• Title/Summary/Keyword: CCS calibration

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Automatic and precise calibration of 4-channel cylindrical capacitive displacement sensor (4채널 원통형 정전용량 변위센서의 자동ㆍ정밀 검보정)

  • 김종혁;김일해;박만진;장동영;한동철;백영종
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2004.04a
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    • pp.387-393
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    • 2004
  • General purpose of cylindrical capacitive displacement sensor(CCS) is measuring run-out motion and deflection of rotor. If CCS has narrow sensing range, its sensitivity coefficients must be calibrated precisely. And x, y component of CCS output can be coupled. In this research, CCS calibration procedure is automated with automatic calibration program and PC-controlled stage. And, coupled-terms of CCS signals were removed and the errors between measured position and mapped CCS signal were reduced obviously by sensitivity matrix that linearly.

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A Study of Calibration Bias in the Analysis of Airborne Carbonyl Compounds between Gaseous and Liquid-phase Standards by High Performance Liquid Chromatography (HPLC) (대기 중 Carbonyl 성분들의 검량 분석 기술에 대한 연구: 액상 대비 기체상 표준시료의 오차발생 특성 연구)

  • Lee, Min-Hee;Kim, Ki-Hyun
    • Journal of Korean Society for Atmospheric Environment
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    • v.28 no.1
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    • pp.52-58
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    • 2012
  • In this study, the effect of standard phase difference in calibration of carbonyl compounds (CC) was evaluated by using their standards prepared in both gaseous and liquid phase. For this analysis, standards in both phases were prepared for 6 different CCs (formaldehyde (FA), acetaldehyde (AA), propionaldehyde (PA), butyraldehyde (BA), isovaleraldehyde (IA) and valeraldehyde (VA)) at similar concentration levels. Their gaseous standard was calibrated after derivatization with three types of DNPH cartridge, and their calibration results were compared against liquid-phase standards. Although there was a strong compatibility between 2 phases for CCs with lower molecular weights (e.g., formaldehyde and acetaldehyde), it was not the case for the heavier CCs. The results of our analysis indicate that the analytical bias of the heavier CCs can be significantly large (by more than a few tens of %). As a result, underestimation of hevier CCs can be significant, if their gaseous samples are quantified by liquid phase standard.

Semiquantitative Analysis of metal for Cigarette Product by Inductively Coupled Plasma Mass Spectrometry (유도결합 플라스마 질량분석기를 이용한 담배 제품의 무기물 반정량 분석)

  • Cho, Sung-Eel;Kim, Hyo-Keun;Hwang, Keon-Joong
    • Journal of the Korean Society of Tobacco Science
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    • v.31 no.2
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    • pp.95-106
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    • 2009
  • Semiquantitative analysis by ICP-MS has proven to be a powerful tool for fast screening, in addition, it does not require the element of interest to be present in the calibration standard, making it especially useful for the analysis of unknown samples. In this study, seven cigarette samples were analyzed by the rapid semi-quantitative analysis method based on the ICP-MS. For each cigarette sample, cut tobacco, cigarette paper, filter (before and after smoking), and smoke condensate were analyzed. The accuracy of the analysis technique was evaluated by comparing results obtained from Calibration Check Standard(CCS) and calibration method. Relative Percentage Error(RPE) value of all elements measured for three CCS showed a stable result of less than ${\pm}20%$. Compared to full quantitative analysis by calibration method, the results for cigarette samples showed average error within ${\pm}15%$.

The effect of relative humidity on the performance of DNPH-cartridge sampling for odorous aldehydes (악취성 Carbonyl 화합물의 카트리지 채취 분석: 습도가 채취효율에 미치는 영향)

  • Lee, Min-Hee;Kim, Ki-Hyun
    • Analytical Science and Technology
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    • v.25 no.1
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    • pp.50-59
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    • 2012
  • In this study, the effect of humidity change on DNPH cartridge sampling efficiency for carbonyl compounds (CCs) has been investigated. For this analysis, gaseous standard of 6 different CCs (formaldehyde (FA), acetaldehyde (AA), propionaldehyde (PA), butyraldehyde (BA), isovaleraldehyde (IA), and valeraldehyde (VA)) was calibrated after derivatization with three types of DNPH cartridge products. Their calibration results derived at RH values between 0 and 80% were then compared against liquid phase standards. If the results of our analysis are compared by the RH values between 20 and 80%, the effect of RH can be distinguished between light and heavy CCs. For lighter CCs (like FA and AA), there was no significant change. However, for the ones heavier than PA, there was fairly noticeable increase in relative recovery ratio in RH value between 20 and 80%. Such patterns are seen consistently from all three DNPH products tested for comparison. The results of our analysis suggest that proper correction for RH change may be needed for heavier CCs by the cartridge method.

Development of an insulation performance measurement unit for full-scale LNG cargo containment system using heat flow meter method

  • Lee, Jin-sung;Kim, Kyung-su;Kim, Yooil
    • International Journal of Naval Architecture and Ocean Engineering
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    • v.10 no.4
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    • pp.458-467
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    • 2018
  • Efforts have been made in this paper to develop the measuring device for the insulation performance of full scale NO96 LNG CCS. The facility was designed to maintain environmental conditions which are similar to operation conditions of full scale LNG CCS. In the facility, the heat sink boundary was kept cryogenic temperature by cold chamber which contains liquefied nitrogen and heat source boundary was made by external case heated by natural convection. Heat Flow Meter method (HFM) was applied to this facility, hence Heat Flux Sensors (HFS) were attached to specimen. The equivalent thermal conductivity of full scale NO96 unit box was targeted to measure and PUF of same size was used for the calibration test. Additionally, the finite element analysis was carried out to check the performance of the developed test facility and experimental results were also compared with those predicted by the numerical method.

Selecting Significant Wavelengths to Predict Chlorophyll Content of Grafted Cucumber Seedlings Using Hyperspectral Images

  • Jang, Sung Hyuk;Hwang, Yong Kee;Lee, Ho Jun;Lee, Jae Su;Kim, Yong Hyeon
    • Korean Journal of Remote Sensing
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    • v.34 no.4
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    • pp.681-692
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    • 2018
  • This study was performed to select the significant wavelengths for predicting the chlorophyll content of grafted cucumber seedlings using hyperspectral images. The visible and near-infrared (VNIR) images and the short-wave infrared images of cucumber cotyledon samples were measured by two hyperspectral cameras. A correlation coefficient spectrum (CCS), a stepwise multiple linear regression (SMLR), and partial least squares (PLS) regression were used to determine significant wavelengths. Some wavelengths at 501, 505, 510, 543, 548, 619, 718, 723, and 727 nm were selected by CCS, SMLR, and PLS as significant wavelengths for estimating chlorophyll content. The results from the calibration models built by SMLR and PLS showed fair relationship between measured and predicted chlorophyll concentration. It was concluded that the hyperspectral imaging technique in the VNIR region is suggested effective for estimating the chlorophyll content of grafted cucumber leaves, non-destructively.