• Title/Summary/Keyword: Bulk samples

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Occupational Exposure to Refractory Ceramic Fibers in the Semiconductor Scrubber Manufacturing Industry

  • Song, Seungwhan;Kim, Sunju;Kim, Donghyeon;Yoon, Chungsik
    • Safety and Health at Work
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    • v.13 no.3
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    • pp.357-363
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    • 2022
  • Background: Refractory ceramic fibers (RCFs) are a suspected carcinogen but have been widely used as insulations. Depending on the temperature, RCFs can transform into crystalline SiO2, which is a carcinogen that can be present in the air during bulk RCF handling. This study analyzed the physicochemical and morphological characteristics of RCFs at high temperatures and determined the exposure levels during the semiconductor scrubber maintenance. Methods: Sampling was conducted at a company that manufactures semiconductor scrubbers using RCFs as insulation. Bulk RCF samples were collected both before and after exposure to a scrubber temperature of 700℃. Airborne RCFs were collected during scrubber maintenance, and their characteristics were analyzed using microscopes. Results: The components of bulk RCFs were SiO2 and Al2O3, having an amorphous structure. Airborne RCFs were morphologically different from bulk RCFs in size, which could negatively affect maintenance workers' health. 58% of airborne RCFs correspond to the size of thoracic and respirable fibers. RCFs did not crystallize at high temperatures. The exposure caused by airborne RCFs during the scrubber frame assembly and insulation replacement was higher than the occupational exposure limit. Conclusion: Workers conducting insulation replacement are likely exposed to airborne RCFs above safe exposure limits. As RCFs are suspected carcinogens, this exposure should be minimized through prevention and precautionary procedures.

Errors in light-emitting diodes positioning when curing bulk fill and incremental composites: impact on properties after aging

  • Abdulrahman A. Balhaddad;Isadora M. Garcia;Haifa Maktabi;Maria Salem Ibrahim;Qoot Alkhubaizi;Howard Strassler;Fabricio M. Collares;Mary Anne S. Melo
    • Restorative Dentistry and Endodontics
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    • v.46 no.4
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    • pp.51.1-51.13
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    • 2021
  • Objectives: This study aimed to evaluate the effect of improper positioning single-peak and multi-peak lights on color change, microhardness of bottom and top, and surface topography of bulk fill and incremental composites after artificial aging for 1 year. Materials and Methods: Bulk fill and incremental composites were cured using multi-peak and single-peak light-emitting diode (LED) following 4 clinical conditions: (1) optimal condition (no angulation or tip displacement), (2) tip-displacement (2 mm), (3) slight tip angulation (α = 20°) and (4) moderate tip angulation (α = 35°). After 1-year of water aging, the specimens were analyzed for color changes (ΔE), Vickers hardness, surface topography (Ra, Rt, and Rv), and scanning electron microscopy. Results: For samples cured by single-peak LED, the improper positioning significantly increases the color change compared to the optimal position regardless of the type of composite (p < 0.001). For multi-peak LED, the type of resin composite and the curing condition displayed a significant effect on ΔE (p < 0.001). For both LEDs, the Vickers hardness and bottom/top ratio of Vickers hardness were affected by the type of composite and the curing condition (p < 0.01). Conclusions: The bulk fill composite presented greater resistance to wear, higher color stability, and better microhardness than the incremental composite when subjected to improper curing. The multi-peak LED improves curing under improper conditions compared to single-peak LED. Prevention of errors when curing composites requires the attention of all personnel involved in the patient's care once the clinical relevance of the appropriate polymerization reflects on reliable long-term outcomes.

