• Restorative Dentistry and Endodontics
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• 제44권4호
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• pp.37.1-37.10
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• 2019

Objectives: This study evaluated the bond strength of various fiberglass post cementation techniques using different resin-based composites. Materials and Methods: The roots from a total of 100 bovine incisors were randomly assigned to 5 treatment groups: G1, post + Scotchbond Multi-Purpose (SBMP) + RelyX ARC luting agent; G2, relined post (Filtek Z250) + SBMP + RelyX ARC; G3, individualized post (Filtek Z250) + SBMP; G4, individualized post (Filtek Bulk-Fill) + SBMP; G5, individualized post (Filtek Bulk-Fill Flow) + SBMP. The samples were subjected to the push-out (n = 10) and pull-out (n = 10) bond strength tests. Data from the push-out bond strength test were analyzed using 2-way analysis of variance (ANOVA) with the Bonferroni post hoc test, and data from the pull-out bond strength test were analyzed using 1-way ANOVA. Results: The data for push-out bond strength presented higher values for G2 and G5, mainly in the cervical and middle thirds, and the data from the apical third showed a lower mean push-out bond strength in all groups. No significant difference was noted for pull-out bond strength among all groups. The most frequent failure modes observed were adhesive failure between dentine and resin and mixed failure. Conclusions: Fiberglass post cementation using restorative and flowable bulk-fill composites with the individualization technique may be a promising alternative to existing methods of post cementation.

• The Journal of Advanced Prosthodontics
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• 제6권5호
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• pp.372-378
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• 2014

PURPOSE. The porcelain fused to gold has been widely used as a restoration both with the natural esthetics of the porcelain and durability and marginal fit of metal casting. However, recently, due to the continuous rise in the price of gold, an interest towards materials to replace gold alloy is getting higher. This study compared the bond strength of porcelain to millingable palladium-silver (Pd-Ag) alloy, with that of 3 conventionally used metal-ceramic alloys. MATERIALS AND METHODS. Four types of metal-ceramic alloys, castable nonprecious nickel-chrome alloy, castable precious metal alloys containing 83% and 32% of gold, and millingable Pd-Ag alloy were used to make metal specimens (n=40). And porcelain was applied on the center area of metal specimen. Three-point bending test was performed with universal testing machine. The bond strength data were analyzed with a one-way ANOVA and post hoc Scheffe's tests (${\alpha}=.05$). RESULTS. The 3-point bending test showed the strongest ($40.42{\pm}5.72$ MPa) metal-ceramic bond in the nonprecious Ni-Cr alloy, followed by millingable Pd-Ag alloy ($37.71{\pm}2.46$ MPa), precious metal alloy containing 83% of gold ($35.89{\pm}1.93$ MPa), and precious metal alloy containing 32% of gold ($34.59{\pm}2.63$ MPa). Nonprecious Ni-Cr alloy and precious metal alloy containing 32% of gold showed significant difference (P<.05). CONCLUSION. The type of metal-ceramic alloys affects the bond strength of porcelain. Every metal-ceramic alloy used in this study showed clinically applicable bond strength with porcelain (25 MPa).

• The Journal of Advanced Prosthodontics
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• 제12권5호
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• pp.291-298
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• 2020

PURPOSE. The aim of this study is to evaluate the influence of repeated surface treatments on wettability and surface roughness for zirconia surface and bond strength of zirconia-based ceramics to resin cement. MATERIALS AND METHODS. Seventy blocks (10 × 10 × 3 mm) of zirconia-based ceramics were fabricated and divided into two groups according to the surface treatments: (A) 110 ㎛ Al₂O₃ airborne-particle abrasion and (R) 110 ㎛ silica modified Al₂O₃ airborne-particle abrasion. At stage 2, each group was subdivided into 5 groups according to the surface retreatments: (a) 110 ㎛ Al₂O₃ airborne-particle abrasion, (r) 110 ㎛ silica modified Al₂O₃ airborne-particle abrasion, (D) diamond bur, (Da) diamond bur + 110 ㎛ Al₂O₃ airborne-particle abrasion, and (Dr) diamond bur + 110 ㎛ silica modified Al₂O₃ airborne-particle abrasion. Cylinders of self-adhesive resin cement were cemented onto each treated ceramic surface and subjected to micro-shear bond strength test. Additional specimens were prepared for roughness and wettability analyses. The data were subjected to t-test and One-way ANOVA followed by Tukey's post hoc test (α=.05). RESULTS. At stage 1, group R presented higher bond strength values than group A (P=.000). There was a statistically significant increase of bond strength at stage 2 for group A (P=.003). The diamond bur influenced the surface roughness, increasing the values (P=.023). Group R provided better wettability. Regardless of the applied surface treatment, most of failures were adhesive. CONCLUSION. The combination of application and reapplication of Rocatec Plus showed the best results of bond strength. Surface retreatment and recementation might be an indicated clinical strategy.

