the Korean Data and Information Science Society
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• 제28권2호
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• pp.349-359
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• 2017

본 논문에서는 미국 국립암연구소의 SEER 프로그램에서 제공하는 우측 대장암 3기 자료에 Cox 비례위험모형을 적합하여 생존분석을 하였다. 우측 대장암 3기 환자의 사망률에 유의한 영향을 미치는 공변량들을 파악하고, 관심있는 공변량들을 가진 환자의 생존율을 추정하였다. Schoenfeld 잔차를 기반한 검정과 Schoenfeld 잔차 도표, $log[-log\{{\hat{S}}(t)\}]$ 도표를 이용하여 분석에 사용된 공변량들이 비례위험 가정을 만족함을 확인하였다. 적합된 Cox 비례위험모형의 타당성을 검증하기 위해 10-fold 교차 검증을 이용하여 calibration 도표와 시간에 의존하는 ROC 곡선 아래 면적을 계산하였다. 이를 통해 적합된 Cox 비례위험모형의 타당성을 확인하였다.