A Study on Penetration of Pea Seedling Taproots as Influenced by strength of Soil (토양(土壤)의 경도(硬度)가 완두뿌리의 신장(伸長)에 미치는 영향(影響))

  • Jo, In-Sang;Cho, Seong-Jin;Im, Jeong-Nam
    • Korean Journal of Soil Science and Fertilizer
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    • v.10 no.1
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    • pp.7-12
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    • 1977
  • This experiment was conducted in the laboratory in order to find out the relationships between the root growth and soil physical properties. The soils selected for this study were Sangju sandy loam, Yeongog loam, Hwadong silty clay loam, which have been considered to be a typical upland soils of Korea. Artificial core samples were made with various moisture contents and bulk densities. Elongation rate of pea seedling taproot and soil strength were measured respectively in these core samples. The results obtained are summarized as follows: 1. The soil strength increased with the bulk density and deceased with moisture content. 2. The correlation between root elongation and soil bulk density was significantly recognized at the same moisture content and the root elongation was influenced by the bulk density more significantly at dry condition. 3. The elongation rate of pea seedling taproot was significantly decreased by increasing the strength (Yamanaka tester and Fine probe) of the soils. 4. The soil strength of $21kg/cm^2$ in fine metal probe or 24mm in Yamanaka tester was considered to be the critical point for plant growth, which was restricting root elongation smaller than 1/4 of the maximum growth rate.

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High Strength Nanostructured Metastable Alloys

  • Eckert, Jurgen;Bartusch, Birgit;Schurack, Frank;He, Guo;Schultz, Ludwig
    • Journal of Powder Materials
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    • v.9 no.6
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    • pp.394-408
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    • 2002
  • Nanostructured high strength metastable Al-, Mg- and Ti-based alloys containing different amorphous, quasicrystalline and nanocrystalline phases are synthesized by non-equilibrium processing techniques. Such alloys can be prepared by quenching from the melt or by powder metallurgy techniques. This paper focuses on one hand on mechanically alloyed and ball milled powders containing different volume fractions of amorphous or nano-(quasi)crystalline phases, consolidated bulk specimens and, on the other hand. on cast specimens containing different constituent phases with different length-scale. As one example. $Mg_{55}Y_{15}Cu_{30}$- based metallic glass matrix composites are produced by mechanical alloying of elemental powder mixtures containing up to 30 vol.% $Y_2O_3$ particles. The comparison with the particle-free metallic glass reveals that the nanosized second phase oxide particles do not significantly affect the glass-forming ability upon mechanical alloying despite some limited particle dissolution. A supercooled liquid region with an extension of about 50 K can be maintained in the presence of the oxides. The distinct viscosity decrease in the supercooled liquid regime allows to consolidate the powders into bulk samples by uniaxial hot pressing. The $Y_2O_3$ additions increase the mechanical strength of the composites compared to the $Mg_{55}Y_{15}Cu_{30}$ metallic glass. The second example deals with Al-Mn-Ce and Al-Cu-Fe composites with quasicrystalline particles as reinforcements, which are prepared by quenching from the melt and by powder metallurgy. $Al_{98-x}Mn_xCe_2$ (x =5,6,7) melt-spun ribbons containing a major quasicrystalline phase coexisting with an Al-matrix on a nanometer scale are pulverized by ball milling. The powders are consolidated by hot extrusion. Grain growth during consolidation causes the formation of a micrometer-scale microstructure. Mechanical alloying of $Al_{63}Cu_{25}Fe_{12}$ leads to single-phase quasicrystalline powders. which are blended with different volume fractions of pure Al-powder and hot extruded forming $Al_{100-x}$$(Al_{0.63}Cu_{0.25}Fe_{0.12})_x$ (x = 40,50,60,80) micrometer-scale composites. Compression test data reveal a high yield strength of ${\sigma}_y{\geq}$700 MPa and a ductility of ${\varepsilon}_{pl}{\geq}$5% for than the Al-Mn-Ce bulk samples. The strength level of the Al-Cu-Fe alloys is ${\sigma}_y{\leq}$550 MPa significantly lower. By the addition of different amounts of aluminum, the mechanical properties can be tuned to a wide range. Finally, a bulk metallic glass-forming Ti-Cu-Ni-Sn alloy with in situ formed composite microstructure prepared by both centrifugal and injection casting presents more than 6% plastic strain under compressive stress at room temperature. The in situ formed composite contains dendritic hcp Ti solid solution precipitates and a few $Ti_3Sn,\;{\beta}$-(Cu, Sn) grains dispersed in a glassy matrix. The composite micro- structure can avoid the development of the highly localized shear bands typical for the room temperature defor-mation of monolithic glasses. Instead, widely developed shear bands with evident protuberance are observed. resulting in significant yielding and homogeneous plastic deformation over the entire sample.

