• Water for future
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• v.28 no.6
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• pp.169-181
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• 1995

No correction has been made for the rating curve of Goan Station since 1986 even though there has been a severe bed degradation until now. Furthermore, it was informed to Han River Flood Control Center that there was a difference between the discharge released from Paldang dam and the discharge observed at Goan station during 1990 flood. By considering such river bed changes, hydraulic model experiment with 1/100 scale was performed for the range of 2.2 km, which covers from Paldang dam to the downstream of Goan station. From this experiment, the rating curve was obtained by considering the discharges from Paldang dam and the corresponding water levels at Goan station. Also, the exsitingand the proposed rating curves were compared with those by computational method of RMA-2V.

• Analytical Science and Technology
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• v.12 no.6
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• pp.558-564
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• 1999

A method for measuring archaeological dose of Packjae pottery shards using thermoluminescence dosimetry(TLD) has been studied. TL measurement has been achieved using quartz crystals in the size range of 90 to $125{\mu}m$ diameter extracted from the pottery shards. The stable temperature region of the TL glow curve which is devoid of anomalous fading components was identified by the plateau test and found to exist from 265 to $300^{\circ}C$. The archaeological dose of the pottery shards was estimated to be 7.43 Gy using the dose calibration curves obtained from sequential irradiation of $^{137}Cs$ gamma source to the samples and TL measurement of natural samples.

• Analytical Science and Technology
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• v.7 no.2
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• pp.155-164
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• 1994

A conventional Grimm-type glow discharge source was constructed and applied to radio-frequency(13.56MHz) discharge for metal and ceramic analysis. We investigated the emission spectrum for aluminium and aluminium oxide and the influence of discharge operating paramaters including argon pressure, rf-power and DC-bias voltages at the sample-side electrode. Scanning Electron Microscope(SEM) also was used to investigate the effect of rf-sputtering on the microstructure formation of the aluminium oxide. Linear analytical calibration curves were constructed for Manganese and zinc element in samples of low alloy steel(BAS 401-405) and brass(NIST 1108-1117).

• Korean Journal of Environmental Agriculture
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• v.19 no.5
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• pp.419-425
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• 2000

Rating curve method and SWMM (Storm Water Management Model) were applied to estimate pollutant loading from Hwa-Ong watershed in Kyunggi-Do. Rating curves were derived from sampling sites and applied to the whole watershed. SWMM version 4.4 was calibrated by field data of sampling sites and applied to the whole watershed. The pollutant loading estimated by rating curve was slightly higher than the one by SWMM, but the difference was not significant considering diffuse pollution characteristics of wide variation. Land use effect of the subcatchments could not be incorporated logically in rating curve method and difficulty in extrapolation was experienced, therefore, the estimate by rating curve method was thought to be less confident. SWMM was satisfactory in estimation of pollution loading, and its great flexibility worked well to describe complex nonurban land uses. Neither of them could exactly describe complex natural phenomena, but SWMM was preferred in this study due to its flexibility and logical hydrologic processes including land use effects. Use of reasonable watershed model rather than rating curve method for watershed pollutant loading estimate can be more practical and is recommended.

• Journal of Food Hygiene and Safety
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• v.18 no.2
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• pp.43-50
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• 2003

A liquid chromatographic method, using matrix solid-phase dispersion (MSPD) is developed for the extraction of residual furazolidone in chicken eggs. Blank or fortified egg samples (0.5 g) were blended with Octadecylsilyl (Bulk $C_{18}$, 40${\mu}{\textrm}{m}$, 18%. load, endcapped. 2 g) derivatized silica. After homogenization, $C_{18}$/egg and Na$_2$S $O_4$matrix were transferred to a column made of 10 ml glass syringe and filter paper and compressed 4.0∼4.5 ml volume. The column was washed with 8 ml of hexane and dried under $N_2$ gas. Furazolidone was eluted with acetonitrile (8 ml) under gravity. The eluate containing furazolidone was free from interfering compounds when analyzed by HPLC with UV detection (365 nm, photodiode array). Calibration curves were linear (r = 0.99985) and inter- (1.47%) and intra-assay (5.29%) variabilities for the concentration range examined (7.8∼497 ng/g of eggs, 20 ${mu}ell$ injection volume) were indicative of an acceptable methodology for the analysis of furazolidone. Average recovery of furazolidone added to egg was 96.2%. The limit of detection for the proposed method was 1 ng/g for furazolidone. The method using MSPD is proposed as an alternative assay to the classical method which involves the use of large volumes of a harmful solvent and requires a long tedious separation and clean-up processes prior to its determination.