• The Journal of Advanced Prosthodontics
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• 제6권3호
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• pp.151-156
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• 2014

PURPOSE. To investigate the microtensile bond strength between two all-ceramic systems; lithium disilicate glass ceramic and zirconia core ceramics bonded with their corresponding glass veneers. MATERIALS AND METHODS. Blocks of core ceramics (IPS e.max$^{(R)}$ Press and Lava$^{TM}$ Frame) were fabricated and veneered with their corresponding glass veneers. The bilayered blocks were cut into microbars; 8 mm in length and $1mm^2$ in cross-sectional area (n = 30/group). Additionally, monolithic microbars of these two veneers (IPS e.max$^{(R)}$ Ceram and LavaTM Ceram; n = 30/group) were also prepared. The obtained microbars were tested in tension until fracture, and the fracture surfaces of the microbars were examined with fluorescent black light and scanning electron microscope (SEM) to identify the mode of failure. One-way ANOVA and the Dunnett's T3 test were performed to determine significant differences of the mean microtensile bond strength at a significance level of 0.05. RESULTS. The mean microtensile bond strength of IPS e.max$^{(R)}$ Press/IPS e.max$^{(R)}$ Ceram ($43.40{\pm}5.51$ MPa) was significantly greater than that of Lava$^{TM}$ Frame/Lava$^{TM}$ Ceram ($31.71{\pm}7.03$ MPa)(P<.001). Fluorescent black light and SEM analysis showed that most of the tested microbars failed cohesively in the veneer layer. Furthermore, the bond strength of Lava$^{TM}$ Frame/Lava$^{TM}$ Ceram was comparable to the tensile strength of monolithic glass veneer of Lava$^{TM}$ Ceram, while the bond strength of bilayered IPS e.max$^{(R)}$ Press/IPS e.max$^{(R)}$ Ceram was significantly greater than tensile strength of monolithic IPS e.max$^{(R)}$ Ceram. CONCLUSION. Because fracture site occurred mostly in the glass veneer and most failures were away from the interfacial zone, microtensile bond test may not be a suitable test for bonding integrity. Fracture mechanics approach such as fracture toughness of the interface may be more appropriate to represent the bonding quality between two materials.

• 한국건설순환자원학회논문집
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• 제4권4호
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• pp.454-462
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• 2016

지오폴리머 콘크리트는 콘크리트 생산과정에서 발생하는 이산화탄소 배출을 감소시킬 수 있는 대안의 하나로 고려되는 새로운 건설재료이다. 지오폴리머 콘크리트의 재료 개발 및 재료 특성 연구는 많이 진행되고 있으나, 이의 구조부재 적용에 대한 연구는 미흡한 실정이다. 이 논문은 지오폴리머 콘크리트에 매입된 철근의 부착특성에 대한 것으로 압축강도 수준 20, 30 및 40MPa 지오폴리머 콘크리트에 대하여 공칭지름 10,16 및 25mm 철근을 매입한 실험체에 대한 연구를 수행하였다. 총 27개의 시험체를 제작하여 EN10080의 규정에 따라 부착강도 및 부착-슬립 관계를 계측한 내용을 정리한 것이다. 실험결과에 따르면, 압축강도 증가에 따라 부착강도가 증가하는 것을 확인하였고, 일반 콘크리트와 유사하게 철근의 지름이 증가함에 따라 부착강도는 감소하였다. 또한, 이 실험의 결과에 근거하여 지오폴리머 콘크리트에 매입된 철근의 기본 정착길이 산정식을 제안하였다.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2008년도 춘계 학술발표회 제20권1호
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• pp.1089-1092
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• 2008

철근과 콘크리트의 부착성능 확보는 철근콘크리트 구조물의 거동에서 중요한 요구사항이다. 구조체에 순환 잔골재 콘크리트를 적용하기 위해 순환 잔골재 콘크리트와 철근의 부착거동에 대한 규명이 매우 중요하다. 이에 따라 본 연구에서는 순환잔골재를 사용한 콘크리트와 철근 상호간의 부착거동을 평가하기 위하여 직접인발 실험을 수행하였다. 연구를 수행함에 있어 실험에 사용된 변수는 0, 100%의 순환잔골재 치환율 및 철근의 위치(상단근, 중간근, 하단근)로 하였다. 실험 결과는 CEB-FIP가 규정한 부착강도와 비교하였다. 본 연구를 통하여 얻어진 실험결과를 종합해 보면, 순환잔골재 콘크리트와 철근의 부착거동은 순환 잔골재 치환율 및 철근 위치에 영향을 받는다. H type 시험체의 경우 블리딩 현상이 일어나 V type 시험체와 HB 시험체만이 CEB-FIP가 규정한 부착강도를 만족하였다.

