• Title/Summary/Keyword: C-S-H phase

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Physical Properties of Microencapsulated Phase Change Material Slurries (미립잠열슬러리의 물성에 관한 실험적 연구)

  • 이효진;홍재창;이재구
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.12 no.9
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    • pp.860-869
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    • 2000
  • The thermal conductivity and density of slurries entrained with the particles of Micro-PCM are measured with respect to its temperatures as well as concentrations. For the thermal conductivity of slurries, a device made from P.A. Hilton (Model No. H470) is adopted. There is a well-scaled 0.3 mm gap between shells into which the slurry is injected. The temperatures of the slurry are changed to $5~25^{\circ}C$ , for which it is controled by the supplied voltage and cooling water circulated around the outer shell. The concentrations of Micro-PCM slurries are varied from 5 wt% to 50 wt%. Some general equations such as Maxwell's equation, are evaluated for their applicability with Micro-PCM slurry. As a result, it happens to be some 20% discrepancy between the experiment and the applied equations. The density measurements of Micro-PCM slurry to its temperature and concentration are peformed by hydrometer. For the experiment, tetradecane encapsulated slurry (($t_m≒6^{\circ}C$) and a mixed wax ($t_m≒50^{\circ}C$) are tested. The temperature changes of tetradecane are applied for $0^{\circ}C\;to\;$20^{\circ}C$and a mixed wax for $20^{\circ}C\;to\;$60^{\circ}C$ and its concentrations are changed from 5 wt% to 30 wt%. The results are compared with a general equation and the referenced data. For the conclusion, the experimental result and a general equation are well agreed.

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Simultaneous Determination of Tetracycline Antibiotics by 3-Phase Hollow Fiber-Liquid Phase Microextraction (HF-LPME) and HPLC-UV/Vis (3-상 속빈 섬유-액체상 미량추출법(HF-LPME)과 HPLC-UV/Vis을 이용한 Tetracycline류 항생제 동시분석)

  • Oh, Woong Kyo;Myung, Seung-Woon
    • Journal of the Korean Chemical Society
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    • v.58 no.6
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    • pp.535-542
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    • 2014
  • A simple and efficient preconcentration method was developed using three-phase liquid phase microextraction prior to HPLC-UV for simultaneous extraction and determination of tetracycline antibiotics (tetracycline, oxytetracycline, and chlortetracycline). The tetracycline antibiotics were separated simultaneously on a column ($C_8$, $3.0{\times}150mm$, $3{\mu}m$) with high selectivity and sensitivity using gradient elution. Under optimized conditions (extraction solvent, heptanal; pH of donor, 9.0; pH of acceptor, 1.0; stirring speed, 700 rpm; NaCl salt, 0%; and extraction time, 60 min), enrichment factors (EF) were between 5.6 and 22.3. The limit of detection (LOD) and limit of quantitation (LOQ) in the spiked urine matrix were in the concentration range of $0.08{\sim}0.8{\mu}g/mL$ and $0.4{\sim}1.6{\mu}g/mL$, respectively. The calibration curves were linear within the range of $0.1{\sim}32{\mu}g/mL$ with the square of the correlation coefficient being more than 0.995. The precision (as a relative standard deviation, RSD) and accuracy (as a relative recovery) within working range were 1.3~9.1% and 84~118%, respectively.

A Study on Crystal Structure Growth of YbBCO Superconductor (YbBCO초전도체의 결정성장에 관한 연구)

  • 박정철;이영매;소대화
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1998.06a
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    • pp.367-370
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    • 1998
  • In this paper, based on the research of high temperature YBCO superconductor, using the Yb instead of Y, with the YbBCO superconductor powder which was combined by means of conventional solid reaction, textured directional crystal was prepared by MCP method and the character was analyzed. Mixing the starting elements and calcining at 890$^{\circ}C$, 900$^{\circ}C$, 910$^{\circ}C$, single phase YbBCO, Yb$_2$BaCuO$\sub$5/ and BaCuO$\sub$2/ were certified. And from the powder which was calcined at 900$^{\circ}C$ the, sample which became texture-growth by MCP method was well oriented. The result of DTA measurement, the fusing point of YbBCO superconductor and it\`s critical current was measured to be 979$^{\circ}C$, 87K respectively. The critical current density was obtained at the value of 700A/$\textrm{cm}^2$(77K. 0H) calculated by Bean's Model using the measured hysteresis curve of VSM.