Relationship of Soil Particle Size and Organic Matter Content to the Bulk Density in Paddy Soil (답토양(畓土壤)의 입경분포(粒徑分布) 및 유기물함량(有機物含量)과 용적밀도(容積密度)와의 관계(關係))

  • Hur, Bong-Koo;Kim, Zhoo-Hyeon;Kim, Young-Sang;Park, Yong-Sun
    • Korean Journal of Soil Science and Fertilizer
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    • v.26 no.3
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    • pp.155-159
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    • 1993
  • This study was initiated to obtain the scientific information for the improvement of paddy soil. Mean values and mutual relationships of bulk density, pH values and the content of organic matter were investigated at the 124 field sites shown to be nationwide high-yielding, young seedling field s and their neighboring fields under the different soil textures and depths. The soil samples were collected and those samples were analyzed in the laboratory of Agricultural Sciences Institute. Mean values among the different soil textures and depths were estimated with loam-textured. Bulk density were significantly correlated with sand and silt in topsoil, and that were appeared to be correlated to sand, silt + clay, pH and content of organic matter highly significant in 1% level. Regression equation of soil bulk density(Y) to clay(C), orgnic matter (OM) and content of silt + clay(S+C) were as follows for the topsoil, Y=1.365+0.006C-0.003(S+C)~0.034OM (R=0.067*), and for the subsoil, Y=1.548 -0.002C-0.0007 (S+C) -0.036OM (R=0.122**).

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A Study on the Measurement of Physical Properties for Miscellaneous Cereal Crops Sorting (잡곡 선별을 위한 물성 측정에 관한 연구)

  • Kim, Hoon;Lee, Hyo-Jai;Han, Jae Woong
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.10
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    • pp.354-360
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    • 2020
  • This study examined the factors for sorting miscellaneous cereal crops using a rice-sorting device by analyzing the physical characteristics according to the moisture content. The initial moisture contents of miscellaneous cereal were 16.3, 19.8, and 16.5%, respectively. The samples were used in the experiment after drying to five levels. The width, length, and area of the samples increased with increasing moisture content except for the roundness, and all the prediction models were developed with a first-order linear equation. The bulk density of Italian millet and sorghum increased with increasing moisture content, whereas the bulk density of common millet was unaffected by the change in moisture content. The terminal velocity of the samples increased with increasing moisture content, and a first-order linear equation was used to develop the prediction models. The measured physical properties of the miscellaneous cereal crops based on the changes in the moisture content could be expressed using a first-order experimental model equation. Therefore, the rice-sorting device could be applied to the terminal velocity, but the other device applying the geometrical characteristics and bulk density was required to change the design of the process depending on the type of grain.

A $2{\times}2$ Microstrip Patch Antenna Array for Moisture Content Measurement of Paddy Rice (산물벼 함수율 측정을 위한 $2{\times}2$ 마이크로스트립 패치 안테나 개발)

  • 김기복;김종헌;노상하
    • Journal of Biosystems Engineering
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    • v.25 no.2
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    • pp.97-106
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    • 2000
  • To develop the grain moisture meter using microwave free space transmission technique, a 10.5GHz microwave signal with the power of 11mW generated by an oscillar with a dielectric resonator is transmitted to an isolator and radiated from a transmitting $2{\times}2$ microstrip patch array antenna into the sample holder filled with the 12 to 26%w.b. of Korean Hwawung paddy rice. the microwave signal, attenuated through the grain with moisture, is collected by a receiving $2{\times}2$ microstrip patch array antenna and detected using a Shottky diode with excellent high frequency characteristic. A pair of light and simple microstrip patch array antenna for measurement of grain moisture content is designed and implemented on atenflon substrate with trleative dielectric constant of 2.6 and thickness of 0.54 by using Ensemble ver. 4.02 software. The aperture of microstrip patch arrays is 41 mm width and 24mm high. The characteristics of microstrip patch antenna such as grain. return loss, and bandwidth are 11.35dBi, -38dB and 0.35GHz($50^{\circ}$ at far-field pattern of E and H plane. The width of the sample holder is large enough to cover the signal between the antennas temperature and bulk density respectively. The calibration model for measurement of grain moisture content is proposed to reduce the effects of fluectuations in bulk density and temperature which give serious errors for the measurements . From the results of regression analysis using the statistically analysis method, the moisture content of grain samples (MC(%)) is expressed in terms of the output voltage(v), temperature (t), and bulk density of samples(${\rho}b$)as follows ;$$MC(%)\;=\;(-3.9838{\times}10^{-8}{\times}v^{3}+8.023{\times}10^{-6}{\times}v^{2}-0.0011{\times}v-0.0004{\times}t+0.1706){\frac{1}{{\rho}b}}{\times}100$ Its determination coefficient, standard error of prediction(SEP) and bias were found to be 0.9855, 0.479%w.b. and -0.0.369 %w.b. respectively between measured and predicted moisture contents of the grain samples.

