• Title/Summary/Keyword: Bond Strength Test

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Improvement of bond strength and durability of concrete incorporating high volumes of class F fly ash

  • Wu, Chung-Hao;Chen, Chien-Jung;Lin, Yu-Feng;Lin, Shu-Ken
    • Advances in concrete construction
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    • v.12 no.5
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    • pp.367-375
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    • 2021
  • This study experimentally investigated the improvement of bond strength and durability of concrete containing high volume fly ash. Concrete mixtures made with 0%, 25% and 60% replacement of cement with class F fly ash were prepared. Water-binder ratios ranged from 0.28 to 0.72. The compressive, flexural and pullout bond strength, the resistance to chloride-ion penetration, and the water permeability of concrete were measured and presented. Test results indicate that except for the concretes at early ages, the mechanical properties, bond strength, and the durability-related chloride-ion permeability and water permeability of concrete containing high volume (60% cement replacement) fly ash were obviously superior to the concrete without fly ash at later ages of beyond 56 days. The enhanced bond strength for the high volume fly-ash concrete either with or without steel confinement is a significant finding which might be valuable for the structural application.

Effect of additional etching and ethanol-wet bonding on the dentin bond strength of one-step self-etch adhesives

  • Ahn, Joonghee;Jung, Kyoung-Hwa;Son, Sung-Ae;Hur, Bock;Kwon, Yong-Hoon;Park, Jeong-Kil
    • Restorative Dentistry and Endodontics
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    • v.40 no.1
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    • pp.68-74
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    • 2015
  • Objectives: This study examined the effects of additional acid etching on the dentin bond strength of one-step self-etch adhesives with different compositions and pH. The effect of ethanol wetting on etched dentin bond strength of self-etch adhesives was also evaluated. Materials and Methods: Forty-two human permanent molars were classified into 21 groups according to the adhesive types (Clearfil SE Bond [SE, control]; G-aenial Bond [GB]; Xeno V [XV]; Beauti Bond [BB]; Adper Easy Bond [AE]; Single Bond Universal [SU]; All Bond Universal [AU]), and the dentin conditioning methods. Composite resins were placed on the dentin surfaces, and the teeth were sectioned. The microtensile bond strength was measured, and the failure mode of the fractured specimens was examined. The data were analyzed statistically using two-way ANOVA and Duncan's post hoc test. Results: In GB, XV and SE ($pH{\leq}2$), the bond strength was decreased significantly when the dentin was etched (p < 0.05). In BB, AE and SU (pH 2.4 - 2.7), additional etching did not affect the bond strength (p > 0.05). In AU (pH = 3.2), additional etching increased the bond strength significantly (p < 0.05). When adhesives were applied to the acid etched dentin with ethanol-wet bonding, the bond strength was significantly higher than that of the no ethanol-wet bonding groups, and the incidence of cohesive failure was increased. Conclusions: The effect of additional acid etching on the dentin bond strength was influenced by the pH of one-step self-etch adhesives. Ethanol wetting on etched dentin could create a stronger bonding performance of one-step self-etch adhesives for acid etched dentin.

Comparative analysis of bond strength to root dentin and compression of bioceramic cements used in regenerative endodontic procedures