• Herbal Formula Science
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• v.18 no.1
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• pp.95-103
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• 2010

Objectives : To develop and validate HPLC-PDA methods for simultaneous determination of seven constituents in Samsoeum(SSE). Methods : Reverse-phase chromatography using a Gemini C18 column operating at $40^{\circ}C$, and photodiode array(PDA) detection at 254 and 280 nm, were used for quantification of the seven marker components of SSE. The mobile phase using a gradient flow consisted of two solvent systems. Solvent A was 1.0% (v/v) aqueous acetic acid and solvent B was acetonitrile with 1.0% (v/v) acetic acid. Results : Calibration curves were acquired with $r^2$>0.9997, and the relative standard deviation (RSD) values (%) for intra- and inter-day precision were less than 3.0%. The recovery rate of each compound was in the range of 100.07-112.65%, with an RSD less than 4.0%. The contents of seven compounds in SSE were 1.24-10.53 mg/g. Conclusions : The established method will be helpful to improve quality control of SSE.

• Analytical Science and Technology
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• v.7 no.3
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• pp.349-359
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• 1994

A gas chromatographic method for analyzing the gas odorants concentration in natural gas was studied. Eight odorants involving TBM and THT were completely separated by using OV-10 column. The optimization of several interrelated key parameters affecting the response of FPD such as hydrogen flow rate, air flow rate and detector temperature were accomplished. A permeation device was used to obtain calibration curves of TBM and THT. This analytical method has applied to measure TBM and THT used as a natural gas odorant blend in natural gas pipeline. In order to elucidate the relationship between odor level and odorant level feasibility test of fragrance meter was demonstrated.

• Analytical Science and Technology
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• v.27 no.4
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• pp.196-200
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• 2014

Currently nonaqueous titration method for the assay method using the hazardous reagent, mercury acetate for difemerine hydrochloride has been used in Korean Pharmaceutical Codex. We developed an alternative titration assay method by substituting the use of the hazardous reagent, mercury acetate to the use of less toxic ones like ethyl alcohol. The linearity of the calibration curves in the desired concentration range was good (r>0.999). Precision was less than 0.64%. Accuracy was obtained with recoveries in range of 99.10% and 99.71%. The developed assay could be expected to become valuable tools for revising the Korean Pharmaceutical Codex.

• The Journal of the Korea Contents Association
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• v.13 no.8
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• pp.11-19
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• 2013

This paper presents a simple method to estimate center of distortion and correct radial distortion from fish-eye lens. If the center of image is not locate that of lens in a straight line, the disadvantage of FOV model is low accurate because of correcting distortion without estimated centre of distortion. We propose a method accurately estimating Distortion center using FOV model and 2D pattern from wide angle lens. Our method determines the center of distortion in least error between straight lines and curves with FOV model. The results of experimental measurements on synthetic and real data are presented.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.7 no.4
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• pp.697-703
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• 2006

In this research, model tests for in-situ Top-Base Foundation are carried out in other to investigate the load delivering mechanism and the incremental effect of bearing capacity. According to the result of model tests, the load-settlement curves of both in-situ Top-Base(In-situ TBF) and Precast Top-Base Foundation(PC-TBF) showed similar results in term of the ground movement and effect of bearing capacity. Also, the range of vertical stresses delivered into ground was decreased with Top-Base method regarding other types foundations.