• Title/Summary/Keyword: Bond test

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The effect of individualization of fiberglass posts using bulk-fill resin-based composites on cementation: an in vitro study

  • Lins, Rodrigo Barros Esteves;Cordeiro, Jairo Matozinho;Rangel, Carolina Perez;Antunes, Thiago Bessa Marconato;Martins, Luis Roberto Marcondes
    • Restorative Dentistry and Endodontics
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    • v.44 no.4
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    • pp.37.1-37.10
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    • 2019
  • Objectives: This study evaluated the bond strength of various fiberglass post cementation techniques using different resin-based composites. Materials and Methods: The roots from a total of 100 bovine incisors were randomly assigned to 5 treatment groups: G1, post + Scotchbond Multi-Purpose (SBMP) + RelyX ARC luting agent; G2, relined post (Filtek Z250) + SBMP + RelyX ARC; G3, individualized post (Filtek Z250) + SBMP; G4, individualized post (Filtek Bulk-Fill) + SBMP; G5, individualized post (Filtek Bulk-Fill Flow) + SBMP. The samples were subjected to the push-out (n = 10) and pull-out (n = 10) bond strength tests. Data from the push-out bond strength test were analyzed using 2-way analysis of variance (ANOVA) with the Bonferroni post hoc test, and data from the pull-out bond strength test were analyzed using 1-way ANOVA. Results: The data for push-out bond strength presented higher values for G2 and G5, mainly in the cervical and middle thirds, and the data from the apical third showed a lower mean push-out bond strength in all groups. No significant difference was noted for pull-out bond strength among all groups. The most frequent failure modes observed were adhesive failure between dentine and resin and mixed failure. Conclusions: Fiberglass post cementation using restorative and flowable bulk-fill composites with the individualization technique may be a promising alternative to existing methods of post cementation.

A comparative study on the bond strength of porcelain to the millingable Pd-Ag alloy

  • Hong, Jun-Tae;Shin, Soo-Yeon
    • The Journal of Advanced Prosthodontics
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    • v.6 no.5
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    • pp.372-378
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    • 2014
  • PURPOSE. The porcelain fused to gold has been widely used as a restoration both with the natural esthetics of the porcelain and durability and marginal fit of metal casting. However, recently, due to the continuous rise in the price of gold, an interest towards materials to replace gold alloy is getting higher. This study compared the bond strength of porcelain to millingable palladium-silver (Pd-Ag) alloy, with that of 3 conventionally used metal-ceramic alloys. MATERIALS AND METHODS. Four types of metal-ceramic alloys, castable nonprecious nickel-chrome alloy, castable precious metal alloys containing 83% and 32% of gold, and millingable Pd-Ag alloy were used to make metal specimens (n=40). And porcelain was applied on the center area of metal specimen. Three-point bending test was performed with universal testing machine. The bond strength data were analyzed with a one-way ANOVA and post hoc Scheffe's tests (${\alpha}=.05$). RESULTS. The 3-point bending test showed the strongest ($40.42{\pm}5.72$ MPa) metal-ceramic bond in the nonprecious Ni-Cr alloy, followed by millingable Pd-Ag alloy ($37.71{\pm}2.46$ MPa), precious metal alloy containing 83% of gold ($35.89{\pm}1.93$ MPa), and precious metal alloy containing 32% of gold ($34.59{\pm}2.63$ MPa). Nonprecious Ni-Cr alloy and precious metal alloy containing 32% of gold showed significant difference (P<.05). CONCLUSION. The type of metal-ceramic alloys affects the bond strength of porcelain. Every metal-ceramic alloy used in this study showed clinically applicable bond strength with porcelain (25 MPa).

The effect of repeated surface treatment of zirconia on its bond strength to resin cement

  • Maciel, Lucas Campagnaro;Amaral, Marina;Queiroz, Daher Antonio;Baroudi, Kusai;Silva-Concilio, Lais Regiane
    • The Journal of Advanced Prosthodontics
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    • v.12 no.5
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    • pp.291-298
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    • 2020
  • PURPOSE. The aim of this study is to evaluate the influence of repeated surface treatments on wettability and surface roughness for zirconia surface and bond strength of zirconia-based ceramics to resin cement. MATERIALS AND METHODS. Seventy blocks (10 × 10 × 3 mm) of zirconia-based ceramics were fabricated and divided into two groups according to the surface treatments: (A) 110 ㎛ Al2O3 airborne-particle abrasion and (R) 110 ㎛ silica modified Al2O3 airborne-particle abrasion. At stage 2, each group was subdivided into 5 groups according to the surface retreatments: (a) 110 ㎛ Al2O3 airborne-particle abrasion, (r) 110 ㎛ silica modified Al2O3 airborne-particle abrasion, (D) diamond bur, (Da) diamond bur + 110 ㎛ Al2O3 airborne-particle abrasion, and (Dr) diamond bur + 110 ㎛ silica modified Al2O3 airborne-particle abrasion. Cylinders of self-adhesive resin cement were cemented onto each treated ceramic surface and subjected to micro-shear bond strength test. Additional specimens were prepared for roughness and wettability analyses. The data were subjected to t-test and One-way ANOVA followed by Tukey's post hoc test (α=.05). RESULTS. At stage 1, group R presented higher bond strength values than group A (P=.000). There was a statistically significant increase of bond strength at stage 2 for group A (P=.003). The diamond bur influenced the surface roughness, increasing the values (P=.023). Group R provided better wettability. Regardless of the applied surface treatment, most of failures were adhesive. CONCLUSION. The combination of application and reapplication of Rocatec Plus showed the best results of bond strength. Surface retreatment and recementation might be an indicated clinical strategy.