  • Maykely Naara Morais Rodrigues;Kely Firmino Bruno;Ana Helena Goncalves de Alencar;Julyana Dumas Santos Silva;Patricia Correia de Siqueira;Daniel de Almeida Decurcio;Carlos Estrela
    • Restorative Dentistry and Endodontics
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    • v.46 no.4
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    • pp.59.1-59.14
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    • 2021
  • Objectives: This study compared the Biodentine, MTA Repair HP, and Bio-C Repair bioceramics in terms of bond strength to dentin, failure mode, and compression. Materials and Methods: Fifty-four slices obtained from the cervical third of 18 single-rooted human mandibular premolars were randomly distributed (n = 18). After insertion of the bioceramic materials, the push-out test was performed. The failure mode was analyzed using stereomicroscopy. Another set of cylindrically-shaped bioceramic samples (n = 10) was prepared for compressive strength testing. The normality of data distribution was analyzed using the Shapiro-Wilk test. The Kruskal-Wallis and Friedman tests were used for the push-out test data, while compressive strength was analyzed with analysis of variance and the Tukey test, considering a significance level of 0.05. Results: Biodentine presented a higher median bond strength value (14.79 MPa) than MTA Repair HP (8.84 MPa) and Bio-C Repair (3.48 MPa), with a significant difference only between Biodentine and Bio-C Repair. In the Biodentine group, the most frequent failure mode was mixed (61%), while in the MTA Repair HP and Bio-C Repair groups, it was adhesive (94% and 72%, respectively). Biodentine showed greater resistance to compression (29.59 ± 8.47 MPa) than MTA Repair HP (18.68 ± 7.40 MPa) and Bio-C Repair (19.96 ± 3.96 MPa) (p < 0.05). Conclusions: Biodentine showed greater compressive strength than MTA Repair HP and Bio-C Repair, and greater bond strength than Bio-C Repair. The most frequent failure mode of Biodentine was mixed, while that of MTA Repair HP and Bio-C Repair was adhesive.

REGIONAL MICRO-SHEAR BOND STRENGTH TO DENTIN:EFFECTS OF DENTINAL HARDNESS, POSITION, AND REMAINING DENTIN THICKNESS (상아질의 경도, 위치 및 잔존 상아질 후경이 상아질에 대한 부위별 미세 전단결합강도에 미치는 영향)

  • Hwang, Seon-Seong;Im, Mi-Kyung;Lee, Yong-Keun
    • Restorative Dentistry and Endodontics
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    • v.23 no.1
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    • pp.401-412
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    • 1998
  • The aim of this study was to measure the regional micro-shear bond strength of dentin bonding agents to dentin, and to investigate the relationship between the micro-shear bond strength and two dentinal characteristics ; Vickers hardness and remaining dentin thickness. Twenty-four freshly extracted, noncarious human molars were selected for this study. The materials tested in this study consisted of two commercially available dentin bonding agents (MAC-BOND, ONE-STEP) and two restorative light-cured composite resins (AELITEFIL, Z100). The occlusal or side surface of tooth crown was sectioned to expose dentin, and the exposed surface was finally polished with # 600 sandpaper. Four groups of application methods were used combining the filling materials and the dentin bonding agents. The composite resin-attached tooth specimens were embeded in a cold cure acrylic resin, and were cut with a low speed diamond saw to the dimension of 1mm $\times$ 1mm. Nine specimens were obtained from each tooth. The cut specimens were divided into three groups depending on the position of the dentin bonding surface. The micro-shear bond strength, remaining dentin thickness, and dentinal hardness were measured. Experimental results were then statistically analyzed with ANOVA. t-test, Scheffe test, and regression analysis. From this experiment, the following results were obtained : 1. In the case of occlusal surface bonding, the pooled micro-shear bond strength of ONST-AELIT group (16.62 MPa) was significantly higher than that of MACB-AELIT group (9.91 MPa) (p<0.05). However, there was no significant difference in the micro-shear bond strength depending on the dentin position (p>0.05). 2. In the case of side surface bonding of crown, the pooled micro-shear bond strength of four different bonding groups was not significantly different among each other (p>0.05). However, in three of the test groups (ONST-AELIT, MACB-Z100, ONST-Z100), the micro-shear bond strength to the lower 1/3(III) position was significantly lower than that to middle 1/3(II) position of surface (p<0.05). 3. In the ONST-AELIT bonding group, the pooled micro-shear bond strength to the occlusal surface was significantly lower than that to the side surface of crown (p<0.05). 4. There was no significant correlation between the micro-shear bond strength and dentin hardness / remaining dentin thickness (p>0.05).