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A study on Dielectric and Electrical Properties Using PMN-PT-BT Ceramics (PMN-PT-BT계 세라믹스의 유전 및 전기적 특성)

  • Ji, S.H.;Lee, N.H.;Kim, Y.H.;Kim, J.S.;Cho, S.W.;Lee, D.C.
    • Proceedings of the KIEE Conference
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    • 1994.07b
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    • pp.1481-1483
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    • 1994
  • The dielectric and electrical properties of $Pb(Mg_{1/3}Nb_{2/3})O_3-PbTiO_3-BaTiO_3$ have been investigated. Perovskite crystalline phase of the specimens is confimed by XRD. The curie temperature decrease with increasing $BaTiO_3$ and hysteresis phenomena decrease with increasement of $BaTiO_3$. The strain vs. applied voltage characteristics exhibit nonlinear relationship and the specimen. of 0.9PMN-0.08PT-0.02BT shows the largest strain.

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Alternating Magnetic Field Crystallization of Amorphous Si Films

  • Kang, K.H.;Park, S.H.;Lee, S.J.;Nam, S.E.;Kim, H.J.
    • Journal of Information Display
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    • v.4 no.1
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    • pp.34-37
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    • 2003
  • We investigate the solid phase crystallization of amorphous Si films on glass substrates under alternating magnetic field induction. The kinetics of crystallization are found to be greatly enhanced by alternating magnetic field. While complete crystallization takes heat treatment of more than 14 hours at 570$^{\circ}C$, it can be reduced by applying the megnetic field to 20 minutes. It is assumed that the enhancement of crystallization is associated with an electromotive force voltage generated by alternating magnetic field. This electric field applied in the amorphous Si may possibly be the reason for acceleration of the atomic mobility of crystallization through the modification of atomic potentials

Interleaved Phase Shifted Full Bridge Converter using Six Switches (스위치 저감형 풀브리지 컨버터의 구조 및 병렬 운전 기법에 관한 연구)

  • Yi, J.H.;Lee, S.W.;Kim, D.H.;Cho, B.H.;Kim, W.S.;Lee, Jae-Ho;Yang, C.S.
    • Proceedings of the KIPE Conference
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    • 2012.07a
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    • pp.199-200
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    • 2012
  • 본 논문에서는 저전압 대전류 출력 구조에 적합한 병렬 운전형 풀브리지 컨버터의 구조 및 운전기법에 대하여 제안하였다. 제안된 회로에서는 6개의 스위치 및 위상각을 이용하여 풀브리지 컨버터 두 모듈의 병렬 운전이 가능하다. 2kW급 하드웨어를 통하여 제안된 회로의 기본 동작원리 및 실험결과를 기술하였다.

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Cultural Conditions of Lactobacillus sp. GM7311 for the Production of Bacteriocin (Lactobacillus sp. GM7311에 의한 박테리오신의 생산 조건)

  • LEE Myung Suk;CHANG Dong Suck;KANG Ji-Hee
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.30 no.5
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    • pp.834-841
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    • 1997
  • A lactic acid bacteria which showed antimicrobial activity was isolated from dairy products and identified as Lactobacillus sp. according to the morphological, physiological and biochemical properties, which was named Lactobacillus sp. SH 7311. The bacteriocin of Lactobacillus sp. GM 7311 showed a broad range of inhibitory spectrum against some gram positive and negative bacteria. Especially, Proteus mirabilis was highly sensitive to bacteriocin and used as indicator strain for further investigation. The optimal condition for the production of bacteriocin was showed on MRS broth at $37^{\circ}C$ and pM 6.0. Bacteriocin production of this strain cultured under optimal condition was increased late logarithmic phase to early stationary phase. This bacteriocin was fully active at the pH range $2.0\~5.0$, also was stable at $100^{\circ}C$ for 60 min. at pH 5.0, But about $40\%$ of bacteriocin activity was diminished by the treatment of acetone, ethanol, iso-butanol and ethyl ether during 2 hours at $4^{\circ}C$.