Tensile strength of bilayered ceramics and corresponding glass veneers

  • Anunmana, Chuchai;Champirat, Tharee;Jirajariyavej, Bundhit
    • The Journal of Advanced Prosthodontics
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    • v.6 no.3
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    • pp.151-156
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    • 2014
  • PURPOSE. To investigate the microtensile bond strength between two all-ceramic systems; lithium disilicate glass ceramic and zirconia core ceramics bonded with their corresponding glass veneers. MATERIALS AND METHODS. Blocks of core ceramics (IPS e.max$^{(R)}$ Press and Lava$^{TM}$ Frame) were fabricated and veneered with their corresponding glass veneers. The bilayered blocks were cut into microbars; 8 mm in length and $1mm^2$ in cross-sectional area (n = 30/group). Additionally, monolithic microbars of these two veneers (IPS e.max$^{(R)}$ Ceram and LavaTM Ceram; n = 30/group) were also prepared. The obtained microbars were tested in tension until fracture, and the fracture surfaces of the microbars were examined with fluorescent black light and scanning electron microscope (SEM) to identify the mode of failure. One-way ANOVA and the Dunnett's T3 test were performed to determine significant differences of the mean microtensile bond strength at a significance level of 0.05. RESULTS. The mean microtensile bond strength of IPS e.max$^{(R)}$ Press/IPS e.max$^{(R)}$ Ceram ($43.40{\pm}5.51$ MPa) was significantly greater than that of Lava$^{TM}$ Frame/Lava$^{TM}$ Ceram ($31.71{\pm}7.03$ MPa)(P<.001). Fluorescent black light and SEM analysis showed that most of the tested microbars failed cohesively in the veneer layer. Furthermore, the bond strength of Lava$^{TM}$ Frame/Lava$^{TM}$ Ceram was comparable to the tensile strength of monolithic glass veneer of Lava$^{TM}$ Ceram, while the bond strength of bilayered IPS e.max$^{(R)}$ Press/IPS e.max$^{(R)}$ Ceram was significantly greater than tensile strength of monolithic IPS e.max$^{(R)}$ Ceram. CONCLUSION. Because fracture site occurred mostly in the glass veneer and most failures were away from the interfacial zone, microtensile bond test may not be a suitable test for bonding integrity. Fracture mechanics approach such as fracture toughness of the interface may be more appropriate to represent the bonding quality between two materials.

An Experiment on Bond Behaviours of Reinforcements Embedded in Geopolymer Concrete Using Direct Pull-out Test (직접 인발 시험을 이용한 지오폴리머 콘크리트의 부착 특성 실험)

  • Kim, Jee-Sang;Park, Jong-Ho
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.4 no.4
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    • pp.454-462
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    • 2016
  • Geopolymer concrete is a new class of construction materials that has emerged as an alternative to ordinary Portland cement concrete to reduce the emission of $CO_2$ in the production of concrete. Many researches have been carried out on material developments of geopolymer concrete, however a few studies have been reported on the structural use of them. This paper presents an experiment on the bond behaviors of reinforcements embedded in fly ash based geopolymer concrete. The development lengths of reinforcement for various compressive strength levels of geopolymer concrete, 20, 30 and 40 MPa, and reinforcement diameters, 10, 16 and 25 mm, are investigated. Total 27 specimens were manufactured and pull-out test according to EN 10080 was applied to measure the bond strength and slips between concrete and reinforcements. As the compressive strength levels of geopolymer concrete increase, the bond strength between geopolymer concrete and reinforcement increase. The bond strengths decrease as the diameters of reinforcements increase, which is similar in normal concrete. Also, an estimation equation for the basic development length of reinforcement embedded in geopolymer concrete is proposed based on the experimental results in this study.

The Bond Behavior between Deformed bars and Recycled Fine Aggregate Concrete according to Bar Position. (철근 위치에 따른 이형철근과 순환잔골재 콘크리트의 부착거동)

  • You, Young-Chan;Jang, Yong-Heon;Lee, Min-Jung;Yun, Hyun-Do;Choi, Ki-Sun;Lee, Do-Heun
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.04a
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    • pp.1089-1092
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    • 2008
  • The bond behavior between concrete and reinforcement is a important requirement for reinforced concrete constructions. For practical application, it is very important to study bond behavior of reinforcing bars in recycled fine aggregate concrete. Therefore, pull-out test in order to investigate the bond behavior between recycled fine aggregate concrete and deformed bars was performed. Recycled fine aggregate concrete replacement ratios (i.e., 0% and 100%) and positions of deformed bars (i.e., vertical and horizontal position) were considered as variables in this study. Test results were compared with the bond strength requirement recommended by CEB-FIP code. Based on the test results, It was found that the bond strength between the recycled fine aggregate concrete and deformed bars were influenced by both recycled fine aggregate concrete replacement ratios and positions of deformed bars. The reduction of bonded area at the soffit of horizontal reinforcement caused by concrete bleeding was observed in H type specimen. So, Only V type and HB specimen satisfied the bond strength requirement recommended by CEB-FIP code.