• 대한토목학회논문집
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• 제26권2A호
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• pp.285-292
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• 2006

이 연구는 탄소섬유쉬트-콘크리트 부착이음 실험 결과로부터 국부적인 부착모텔(부착응력-미끄럼 모델)을 결정하는 방법을 제안하고, 실제 실험 결과와 비교하여 이러한 부착 조건에 적용 기능한 부착모델을 제시한다. 부착모델의 형상은 임의의 곡선 형태를 고려할 수 있도록 디중선형곡선(multi-linear curve)으로 가정하였으며, 수치적인 방법으로 부착이음의 해를 계산하여 실험 결과와 오차를 최소화하는 방법으로 부착모델을 결정하였다. 이중선형곡선(bilinear curve)을 도입한 부착모델 역시 최적화를 수행하여 다중선형모텔과 비교하였다. 최적화의 대상은 동일 조건의 부착모텔에 대해 여러 실험체로부터 구한 극한하중-부착길이 곡선과 개별 실험체의 하중-변위 곡선이다. 최적화를 위한 정식화는 physical programming을 사용하였으며 최적화 방법은 유전알고리즘(genetic algorithm)을 이용하였다.

• 콘크리트학회논문집
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• 제25권2호
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• pp.155-163
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• 2013

이 연구는 도넛형 이방향 중공슬래브에 매입된 이형철근의 부착특성 및 부착강도 산정을 위한 기초적인 연구이다. 도넛형 이방향 중공슬래브의 철근 부착특성 및 부착강도 산정을 위해 pull-out test를 수행하였다. 도넛형 중공형성체는 슬래브 내부에 배치되어 철근과 중공형성체 사이에 내부의 피복이 형성된다. 이러한 내부피복두께는 외부피복두께보다 상대적으로 작은 피복두께를 가지며 중공형상에 따라 $2.5d_b$보다 작은 내부피복두께가 형성되기 때문에 철근의 부착에 영향을 미치게 된다. 또한 중공형성체가 일정 간격으로 떨어져 배치되어 있으므로 인장철근을 감싸고 있는 피복두께의 조건이 철근의 길이방향으로 변하게 된다. 따라서 도넛형 이방향 중공슬래브의 부착특성을 알아보기 위해서 중공형성체 형상에 따라 부착구간을 구분하였다. 구간별로 내부피복두께에 따른 부착응력-슬립 관계를 확인하였으며, 중공형성체 전 구간에 걸친 부착응력분포를 확인하여 철근의 길이방향에 따른 부착응력의 발현정도를 확인하였다. 또한 구간별 부착응력-슬립 관계를 기반으로 하여 도넛형 중공슬래브의 부착강도를 산정할 수 있는 부착강도 산정 방법을 제안하였다.

• 산업기술연구
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• 제21권B호
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• pp.295-300
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• 2001

Significant improvements in bond strength between new and existing concrete can be achieved through the modification of the new concrete by latex modification. But, no test method has been adopted as a standard to measure the bond strength between the concrete used to repair and the substrate being repaired. The performance of old and the new concrete construction defends upon band strength between old and the new concrete. Current adhesion strength measurement method is inaccurate method that ignore effect of stress concentration by shape of specimens. Therefore, this research calculates stress concentration coefficient using finite element analysis and direction tensile strength test (pull-off test). The result shows that the required core depth is 2.5 cm. Elastic modulus and overlay thickness do not influence in stress concentration.

• 대한기계학회논문집A
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• 제32권7호
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• pp.569-575
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• 2008

In this study, disk type of thermal barrier coating system for gas turbine blade was isothermally aged in the furnace changing exposure time and temperature. For each aging condition, bond tests for three samples were conducted for evaluating degradation of adhesive or cohesive strength of thermal barrier coating system. For as-sprayed condition, the location of fracture in the bond test was in the middle of epoxy which have bond strength of 57 MPa. As specimens are degraded by thermal aging, bond strength gradually decreased and the location of failure was also changed from within top coat at the earlier stage of thermal aging to the interface between top coat and TGO at the later stage due to the delamination in the coating.