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An Experimental Study on the Bond Strength after Surface Treatment of Non-precious Metal Alloy for porcelain Crown (도재용 비금속합금의 표면처리에 따른 결합강도에 관한 실험적 연구)

  • So, Myung-Sub
    • Journal of Technologic Dentistry
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    • v.9 no.1
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    • pp.39-49
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    • 1987
  • This study done to evaluate some surface treatment methods in metal coping which can increase the bond strength between porcelain and metal. Therefore this experiment was performed according to the Mc Lean's Theory of bond strength between porcelain and strength between porcelain and metal. In the experiment the author measured respective thermal expansion coefficents in three types of metal(Tallasium, Vera Bond and Rexillium) and Vita Porcelain to get the differences in the coefficents between porcelain and metals. And using insteron testing machine, the author also performed Planar interface shear bond tests on the 45 specimens(15 specimens in oxide surface, rough surface and fine surface treatment methods respectively) to measure bond strength between metal and porcelain. The results Were as follows, 1. The differences in thermal expansion coefficients between three types of metal and Vita procelain: Talladium - $1.2\;10^{-6/0}\;C$, Vera Bond - $1.6\;10^{-6/0}\;C$, Rexillium - $1.9\;10^{-6/0}\;C$. 2. The bond strength in oxide surface on the Shear bond test was the lowest among the treatment methods. 3. There was no significant differences in treatment methods of rough surface of fine surface. 4. In the oxide surface treatment method, there were significant differences(P<0.05)between Vera bond and Rexillium, and between Talladium and Rexillium. 5. In the fine surface treatment, there was a significant difference(P<0.05)between Talladium and Rexillium.

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A STUDY ON THE BOND STRENGTH OF REPAIRED GLASS IONOMER CEMENTS (Repaired glass ionomer cement의 결합강도에 관한 연구)

  • Seo, Su-Jeong;Kim, Shin
    • Journal of the korean academy of Pediatric Dentistry
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    • v.23 no.2
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    • pp.347-355
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    • 1996
  • The purpose of this study was to compare the bond strengths of different kinds of glass ionomer cements (GIC), which is recently increasing the clinical application in the field of pediatric dentistry and measure the repaired bond strengths in order to examine the clinical applicabilty of partial repaired cases. By using one kind of the light cured type GIC and three kinds of the chemical cured type GIC, the bond strengths of the followings were compared : unrepaired group as control, repaired conditioning group, which was treated the repaired surface using 25% polyacrylic acid and repaired non-conditioning group without surface treatment. Three point bending test was performed under Universal Testing Machine in order to measure the compressive bond strengths. The results were as follows : 1. Light cured GIC had higher bond strength than chemical cured type GIC in both of repaired and unrepaired groups. 2. In repaired cases, all of the materials decreased the bond strength when compared to the control group. In the light cured type, the bond strength of repaired conditioning group decreased 31.6%, repaired non-conditioning group decreased 40.8%. In chemical cured types, the bond strength of repaired conditining group decreased 11.8%, repaired non-conditioning group decreased 20.9%. 3. All the materials, in the case of the chemical treatment on the repaired surface using 25% polyacrylic acid had higher bond strength than untreated but, lower than control group.

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Bond Strength Analysis of High Relative Rib Area Bars Using Decreasing Bearing Angle Theory (지압각 감소이론을 이용한 높은마디면적 철근의 부착강도 해석)

  • Yang, Seung-Yul;Seo, Dong-Min;Park, Young-Su;Hong, Gun-Ho;Choi, Oan-Chul
    • Proceedings of the Korea Concrete Institute Conference
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    • 2005.11a
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    • pp.185-188
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    • 2005
  • Bond between reinforcing bar and surrounding concrete is supposed to transfer load safely in the process of design of reinforced concrete structures. Bond strength of ribbed reinforcing bars tends to split concrete cover, by wedging action, or shear the concrete in front of the ribs. In this study, using a reducing bearing angle theory, bond strengths of beam end specimen are predicted. Values of bond strength obtained using the analytical model are in good agreement with the bond test results. The analytical model provides insight into bond mechanism and the effects of bearing angle on the bond strength of deformed bars to concrete.