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Characteristics of ZnO thin films by RF magnetron sputtering for FBAR application (RF 마그네트론 스퍼터링을 이용한 FBAR 소자용 ZnO 박막의 특성)

  • Kim, S.Y.;Lee, N.H.;Kim, S.G.;Park, S.H.;Jung, M.G.;Shin, Y.H.;Ji, S.H.;Lee, D.C.
    • Proceedings of the KIEE Conference
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    • 2003.07c
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    • pp.1523-1525
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    • 2003
  • Due to the rapid development of wireless networking system, researches on the communication devices are mainly focus on microwave frequency devices such as filters, resonators, and phase shifters. Among them, Film bulk acoustic resonator (FBAR) has been paid extensive attentions for their high performance. In this research, ZnO thin films were deposited by RF-magnetron sputtering on Al/$SiO_2$/Si wafer and then crystalline properties and surface morphology were examined. To measure crystalline structure and surface morphology X-ray diffraction (XRD) and Scanning Electron Microscope (SEM) were employed. It was showed that crystalline properties of ZnO thin films were strongly dependant on the deposition conditions. As increasing the deposition temperature and the deposition pressures, the peak intensities of ZnO(002) plane were increased until $300^{\circ}C$, then decreased rapidly. At the sputtering conditions of RF power of 213 W and working pressure of 15 m Torr, ZnO film had excellent c-axis orientation, surface morphology, and adhesion to the substrate. In conclusion we optimized smooth surface with very small grains as well as highly c-axis oriented ZnO film for FBAR applications.

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Formation of D-Glucose Isomerase by Streptomyces sp. (Streptomyces sp.에 의한 포도당 이성화효소의 생성)

  • Rhee, In-Koo;Seu, Jung-Hwn
    • Microbiology and Biotechnology Letters
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    • v.8 no.3
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    • pp.173-180
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    • 1980
  • A source of D-xylose was required for the enhanced production of D-glucose isomerase of Streptomyces sp. strain K-17. D-glucose supported the luxuriant growth of the organism as well as D-xylose, but D-glucose isomerase activity was hardly detected in the D-glucose-grown cells. When the D-glucose-grown cells were incubated aerobically for a few hours in 0.5% xylose solution in 0.05 M phosphate buffer, pH 7.0, it was found that inductive formation of D-glucose isomerase occurred in the cells without multiplication. In the non-growth phase of cells the inductive formation of D-glucose isomerase occurred because a source of nitrogen for the synthesis of enzymes was obtained from turnover of protein accumulated in cells. D-ribose, L-arabinose, D-glucose, D-mannose, citrate, succinate and tartrate could not induce the formation of D-glucose isomerase, but D-xylose could induce. Inductinn of D-glucose isomerase was repressed by D-glucose and its catabolites : glycerol, succinate and citrate. Inductive formation of the enzymes in the non-growth phase was stimulated by $Ba^{2+}$, $Mg^{2+}$ and $Co^{2+}$, and inhibited by C $u^{2+}$, C $d^{2+}$, A $g^{+}$and H $g^{2+}$. The synthesis of enzymes in the induction system composed of 0.5% xylose solution was disrupted by actinomycin D, streptomycin, chloramphenicol, kanamycin, tetracycline, p-chloromercuribenzo ate, arsenate and 2, 4-dinitrophenol, but not disrupted by mitomycin C and penicillin G.icillin G.

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The Effect of Hot Stamping Operation Condition on the Mechanical Properties (핫스탬핑 공정조건에 따른 기계적 특성)

  • Kim, H.D.;Moon, M.B.;Lee, S.H.;Yoon, K.W.;Yoo, J.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.10a
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    • pp.317-320
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    • 2008
  • The Hot Stamping process, which is the hot pressing of steel parts using cold dies. can utilize both case of shaping and high strength due to the hardening effect of rapid quenching during the pressing. We carried out experiments of quenching rate and tempering treatments at temperatures of $200^{\circ}C$ and $300^{\circ}C$ and different soaking times. Tn this study, the mechanical properties and microstructure of micro boron alloyed steels after heat treatments are compared.

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