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Bond-Slip Model for CFRP Sheet-Concrete Adhesive Joint (탄소섬유쉬트-콘크리트 부착이음의 부착 모델)

  • Cho, Jeong-Rae;Cho, Keunhee;Park, Young-Hwan;Park, Jong-Sup
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.26 no.2A
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    • pp.285-292
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    • 2006
  • In this study, a method determining the local bond-slip model from pure shear test results of CFRP sheet-concrete adhesive joints is proposed and local bond-slip models are presented. Adhesive joints with a specific bond-slip model, which is assumed as multi-linear curve in order to represent arbitary function, are solved numerically. The difference between the solution and test results are minimized for finding the bond-slip model. The model with bilinear curve is also optimized to verify the improvement of multi-linear model. The selected test results are ultimate load-adhesive length curves from a series of adhesive joints and load-displacement curves for each joint. The optimization problem is formulated by physical programming, and the optimized bond-slip model is found using genetic algorithm.

An Experimental Study for Bond Characteristics of Deformed Bar Embedded in Donut Type Biaxial Hollow Slab (도넛형 이방향 중공슬래브의 부착특성에 관한 실험적 연구)

  • Chung, Joo-Hong;Kang, Sung-Hoon;Lee, Seung-Chang;Choi, Chang-Sik;Choi, Hyun-Ki
    • Journal of the Korea Concrete Institute
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    • v.25 no.2
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    • pp.155-163
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    • 2013
  • This study investigated the bond characteristics of embedded deformed steel bar in donut type biaxial hollow slabs. The donut type hollow sphere make concrete inner cover formed between steel bar and hollow sphere due to the hollow shape and arrangement. Generally, inner cover was thinner than outer cover, and some part of donut type biaxial hollow slab has smaller inner cover thickness than $2.5d_b$. It was affected to the bond condition of deformed bar. Furthermore, inner cover thickness changes along the longitudinal deformed bar due to hollow shape. Therefore, donut type hollow slab was divided 3 regions according to the hollow shape such as insufficient region, transition region, sufficient region. Pull-out test were performed to find out the effect of bond condition by the region. Main parameters are inner cover thickness, embedded length and bond location. Bond characteristics of donut type biaxial hollow slab were confirmed through comparison of bond stress-slip relationship, maximum bond strength and bond stress distribution of each regions. And the calculation method of bond strength of donut type biaxial hollow slab was suggested based on the test results.

Proposal of Bond Strength Evaluation Method for Overlay Concrete at Field (유한요소해석을 이용한 현장 덧씌우기 콘크리트의 부착강도 평가 방법 제안)

  • Lee, Bong-Hak;Hong, chang-Woo;Lee, Joo-Hyung;Kim, Seong-Hwan
    • Journal of Industrial Technology
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    • v.21 no.B
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    • pp.295-300
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    • 2001
  • Significant improvements in bond strength between new and existing concrete can be achieved through the modification of the new concrete by latex modification. But, no test method has been adopted as a standard to measure the bond strength between the concrete used to repair and the substrate being repaired. The performance of old and the new concrete construction defends upon band strength between old and the new concrete. Current adhesion strength measurement method is inaccurate method that ignore effect of stress concentration by shape of specimens. Therefore, this research calculates stress concentration coefficient using finite element analysis and direction tensile strength test (pull-off test). The result shows that the required core depth is 2.5 cm. Elastic modulus and overlay thickness do not influence in stress concentration.

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Evaluation of Bond Strength of Isothermally Aged Plasma Sprayed Thermal Barrier Coating (플라즈마 용사 열차폐 코팅의 열화에 따른 접착강도 평가)

  • Kim, Dae-Jin;Lee, Dong-Hoon;Koo, Jae-Mean;Song, Sung-Jin;Seok, Chang-Sung;Kim, Mun-Young
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.32 no.7
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    • pp.569-575
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    • 2008
  • In this study, disk type of thermal barrier coating system for gas turbine blade was isothermally aged in the furnace changing exposure time and temperature. For each aging condition, bond tests for three samples were conducted for evaluating degradation of adhesive or cohesive strength of thermal barrier coating system. For as-sprayed condition, the location of fracture in the bond test was in the middle of epoxy which have bond strength of 57 MPa. As specimens are degraded by thermal aging, bond strength gradually decreased and the location of failure was also changed from within top coat at the earlier stage of thermal aging to the interface between top coat and TGO at the later stage due to the delamination in the coating.