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Bond Strength Properties of Antiwashout Underwater Concrete (수중 불분리성 콘크리트의 부착 강도 특성에 관한 연구)

  • 김명식;김기동;윤재범
    • Journal of the Korea Concrete Institute
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    • v.12 no.1
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    • pp.89-99
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    • 2000
  • The objective of this study is to investigate the bond strength properties of antiwashout underwater concrete. The arrangement of bars (vertical bar, horizontal upper bar, horizontal lower bar), condition of casting and curing (fresh water, sea water), type of fine aggregate (river sand, blended sand(river sand : sea sand = 1:1), and proportioning strength of concrete (210, 240, 270, 300, 330kgf/$\textrm{cm}^2$)are chosen as the experimental parameters. The test results(ultimate bond stress) are compared with bond and development provisions of the ACI Building Code(ACI 318-89) and proposed equations from previous research(which was proposed by Orangun et. al). The experimental results show that ultimate bond stress of antiwashout underwater concrete which arranged bar on the horizontal lower, used the blend sand, and was cast and cured in the fresh water are higher that other conditions. The ultimate bond stress were increased in proportion to {{{{( SQRT {fcu }) }}3 2. From this study, rational analytic formula for the ultimate bond stress are to be from compressive strength of concrete.

An Experimental Study on Flexural Tensile Strength and Bond Strength Between Concrete-to-Concrete (콘크리트의 휨인장강도 및 신·구콘크리트 사이의 부착강도에 관한 실험 연구)

  • Yang, In-Hwan;Yoo, Sung-Won;Seo, Jung-In
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.13 no.3 s.55
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    • pp.155-163
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    • 2009
  • The purpose of this paper is to investigate the bond strength between old and new concrete as well as flexural tensile strength of concrete. To achieve this purpose, a comprehensive experimental program has been set up and strength tests using a series of specimens have been carried out. The present study represents that the flexural bond strength between old and new concrete is much smaller than that of flexural tensile strength. The ratio of bond strength to flexural tensile strength ranged through 15~27%. It is seen that concrete-to-concrete bond strength has been affected by curing condition. Also, test results of tensile strength show that recommendation by ACI 363 committee is estimated to be more realistic than another recommendations for predicting tensile strength of concrete.

Influence of nano-structured alumina coating on shear bond strength between Y-TZP ceramic and various dual-cured resin cements

  • Lee, Jung-Jin;Choi, Jung-Yun;Seo, Jae-Min
    • The Journal of Advanced Prosthodontics
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    • v.9 no.2
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    • pp.130-137
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    • 2017
  • PURPOSE. The purpose of this study was to evaluate the effect of nano-structured alumina surface coating on shear bond strength between Y-TZP ceramic and various dual-cured resin cements. MATERIALS AND METHODS. A total of 90 disk-shaped zirconia specimens (HASS CO., Gangneung, Korea) were divided into three groups by surface treatment method: (1) airborne particle abrasion, (2) tribochemicalsilica coating, and (3) nano-structured alumina coating. Each group was categorized into three subgroups of ten specimens and bonded with three different types of dual-cured resin cements. After thermocycling, shear bond strength was measured and failure modes were observed through FE-SEM. Two-way ANOVA and the Tukey's HSD test were performed to determine the effects of surface treatment method and type of cement on bond strength (P<.05). To confirm the correlation of surface treatment and failure mode, the Chi-square test was used. RESULTS. Groups treated with the nano-structured alumina coating showed significantly higher shear bond strength compared to other groups treated with airborne particle abrasion or tribochemical silica coating. Clearfil SA Luting showed a significantly higher shear bond strength compared to RelyX ARC and RelyX Unicem. The cohesive failure mode was observed to be dominant in the groups treated with nano-structured alumina coating, while the adhesive failure mode was prevalent in the groups treated with either airborne particle abrasion or tribochemical silica coating. CONCLUSION. Nano-structured alumina coating is an effective zirconia surface treatment method for enhancing the bond strength between Y-TZP ceramic and various dual-cured resin cements.