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A Study on the Chemical Characteristics of Acid Rain in Taejon City (대전지역 산성강우의 화학적 특성에 관한 연구)

  • 구자공;박경렬
    • Journal of Korean Society for Atmospheric Environment
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    • v.9 no.2
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    • pp.147-153
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    • 1993
  • From March 1990 to August 1991, every each 5mm bulk precipitation samples were collected at one residental area in Taejon City to investigate chemical characteristics of acid rain. Major ion concentrations of rain samples $(pH, SO_4^{2-}, NO_3^-, CL^-, NH_4^+, Na^+, K^+, Ca^{2+}, Mg^{2+})$ were analysed and compared with the concentration of air pollutants (T. S. P, $SO_2, NO_x$) that were measured by Ministry of Environment. The results of statistical analysis are as followings. Rain pH was relatively high on October and January and relatively low on August, November and February. Major anion is sulfate, and it's concentration is 2.36 times higher than nitrate's, and major cations are ammonium, sodium and calcium ion. Monthly variation of sulfate and calcium concentrations are higher than the others. Ion concentration and rain pH were correlated negatively with rainfall amount. Major ions in rain samples were $SO_4^{2-}, NO_3^-, NH_4^+, Ca^{2+}$ and regression equations are proposed by multiple regression of measured data. Also, regression equation between air pollutants(T. S. P, $SO_2$) and $SO_4^{2-}, Na^+, K^+, Ca^{2+}, Mg^{2+} ions in rain samples were made. From this wer can predict rain pH.

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A Scientific Study for Physical Properties of Celadon in Firing Experiment (소성실험을 통한 청자의 물리적 특성 변화 연구)

  • Han, Min-su;Hong, Jong-Uk;Park, Ji-hee
    • 보존과학연구
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    • s.27
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    • pp.145-163
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    • 2006
  • This study is to be investigated through firing experiment in studio in order to reveal a physical properties of celadon according to change firing temperature. The results can be briefly summarized as below; Firstly, in measurement of color chromaticity, samples of first firing in body were effective in differentiating of changed color in samples from each other but there of second firing were not. The color of the glaze was more effective change than that of the body. Secondly, bulk density of body was increased with temperature and it was attained highest point in $1200^{\circ}C$ Additionally, water absorption ratio was most rapidly changed between $1000^{\circ}C$ and $1200^{\circ}C$Thirdly, in the microstructural analysis, body of samples in first firing have not specific characteristics in the changed patterns of microstructure. body and glaze of samples in second firing have many that. Consequently, we knew that this experiment can be provided researcher with physical properties and firing mechanisms of celadon.

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A Study on the Sound Absorption Coefficient by Varying Sample Size (시편의 크기에 따른 흡음계수 변화 연구)

  • 정성수;이우섭;조문재;서상준
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.11 no.5
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    • pp.83-88
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    • 2001
  • The sound absorption coefficient of glass wool (bulk density of 48 kg/m:1 and 32 kg/m7) was measured by reverberation room method as varying their cross-sectional area. The results show that the absorption is larger for smaller samples because of edge effect. The absorption coefficient with two different kinds of sources. 1/.7-octave band and while noise, gives similar values.

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